Dimorphite Whitfield H J Journal of the Chemical Society, Dalton Transactions, Inorganic Chemistry 1973 (1973) 1737-1738 Crystal structure of the beta-form of tetraarsenic trisulphide Locality: synthetic _database_code_amcsd 0014106 CELL PARAMETERS: 11.2100 9.9000 6.5800 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 730.242 Density (g/cm3): 3.600 MAX. ABS. INTENSITY / VOLUME**2: 16.25990997 RIR: 1.471 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 15.62 48.74 5.6746 1 0 1 4 15.81 19.70 5.6050 2 0 0 2 16.17 39.09 5.4800 0 1 1 4 17.92 100.00 4.9500 0 2 0 2 18.02 7.56 4.9232 1 1 1 8 18.19 62.86 4.8775 2 1 0 4 20.82 10.55 4.2668 2 0 1 4 22.69 87.12 3.9184 2 1 1 8 23.85 35.76 3.7302 1 2 1 8 23.98 10.19 3.7102 2 2 0 4 27.10 27.31 3.2900 0 0 2 2 27.45 22.41 3.2493 3 0 1 4 27.60 48.79 3.2319 2 2 1 8 28.27 21.56 3.1569 1 0 2 4 28.92 71.90 3.0873 3 1 1 8 29.70 1.39 3.0076 1 1 2 8 30.30 71.21 2.9498 0 3 1 4 31.36 9.85 2.8527 1 3 1 8 31.46 38.84 2.8437 2 3 0 4 31.53 29.35 2.8373 2 0 2 4 32.68 12.47 2.7400 0 2 2 4 32.84 38.07 2.7275 2 1 2 8 33.22 9.63 2.6965 4 1 0 4 33.67 41.19 2.6616 1 2 2 8 34.79 41.59 2.5784 4 0 1 4 35.99 12.88 2.4951 4 1 1 8 36.38 25.03 2.4693 3 0 2 4 36.50 3.26 2.4616 2 2 2 8 39.40 4.51 2.2868 4 2 1 8 39.50 6.76 2.2812 1 3 2 8 39.73 19.37 2.2686 1 4 1 8 39.81 3.32 2.2641 2 4 0 4 40.84 2.52 2.2096 3 2 2 8 42.20 1.74 2.1414 0 1 3 4 42.21 67.48 2.1409 2 4 1 8 42.31 31.53 2.1361 4 3 0 4 42.60 3.41 2.1222 5 0 1 4 43.39 9.57 2.0855 4 1 2 8 43.62 6.01 2.0751 5 1 1 8 44.35 9.94 2.0425 2 0 3 4 44.60 1.73 2.0318 4 3 1 8 45.88 2.29 1.9778 0 4 2 4 45.90 7.56 1.9771 3 3 2 8 45.98 8.62 1.9740 1 2 3 8 46.34 2.33 1.9592 4 2 2 8 46.56 2.71 1.9505 5 2 1 8 46.63 6.85 1.9477 1 4 2 8 47.98 10.98 1.8960 0 5 1 4 48.20 5.37 1.8881 2 2 3 8 48.71 2.00 1.8695 1 5 1 8 48.74 3.01 1.8683 6 0 0 2 48.78 3.08 1.8669 2 5 0 4 48.83 13.11 1.8651 2 4 2 8 49.03 13.35 1.8579 3 1 3 8 49.18 1.31 1.8527 5 0 2 4 49.66 6.49 1.8359 6 1 0 4 49.93 8.86 1.8267 0 3 3 4 50.09 7.34 1.8211 5 1 2 8 50.63 12.61 1.8029 1 3 3 8 50.80 1.60 1.7973 6 0 1 4 50.84 1.10 1.7960 2 5 1 8 50.97 27.04 1.7916 4 3 2 8 51.16 8.36 1.7855 4 4 1 8 51.69 37.54 1.7684 6 1 1 8 51.74 3.68 1.7669 3 2 3 8 52.70 14.42 1.7368 2 3 3 8 53.02 19.90 1.7272 4 0 3 4 54.25 3.45 1.6908 3 5 1 8 54.72 3.57 1.6774 1 5 2 