Ca3.11 Na8 O17.52 U3.7 Gasperin M, Cousson A, He L, Jove J Journal of the Less-Common Metals 152 (1989) 339-348 Structure d'un Oxyde d'Uranium a Valence Mixte et Etude par Spectroscopie Mossbauer (237 Np) d'un Oxyde Isotype de Neptunium _cod_database_code 1001410 _database_code_amcsd 0014165 CELL PARAMETERS: 8.2580 8.2710 8.2500 90.000 91.780 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 563.219 Density (g/cm3): 4.324 MAX. ABS. INTENSITY / VOLUME**2: 42.00802651 RIR: 3.163 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.95 23.87 5.9264 -1 0 1 2 15.16 36.73 5.8425 1 1 0 4 15.17 37.10 5.8396 0 1 1 4 15.42 21.81 5.7451 1 0 1 2 21.49 75.47 4.1355 0 2 0 2 21.53 77.06 4.1270 2 0 0 2 21.55 76.91 4.1230 0 0 2 2 26.17 9.93 3.4058 -2 1 1 4 26.18 10.56 3.4041 -1 1 2 4 26.28 12.86 3.3914 -1 2 1 4 26.56 12.40 3.3564 1 2 1 4 26.72 9.38 3.3359 2 1 1 4 26.74 9.20 3.3343 1 1 2 4 30.16 52.30 2.9632 -2 0 2 2 30.60 100.00 2.9212 2 2 0 4 30.62 99.32 2.9198 0 2 2 4 31.14 45.63 2.8725 2 0 2 2 34.03 4.40 2.6346 -3 0 1 2 34.06 1.46 2.6325 -1 0 3 2 34.29 4.59 2.6150 1 3 0 4 34.30 4.59 2.6147 0 3 1 4 34.35 4.85 2.6107 3 1 0 4 34.38 4.88 2.6084 0 1 3 4 34.72 5.16 2.5839 1 0 3 2 36.14 2.34 2.4856 1 3 1 4 37.33 17.63 2.4087 -2 2 2 4 38.15 18.95 2.3592 2 2 2 4 40.34 2.77 2.2357 -3 1 2 4 40.36 2.90 2.2349 -2 1 3 4 40.60 5.96 2.2220 -3 2 1 4 40.63 1.23 2.2207 -1 2 3 4 40.67 2.69 2.2186 -2 3 1 4 40.67 2.59 2.2182 -1 3 2 4 41.05 2.82 2.1990 2 3 1 4 41.05 2.82 2.1985 1 3 2 4 41.17 1.86 2.1925 3 2 1 4 41.20 5.21 2.1913 1 2 3 4 41.48 2.67 2.1769 3 1 2 4 41.50 2.64 2.1761 2 1 3 4 43.78 25.55 2.0677 0 4 0 2 43.88 24.64 2.0635 4 0 0 2 43.92 24.44 2.0615 0 0 4 2 46.34 1.90 1.9592 -4 1 1 4 46.38 1.89 1.9576 -1 1 4 4 46.52 2.49 1.9523 -1 4 1 4 46.64 1.69 1.9475 3 3 0 4 46.66 1.86 1.9465 0 3 3 4 46.69 2.35 1.9456 1 4 1 4 47.03 1.85 1.9323 4 1 1 4 47.07 1.87 1.9308 1 1 4 4 48.73 10.33 1.8687 -4 0 2 2 48.76 8.97 1.8676 -2 0 4 2 49.29 15.51 1.8487 2 4 0 4 49.30 15.26 1.8483 0 4 2 4 49.36 15.37 1.8464 4 2 0 4 49.40 16.06 1.8450 0 2 4 4 50.04 5.94 1.8228 4 0 2 2 50.07 6.97 1.8217 2 0 4 2 51.25 1.66 1.7825 -3 2 3 4 51.45 1.47 1.7761 -3 3 2 4 51.46 1.32 1.7757 -2 3 3 4 52.40 1.33 1.7462 3 3 2 4 52.41 1.23 1.7458 2 3 3 4 52.67 1.57 1.7378 3 2 3 4 53.84 18.77 1.7029 -4 2 2 4 53.86 17.08 1.7021 -2 2 4 4 54.08 21.08 1.6957 -2 4 2 4 54.69 19.39 1.6782 2 4 2 4 55.06 19.99 1.6679 4 2 2 4 55.09 21.63 1.6672 2 2 4 4 56.00 1.07 1.6421 -4 1 3 4 56.02 1.06 1.6416 -3 1 4 4 56.54 1.02 1.6277 -4 3 1 4 56.58 1.06 1.6267 -1 3 4 4 56.58 1.27 1.6266 -3 4 1 4 56.60 1.37 1.6261 -1 4 3 4 56.76 1.06 1.6219 0 5 1 4 56.93 1.04 1.6174 0 1 5 4 57.05 1.44 1.6145 1 4 3 4 57.31 1.22 1.6077 1 0 5 2 61.17 1.95 1.5152 -5 2 1 4 61.87 1.15 1.4996 5 2 1 4 61.93 1.06 1.4984 1 2 5 4 62.71 6.06 1.4816 -4 0 4 2 63.71 11.59 1.4606 4 4 0 4 63.75 11.42 1.4599 0 4 4 4 64.93 4.90 1.4363 4 0 4 2 65.02 1.16 1.4343 -3 0 5 2 67.11 5.49 1.3948 -4 2 4 4 67.57 5.84 1.3864 -4 4 2 4 67.59 5.74 1.3859 -2 4 4 4 68.01 1.50 1.3785 0 6 0 2 68.17 1.86 1.3757 6 0 0 2 68.24 1.83 1.3743 0 0 6 2 68.64 4.08 1.3673 4 4 2 4 68.66 4.23 1.3669 2 4 4 4 69.25 5.00 1.3568 4 2 4 4 71.29 1.15 1.3228 5 2 3 4 71.64 3.05 1.3173 -6 0 2 2 71.70 3.01 1.3162 -2 0 6 2 72.26 6.43 1.3075 2 6 0 4 72.27 6.33 1.3074 0 6 2 4 72.40 5.88 1.3053 6 2 0 4 72.47 5.80 1.3042 0 2 6 4 73.20 3.01 1.2929 6 0 2 2 73.27 2.71 1.2920 2 0 6 2 75.79 3.37 1.2552 -6 2 2 4 75.85 3.53 1.2543 -2 2 6 4 76.17 3.14 1.2499 -2 6 2 4 76.68 3.20 1.2428 2 6 2 4 77.32 3.39 1.2340 6 2 2 4 77.39 3.34 1.2332 2 2 6 4 79.60 4.82 1.2044 -4 4 4 4 81.62 4.25 1.1796 4 4 4 4 83.21 1.30 1.1611 -6 0 4 2 83.25 1.67 1.1606 -4 0 6 2 84.53 2.03 1.1463 4 6 0 4 84.56 2.09 1.1459 0 6 4 4 84.61 2.29 1.1453 6 4 0 4 84.68 2.27 1.1446 0 4 6 4 87.21 2.47 1.1178 -6 2 4 4 87.24 2.96 1.1174 -4 2 6 4 87.88 3.32 1.1110 -6 4 2 4 87.94 3.21 1.1104 -2 4 6 4 88.05 2.96 1.1093 -4 6 2 4 88.07 3.12 1.1091 -2 6 4 4 89.04 3.65 1.0995 4 6 2 4 89.06 3.52 1.0993 2 6 4 4 89.37 3.18 1.0963 6 4 2 4 89.43 3.00 1.0957 2 4 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.