H10 O14 P2 Te Tl2 Averbuch-Pouchot M, Durif A Materials Research Bulletin 16 (1981) 71-76 Crystal data for two new phosphate-tellurates: Te(OH)6(Tl(H2PO4))2(Tl2(HPO4)) and Te(OH)6(Tl(H2PO4))2. Crystal structure of Te (O H)6 (Tl (H2 P O4))2. _cod_database_code 1007136 _database_code_amcsd 0014290 CELL PARAMETERS: 6.2850 14.7400 7.8440 90.000 113.380 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 667.010 Density (g/cm3): 4.094 MAX. ABS. INTENSITY / VOLUME**2: 38.08814507 RIR: 3.029 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.01 100.00 7.3700 0 2 0 2 13.69 37.90 6.4694 0 1 1 4 16.54 7.74 5.3580 -1 1 1 4 17.22 25.94 5.1502 0 2 1 4 19.54 42.86 4.5427 1 2 0 4 19.58 12.27 4.5342 -1 2 1 4 21.90 27.05 4.0584 0 3 1 4 23.27 80.92 3.8223 1 0 1 2 23.79 15.26 3.7406 1 3 0 4 23.82 81.00 3.7358 -1 3 1 4 24.05 1.01 3.7000 1 1 1 4 24.14 97.63 3.6861 -1 1 2 4 24.15 1.39 3.6850 0 4 0 2 24.73 17.16 3.6000 0 0 2 2 25.47 4.32 3.4972 0 1 2 4 26.26 24.63 3.3931 1 2 1 4 26.35 14.28 3.3825 -1 2 2 4 27.18 24.60 3.2803 0 4 1 4 27.58 7.34 3.2347 0 2 2 4 28.75 58.52 3.1055 1 4 0 4 28.77 7.52 3.1028 -1 4 1 4 29.05 91.24 3.0734 -2 1 1 4 29.61 20.66 3.0169 1 3 1 4 30.79 57.77 2.9039 0 3 2 4 30.94 1.78 2.8907 -2 2 1 4 31.00 8.53 2.8845 2 0 0 2 31.10 3.63 2.8757 -2 0 2 2 31.61 5.23 2.8308 2 1 0 4 32.83 32.59 2.7282 0 5 1 4 33.36 1.22 2.6861 2 2 0 4 33.45 1.53 2.6790 -2 2 2 4 33.85 8.69 2.6478 -1 4 2 4 34.16 5.84 2.6251 1 5 0 4 34.18 14.21 2.6235 -1 5 1 4 34.30 14.03 2.6141 -1 0 3 2 34.75 10.40 2.5818 1 1 2 4 34.84 2.41 2.5751 0 4 2 4 36.11 17.28 2.4875 2 3 0 4 36.19 4.96 2.4819 -2 3 2 4 36.36 2.02 2.4706 1 2 2 4 36.47 3.09 2.4637 -1 2 3 4 36.58 7.12 2.4567 0 6 0 2 37.62 1.05 2.3911 -2 4 1 4 37.99 4.52 2.3688 0 1 3 4 38.43 1.92 2.3421 2 1 1 4 38.59 10.95 2.3328 -2 1 3 4 38.63 5.35 2.3309 -1 5 2 4 38.93 4.57 2.3134 1 3 2 4 39.49 16.07 2.2820 0 2 3 4 39.51 6.07 2.2808 0 5 2 4 39.68 9.18 2.2714 2 4 0 4 39.76 11.63 2.2671 -2 4 2 4 39.90 2.84 2.2592 -1 6 1 4 39.92 12.98 2.2582 2 2 1 4 40.08 9.87 2.2498 -2 2 3 4 41.89 2.69 2.1565 0 3 3 4 42.02 6.91 2.1500 -2 5 1 4 42.31 1.37 2.1363 2 3 1 4 42.39 10.17 2.1321 -1 4 3 4 42.45 2.54 2.1292 -2 3 3 4 43.81 2.13 2.0666 1 6 1 4 43.92 3.06 2.0617 2 5 0 4 43.99 3.74 2.0585 -2 5 2 4 44.09 2.60 2.0541 -3 1 1 4 44.85 20.52 2.0211 0 7 1 4 45.08 15.42 2.0111 0 4 3 4 45.47 14.15 1.9947 2 4 1 4 45.47 8.16 1.9946 -3 2 2 4 45.61 12.98 1.9889 -2 4 3 4 45.88 6.59 1.9781 1 7 0 4 45.89 3.39 1.9774 -1 7 1 4 46.34 16.56 1.9593 1 5 2 4 