8 55.71 9.25 1.6500 0 6 0 2 56.42 1.67 1.6308 4 2 3 8 56.54 6.52 1.6276 1 0 4 4 56.61 1.40 1.6258 6 3 0 4 56.67 17.01 1.6242 1 4 3 8 56.69 1.21 1.6237 2 5 2 8 56.94 23.44 1.6171 4 5 0 4 56.99 2.64 1.6159 4 4 2 8 57.00 22.07 1.6155 5 3 2 8 57.18 2.14 1.6110 5 4 1 8 57.37 16.70 1.6060 1 1 4 8 58.23 4.25 1.5844 1 6 1 8 58.91 1.61 1.5678 5 0 3 4 59.19 1.92 1.5611 0 2 4 4 59.28 4.13 1.5587 2 1 4 8 59.40 1.06 1.5560 7 0 1 4 59.71 6.06 1.5485 5 1 3 8 59.92 3.32 1.5436 6 2 2 8 60.12 2.53 1.5389 2 6 1 8 60.20 2.75 1.5371 7 1 1 8 60.50 1.13 1.5303 4 3 3 8 62.10 2.66 1.4947 5 2 3 8 62.26 3.83 1.4912 6 4 0 4 62.63 1.25 1.4832 5 4 2 8 63.20 2.00 1.4712 3 6 1 8 63.27 8.45 1.4697 0 5 3 4 63.63 1.45 1.4623 1 6 2 8 63.88 1.27 1.4573 1 5 3 8 64.02 3.59 1.4543 6 4 1 8 64.17 3.61 1.4513 4 5 2 8 65.68 1.95 1.4217 2 5 3 8 66.59 4.81 1.4043 4 1 4 8 66.76 5.39 1.4013 8 0 0 2 68.38 1.37 1.3719 3 6 2 8 68.49 4.13 1.3700 0 4 4 4 69.17 10.86 1.3582 6 4 2 8 69.20 1.64 1.3576 8 1 1 8 69.48 5.53 1.3528 5 5 2 8 70.10 2.49 1.3425 2 7 1 8 71.48 1.41 1.3197 7 3 2 8 71.64 1.05 1.3173 7 4 1 8 72.29 2.16 1.3070 1 0 5 4 72.35 3.46 1.3061 6 3 3 8 72.45 1.17 1.3045 0 1 5 4 72.95 2.71 1.2968 3 7 1 8 73.18 1.22 1.2934 7 0 3 4 73.41 2.13 1.2898 8 3 0 4 73.45 1.03 1.2892 8 0 2 4 73.65 6.34 1.2863 3 4 4 8 73.99 1.69 1.2812 2 0 5 4 75.04 2.29 1.2658 2 7 2 8 75.05 3.37 1.2657 8 3 1 8 77.07 3.84 1.2375 0 8 0 2 78.12 1.14 1.2234 7 5 1 8 78.75 2.27 1.2152 1 3 5 8 79.28 1.67 1.2084 2 8 0 4 79.61 1.54 1.2042 7 3 3 8 80.03 2.06 1.1990 8 4 1 8 80.07 1.18 1.1985 3 5 4 8 80.50 2.20 1.1931 4 6 3 8 82.52 3.49 1.1690 5 4 4 8 82.88 1.69 1.1649 9 0 2 4 82.91 2.00 1.1645 7 5 2 8 83.14 3.08 1.1618 3 3 5 8 83.41 1.23 1.1587 1 6 4 8 83.45 3.18 1.1583 0 8 2 4 83.68 1.64 1.1558 1 4 5 8 83.73 1.43 1.1551 6 5 3 8 84.00 2.62 1.1521 1 8 2 8 84.53 2.41 1.1463 7 4 3 8 84.79 1.11 1.1434 8 4 2 8 85.12 2.28 1.1398 7 1 4 8 85.57 3.33 1.1349 5 0 5 4 85.67 2.81 1.1339 9 2 2 8 85.78 1.73 1.1327 3 7 3 8 85.84 1.23 1.1320 7 6 1 8 86.33 1.36 1.1269 8 5 1 8 86.59 1.02 1.1242 5 7 2 8 87.42 4.10 1.1157 4 8 1 8 87.76 1.14 1.1122 3 6 4 8 87.84 5.20 1.1114 6 7 1 8 88.34 1.14 1.1063 3 8 2 8 88.36 2.06 1.1062 5 2 5 8 88.50 2.02 1.1048 6 4 4 8 88.79 2.09 1.1019 5 5 4 8 89.94 1.72 1.0908 1 5 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.