Volkovskite Rastsvetaeva R K, Andrianov V I, Genkina E A, Sokolova T N, Kashaev A A Kristallografiya 37 (1992) 326-333 Crystal structure of volkovskite KCa4B22O32(OH)10Cl*4H2O from Nepkii deposit (E. Siberia) Locality: Eastern Siberia _database_code_amcsd 0014191 6.50 23.96 6.62 95.68 119.6 90.59 P1 atom x y z Biso K .0227 .0230 .0367 3.58 Ca1 .8140 .1653 .6591 2.70 Ca2 .7182 .5818 .3904 2.53 Ca3 .4972 .9070 .0221 2.60 Ca4 .1926 .4890 .3451 2.48 B1 .042 .6116 .082 2.5 B2 .991 .8903 .108 2.5 B3 .303 .5999 .903 2.5 B4 .395 .9171 .427 2.4 B5 .767 .4715 .840 2.4 B6 .401 .1609 .155 2.5 B7 .241 .2651 .562 3.3 B8 .709 .1544 .058 2.5 B9 .221 .6127 .508 2.5 B10 .164 .7010 .331 3.1 B11 .573 .3701 .172 3.0 B12 .081 .4806 .748 2.5 B13 .872 .8044 .820 3.2 B14 .497 .4596 .006 2.6 B15 .138 .1719 .336 2.8 B16 .612 .5905 .803 2.4 B17 .840 .2894 .748 3.0 B18 .317 .1791 .763 2.6 B19 .813 .8979 .686 2.7 B20 .456 .7827 .983 3.1 B21 .678 .4582 .433 2.6 B22 .081 .9106 .519 2.3 O1 .139 .1532 .539 2.5 O2 .818 .9152 .905 2.6 O3 .036 .9164 .702 2.8 O4 .042 .5874 .280 2.5 O5 .918 .4879 .523 2.6 O6 .604 .4678 .610 2.5 O7 .141 .6033 .676 2.5 O9 .838 .5891 .856 2.6 O10 .541 .5987 .969 2.6 O11 .321 .9156 .591 2.7 O12 .245 .1670 .934 2.8 O13 .036 .6730 .111 2.7 O14 .784 .8357 .639 2.9 O16 .233 .9143 .195 2.7 O17 .723 .4752 .020 2.6 O18 .352 .1559 .333 2.8 O19 .274 .6724 .523 2.9 O20 .445 .5829 .571 2.5 O21 .622 .9214 .487 2.7 O22 .512 .4837 .227 2.6 O23 .008 .4723 .908 2.5 O24 .641 .1587 .227 2.6 O25 .920 .9014 .290 2.7 O27 .254 .5960 .078 2.5 O28 -.018 .8283 .049 2.9 O30 .555 .1579 .831 2.7 O31 .936 .1462 .114 2.5 O32 .130 .2341 .347 2.8 O33 .337 .2413 .763 3.2 O34 .701 .3982 .390 2.8 O37 .307 .4812 .801 2.6 O42 .461 .3974 .976 2.8 OH8 .903 .2542 .912 3.4 OH15 .533 .8172 .183 3.4 OH26 .369 .8120 .796 3.6 OH29 .571 .3126 .159 3.9 OH35 .860 .7473 .772 4.0 OH36 .244 .3229 .565 3.9 OH38 .737 .2598 .531 3.6 OH40 .866 .3462 .791 4.0 OH41 .187 .7581 .373 4.0 OH45 .467 .7261 .973 4.2 Cl .5288 .0224 .0627 3.46 Wat39 .717 .6778 .386 3.8 Wat43 .736 .0655 .601 3.7 Wat44 .276 .0422 .523 4.6 Wat46 .138 .3936 .249 3.8 H1 -.01 .243 .05 3.4 H2 .61 .813 .34 3.4 H3 .30 .795 .63 3.6 H4 .48 .289 .02 3.9 H5 .93 .726 .88 4. H6 .31 .348 .71 3.9 H7 .68 .276 .40 3.6 H8 .78 .355 .65 4. H9 .09 .777 .27 4. H10 .39 .709 .81 4.2 H11 .78 .699 .53 3.8 H12 .65 .684 .25 3.8 H13 .58 .058 .57 3.7 H14 .68 .051 .43 3.7 H15 .22 .077 .63 4.6 H16 .33 .027 .67 4.6 H17 .21 .370 .38 3.8 H18 .05 .377 .09 3.8