data_global
_amcsd_formula_title 'Pd20Sb7'
loop_
_publ_author_name
'Wopersnow W'
'Schubert K'
_journal_name_full 'Journal of the Less-Common Metals'
_journal_volume 51 
_journal_year 1977
_journal_page_first 35
_journal_page_last 44
_publ_section_title
;
 Kristallstrukturen von Pd20Sb7 und Pd20Te7
 Note: isotypic with keithconnite
;
_database_code_amcsd 0014139
_chemical_formula_sum 'Pd20 Sb7'
_cell_length_a 11.734
_cell_length_b 11.734
_cell_length_c 11.021
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 120
_cell_volume 1314.147
_exptl_crystal_density_diffrn     11.299
_symmetry_space_group_name_H-M 'R -3'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  '2/3+x,1/3+y,1/3+z'
  '1/3+x,2/3+y,2/3+z'
  'y,-x+y,-z'
  '2/3+y,1/3-x+y,1/3-z'
  '1/3+y,2/3-x+y,2/3-z'
  '-x+y,-x,z'
  '2/3-x+y,1/3-x,1/3+z'
  '1/3-x+y,2/3-x,2/3+z'
  '-x,-y,-z'
  '2/3-x,1/3-y,1/3-z'
  '1/3-x,2/3-y,2/3-z'
  '-y,x-y,z'
  '2/3-y,1/3+x-y,1/3+z'
  '1/3-y,2/3+x-y,2/3+z'
  'x-y,x,-z'
  '2/3+x-y,1/3+x,1/3-z'
  '1/3+x-y,2/3+x,2/3-z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
Pd1   0.00000   0.00000   0.37740  -0.00051
Pd2   0.15050   0.96390   0.18810   0.00329
Pd3   0.20410   0.95170   0.93970   0.00203
Pd4   0.21330   0.97120   0.44810  -0.00063
Sb1   0.00000   0.00000   0.00000   0.00089
Sb2   0.19180   0.96130   0.68480   0.00266