Quenstedtite Westland R E Master's Thesis, Queen's University 2012 (2012) 1-161 New phases in the hydrous ferric sulfate system, a supporting argument that the mineral lausenite is of formula Fe2(SO4)3*5H2O and the crystal structure refinement and hydrogen bonding scheme of the minerals quenstedtite and romerite Locality: Alcaparossa, Chile _database_code_amcsd 0021045 CELL PARAMETERS: 6.1741 23.5062 6.5282 85.633 101.553 83.745 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 918.034 Density (g/cm3): 2.163 MAX. ABS. INTENSITY / VOLUME**2: 4.451780603 RIR: 0.670 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 3.80 3.97 23.2477 0 1 0 2 7.61 9.00 11.6239 0 2 0 2 11.42 3.59 7.7492 0 3 0 2 13.92 4.06 6.3635 0 0 1 2 14.05 14.39 6.3012 0 1 1 2 14.76 6.71 5.9999 1 0 0 2 14.77 14.20 5.9970 1 1 0 2 14.80 1.97 5.9863 0 -1 1 2 15.19 3.86 5.8345 0 2 1 2 15.24 76.26 5.8119 0 4 0 2 15.72 12.12 5.6387 -1 1 0 2 15.74 28.16 5.6314 1 2 0 2 16.54 38.45 5.3593 0 -2 1 2 17.12 8.00 5.1800 0 3 1 2 17.47 26.56 5.0751 -1 2 0 2 17.51 29.83 5.0662 1 3 0 2 18.36 10.65 4.8316 -1 -1 1 2 18.56 19.60 4.7802 -1 1 1 2 18.91 3.95 4.6918 0 -3 1 2 19.09 2.56 4.6495 0 5 0 2 19.43 1.66 4.5679 -1 -2 1 2 19.83 9.53 4.4766 -1 3 0 2 19.87 28.91 4.4681 1 4 0 2 21.16 100.00 4.1991 -1 -3 1 2 21.68 88.91 4.0999 -1 3 1 2 21.72 25.40 4.0914 0 -4 1 2 22.16 9.65 4.0108 1 1 1 2 22.59 1.78 3.9365 1 2 1 2 22.61 6.95 3.9322 -1 4 0 2 22.66 2.25 3.9247 1 5 0 2 22.95 25.26 3.8746 0 6 0 2 23.29 67.98 3.8200 1 -1 1 2 23.64 18.52 3.7635 1 3 1 2 24.03 5.17 3.7035 -1 4 1 2 24.75 5.05 3.5976 1 -2 1 2 24.83 1.46 3.5863 0 -5 1 2 25.25 18.40 3.5274 1 4 1 2 25.69 20.64 3.4680 0 6 1 2 25.74 4.63 3.4617 1 6 0 2 26.70 10.09 3.3389 1 -3 1 2 26.75 2.26 3.3329 -1 5 1 2 27.32 23.88 3.2644 1 5 1 2 27.92 1.01 3.1958 0 1 2 2 28.04 23.54 3.1817 0 0 2 2 28.14 7.26 3.1708 0 -6 1 2 28.33 19.86 3.1506 0 2 2 2 28.70 3.72 3.1106 0 -1 2 2 28.97 1.83 3.0819 -1 -6 1 2 28.98 4.64 3.0813 -1 6 0 2 29.00 1.58 3.0792 -1 1 2 2 29.03 2.07 3.0761 1 7 0 2 29.05 11.52 3.0738 0 7 1 2 29.25 5.37 3.0534 -1 -1 2 2 29.25 1.67 3.0532 0 3 2 2 29.64 2.97 3.0135 -1 2 2 2 29.74 13.32 3.0037 -1 6 1 2 29.80 4.08 2.9985 2 2 0 2 29.85 1.46 2.9931 0 -2 2 2 30.08 8.15 2.9705 -2 -1 1 2 30.14 1.54 2.9648 -2 0 1 2 30.70 8.25 2.9124 -2 1 1 2 30.78 3.27 2.9053 -1 3 2 2 31.45 1.79 2.8449 -2 -3 1 2 31.48 1.06 2.8415 -1 -3 2 2 31.62 13.99 2.8298 0 -7 1 2 31.72 7.18 2.8209 1 -5 1 2 31.73 9.28 2.8201 -2 2 1 2 31.74 4.96 2.8193 -2 2 0 2 31.78 18.21 2.8157 2 4 0 2 32.13 13.00 2.7856 -1 -7 1 2 32.43 4.50 2.7608 -1 7 0 2 32.46 1.05 2.7583 0 5 2 2 32.95 18.18 2.7181 -1 7 1 2 33.19 6.03 2.6990 -2 3 1 2 33.44 2.39 2.6797 0 -4 2 2 34.30 1.75 2.6146 -1 5 2 2 34.37 14.91 2.6089 1 2 2 2 34.58 20.55 2.5942 -2 -5 1 2 34.58 23.41 2.5941 1 0 2 2 34.63 4.89 2.5900 0 6 2 2 34.65 4.31 2.5889 1 -6 1 2 35.04 9.10 2.5606 -2 4 1 2 35.22 1.59 2.5483 0 -8 1 2 35.30 3.83 2.5425 2 1 1 2 35.37 2.89 2.5375 -2 4 0 2 35.47 2.40 2.5305 -1 -8 1 2 35.51 3.22 2.5282 1 8 1 2 35.76 2.95 2.5107 0 -5 2 2 35.86 3.22 2.5040 2 3 1 2 35.93 4.33 2.4997 1 4 2 2 36.01 3.49 2.4939 -1 8 0 2 36.07 5.04 2.4903 1 9 0 2 36.47 1.38 2.4640 2 -1 1 2 36.51 1.04 2.4612 1 -2 2 2 36.69 10.31 2.4496 -2 -6 1 2 36.70 1.44 2.4491 -2 -1 2 2 36.78 2.02 2.4439 2 4 1 2 37.11 3.37 2.4225 0 7 2 2 37.22 1.73 2.4158 -2 -2 2 2 37.23 6.95 2.4151 -2 5 1 2 37.31 1.47 2.4102 1 5 2 2 37.63 2.76 2.3901 -2 2 2 2 37.66 1.43 2.3886 2 -2 1 2 37.70 2.95 2.3864 -2 5 0 2 38.06 1.71 2.3644 1 -3 2 2 38.37 1.77 2.3459 0 -6 2 2 38.93 1.90 2.3137 0 -9 1 2 39.10 1.20 2.3037 -2 -7 1 2 39.45 3.94 2.2840 -2 -4 2 2 39.71 8.16 2.2700 -1 9 0 2 40.24 2.91 2.2411 -2 4 2 2 40.37 1.05 2.2340 2 8 0 2 40.49 1.64 2.2280 -1 -7 2 2 41.11 1.87 2.1959 1 -8 1 2 42.06 1.76 2.1482 1 10 1 2 42.40 1.22 2.1319 0 1 3 2 42.44 1.16 2.1299 -2 7 1 2 42.55 1.28 2.1248 0 2 3 2 42.58 1.62 2.1231 -1 -10 1 2 42.62 1.53 2.1212 0 0 3 2 43.08 1.53 2.0995 -2 -6 2 2 43.31 1.34 2.0890 2 -5 1 2 43.51 1.74 2.0801 -1 10 1 2 43.75 1.52 2.0689 0 11 1 2 43.94 2.81 2.0605 0 4 3 2 44.14 3.16 2.0518 -1 4 3 2 44.17 1.32 2.0506 0 -2 3 2 44.18 1.08 2.0499 -2 6 2 2 44.54 2.14 2.0343 -3 0 1 2 44.68 8.23 2.0283 -2 -9 1 2 44.99 2.89 2.0149 -1 9 2 2 45.16 7.95 2.0076 0 5 3 2 45.29 1.41 2.0021 2 1 2 2 45.45 4.53 1.9954 0 -3 3 2 45.49 3.94 1.9939 2 3 2 2 46.08 2.45 1.9698 3 4 0 2 46.17 1.94 1.9661 -2 8 0 2 46.26 1.22 1.9624 2 10 0 2 46.32 1.87 1.9603 -1 -11 1 2 46.53 4.77 1.9520 -1 -9 2 2 46.71 2.16 1.9448 0 6 3 2 46.90 4.45 1.9373 0 12 0 2 47.06 1.29 1.9310 0 -4 3 2 47.29 1.12 1.9223 -3 3 1 2 47.39 3.24 1.9184 -1 11 0 2 47.45 3.52 1.9162 1 12 0 2 47.65 2.26 1.9086 -1 -5 3 2 47.78 1.25 1.9037 -2 -10 1 2 47.86 1.66 1.9007 -2 -8 2 2 48.03 2.75 1.8942 1 2 3 2 48.20 1.75 1.8879 -1 10 2 2 48.31 2.84 1.8839 -3 -1 2 2 48.39 2.96 1.8809 -3 0 2 2 48.48 1.09 1.8778 -3 -6 1 2 48.53 2.09 1.8758 -2 9 1 2 48.55 1.06 1.8753 0 7 3 2 48.56 6.58 1.8746 -3 -2 2 2 48.85 1.02 1.8644 -3 4 1 2 48.98 1.08 1.8599 1 4 3 2 49.03 1.33 1.8578 2 -3 2 2 49.13 1.20 1.8542 1 -1 3 2 49.20 2.24 1.8518 -2 8 2 2 49.22 3.86 1.8511 -1 7 3 2 49.30 1.35 1.8482 0 11 2 2 49.40 1.95 1.8449 -2 9 0 2 49.50 3.39 1.8415 2 11 0 2 49.56 3.82 1.8394 -3 2 2 2 49.94 3.04 1.8262 1 5 3 2 49.96 3.09 1.8255 2 7 2 2 50.07 2.57 1.8219 -3 -4 2 2 50.16 5.02 1.8188 1 -2 3 2 50.16 1.53 1.8187 -1 -12 1 2 50.17 2.12 1.8185 3 7 0 2 50.27 2.31 1.8151 -3 -7 1 2 50.61 1.13 1.8035 0 -12 1 2 50.70 3.11 1.8006 -3 5 1 2 50.95 1.84 1.7922 -2 5 3 2 51.21 3.76 1.7837 1 6 3 2 51.33 1.53 1.7799 -2 -5 3 2 51.43 3.27 1.7767 1 13 0 2 51.49 2.69 1.7748 1 -3 3 2 51.70 1.94 1.7681 3 5 1 2 51.85 2.20 1.7632 -2 10 1 2 51.93 1.00 1.7609 1 11 2 2 52.01 3.06 1.7584 -1 -7 3 2 52.06 1.93 1.7568 -2 9 2 2 52.11 2.87 1.7550 3 8 0 2 52.33 1.09 1.7483 -3 -8 1 2 52.47 2.15 1.7439 3 -2 1 2 52.68 1.57 1.7375 -2 6 3 2 52.75 3.97 1.7353 2 -5 2 2 52.81 1.28 1.7335 -3 -6 2 2 52.86 1.92 1.7319 3 6 1 2 53.12 1.73 1.7240 -2 -6 3 2 53.28 1.01 1.7194 -1 -11 2 2 53.98 1.54 1.6987 2 9 2 2 54.22 2.35 1.6917 -3 6 0 2 54.49 1.12 1.6841 0 -11 2 2 54.50 1.75 1.6837 -2 -12 1 2 54.63 1.28 1.6800 1 8 3 2 55.00 1.09 1.6695 2 -6 2 2 55.11 1.73 1.6665 -2 10 2 2 55.45 1.03 1.6571 -1 13 0 2 55.58 5.19 1.6535 -3 6 2 2 55.64 1.11 1.6519 0 10 3 2 55.78 1.51 1.6482 1 -12 1 2 56.35 1.70 1.6328 -2 11 0 2 56.46 1.03 1.6299 2 13 0 2 56.67 3.51 1.6242 -3 -8 2 2 56.71 2.14 1.6233 -2 -11 2 2 56.88 1.49 1.6188 1 14 1 2 57.16 3.03 1.6114 1 -6 3 2 57.20 1.91 1.6105 -3 -10 1 2 57.79 1.40 1.5953 -3 8 1 2 57.80 1.34 1.5953 2 -10 1 2 57.80 1.31 1.5952 2 3 3 2 57.85 5.37 1.5939 2 1 3 2 58.00 1.86 1.5902 0 3 4 2 58.81 3.40 1.5703 -1 13 2 2 58.87 1.41 1.5688 -1 -3 4 2 58.87 1.49 1.5687 0 -14 1 2 58.97 1.02 1.5663 -2 12 1 2 58.99 2.19 1.5659 2 11 2 2 59.09 3.05 1.5634 1 10 3 2 59.30 3.05 1.5584 3 4 2 2 59.55 2.14 1.5524 3 0 2 2 59.58 1.12 1.5516 3 -6 1 2 59.76 1.47 1.5475 1 -13 1 2 60.03 1.39 1.5412 -4 -1 1 2 60.64 2.20 1.5270 -1 -13 2 2 61.21 1.18 1.5143 2 7 3 2 61.49 1.01 1.5080 0 12 3 2 61.55 1.11 1.5067 -2 4 4 2 62.12 2.96 1.4942 -2 10 3 2 62.13 1.78 1.4939 0 -10 3 2 62.35 2.41 1.4894 -1 -15 1 2 62.65 1.56 1.4828 -2 -4 4 2 62.75 1.47 1.4807 -4 -6 1 2 62.79 1.05 1.4799 -2 -10 3 2 62.90 1.02 1.4777 -4 -3 2 2 63.01 2.11 1.4752 -4 3 1 2 63.14 4.80 1.4726 2 -9 2 2 63.41 1.79 1.4669 -1 15 1 2 63.62 2.91 1.4625 1 4 4 2 63.90 1.10 1.4568 -2 13 0 2 64.02 1.27 1.4544 2 15 0 2 64.11 1.09 1.4526 -2 6 4 2 64.13 1.52 1.4522 -4 -7 1 2 64.31 1.01 1.4485 0 16 1 2 64.86 2.80 1.4375 2 13 2 2 65.68 2.30 1.4216 -1 -7 4 2 65.78 3.47 1.4197 -1 9 4 2 66.69 1.60 1.4024 -2 14 1 2 67.08 1.74 1.3952 -4 -7 2 2 67.85 1.35 1.3812 -4 5 2 2 69.26 1.44 1.3566 4 7 1 2 69.83 1.35 1.3469 -4 -4 3 2 70.69 1.15 1.3326 1 14 3 2 72.06 1.30 1.3107 -2 15 0 2 72.18 1.32 1.3087 2 17 0 2 74.78 1.26 1.2696 1 -12 3 2 76.33 1.51 1.2476 -1 -11 4 2 76.47 1.07 1.2456 -1 13 4 2 77.29 1.55 1.2345 3 -12 1 2 78.66 1.26 1.2164 4 12 1 2 78.98 1.52 1.2122 2 17 2 2 80.91 1.06 1.1881 2 -11 3 2 81.34 1.23 1.1829 -3 3 5 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.