46.39 11.56 1.9575 1 0 3 2 46.82 1.56 1.9404 1 1 3 4 46.94 11.09 1.9358 -1 1 4 4 47.42 13.16 1.9172 -3 0 3 2 47.58 3.07 1.9112 2 0 2 2 47.58 7.86 1.9110 -3 3 1 4 47.63 3.79 1.9091 -3 3 2 4 47.69 12.02 1.9068 3 1 0 4 47.78 1.94 1.9036 -2 0 4 2 47.85 2.88 1.9011 -3 1 3 4 48.00 1.82 1.8953 2 1 2 4 48.09 3.12 1.8919 1 2 3 4 48.20 3.93 1.8879 -2 1 4 4 48.21 3.31 1.8876 -1 2 4 4 48.69 9.34 1.8703 2 6 0 4 48.75 10.18 1.8679 -2 6 2 4 48.95 2.20 1.8607 3 2 0 4 49.10 7.08 1.8554 -3 2 3 4 49.26 3.82 1.8500 2 2 2 4 49.45 1.44 1.8431 -2 2 4 4 49.46 2.07 1.8426 -1 7 2 4 50.17 5.77 1.8185 1 3 3 4 50.19 1.94 1.8176 0 7 2 4 50.49 3.03 1.8076 -3 4 1 4 50.54 9.09 1.8060 -3 4 2 4 50.72 2.89 1.8000 0 0 4 2 51.02 15.77 1.7902 -1 6 3 4 51.14 4.69 1.7860 -3 3 3 4 51.18 4.13 1.7850 0 8 1 4 51.29 11.54 1.7812 2 3 2 4 51.48 7.58 1.7750 -2 3 4 4 52.11 6.18 1.7552 1 8 0 4 52.13 1.54 1.7547 -1 8 1 4 52.30 3.75 1.7493 -2 7 1 4 53.08 2.73 1.7254 -1 4 4 4 53.77 2.07 1.7048 3 4 0 4 53.91 2.70 1.7007 2 7 0 4 53.97 1.13 1.6989 -2 7 2 4 54.02 2.01 1.6975 3 0 1 2 54.06 4.74 1.6965 -3 5 1 4 54.27 2.43 1.6901 0 3 4 4 54.64 2.51 1.6798 -3 1 4 4 55.40 1.03 1.6585 -1 8 2 4 56.01 15.75 1.6419 1 7 2 4 56.93 3.00 1.6174 0 4 4 4 57.47 2.19 1.6037 2 5 2 4 57.64 2.61 1.5992 -2 5 4 4 57.66 1.09 1.5988 -3 3 4 4 57.73 1.10 1.5970 0 9 1 4 58.21 4.10 1.5849 -3 6 1 4 58.61 5.11 1.5752 -1 9 1 4 58.77 6.65 1.5712 -4 0 2 2 59.40 1.60 1.5560 2 1 3 4 59.54 4.48 1.5528 2 8 0 4 59.59 4.55 1.5514 -2 8 2 4 59.63 1.22 1.5505 -2 1 5 4 60.00 3.50 1.5418 3 4 1 4 60.22 3.04 1.5367 -4 2 2 4 61.01 2.57 1.5188 1 2 4 4 61.58 5.48 1.5060 -1 8 3 4 61.67 3.41 1.5041 -4 2 1 4 62.27 1.26 1.4909 2 3 3 4 62.28 4.26 1.4908 0 9 2 4 62.50 1.19 1.4861 -2 3 5 4 62.89 1.67 1.4778 -3 7 1 4 62.91 5.85 1.4773 -1 3 5 4 62.93 1.17 1.4769 -3 7 2 4 63.07 1.78 1.4740 0 10 0 2 63.42 6.34 1.4667 -3 5 4 4 63.51 3.57 1.4648 -3 0 5 2 63.57 3.51 1.4636 3 1 2 4 63.67 3.49 1.4615 0 8 3 4 63.98 2.83 1.4552 2 8 1 4 64.09 2.80 1.4529 -2 8 3 4 64.14 4.94 1.4520 0 6 4 4 64.62 2.30 1.4424 3 2 2 4 64.72 1.40 1.4402 2 4 3 4 64.84 1.31 1.4379 -4 0 4 2 64.90 2.45 1.4367 -3 2 5 4 64.94 1.09 1.4359 -2 4 5 4 64.97 1.11 1.4354 4 1 0 4 65.08 6.45 1.4332 0 1 5 4 65.23 4.93 1.4304 1 4 4 4 65.34 3.10 1.4281 1 10 0 4 65.35 1.53 1.4280 -1 4 5 4 65.54 1.92 1.4242 2 9 0 4 65.76 1.19 1.4200 3 7 0 4 65.86 2.46 1.4181 -4 4 1 4 65.97 1.63 1.4160 -4 4 3 4 66.01 1.47 1.4152 2 7 2 4 66.18 1.61 1.4121 -2 7 4 4 66.22 1.57 1.4113 -4 2 4 4 66.62 1.36 1.4037 -3 3 5 4 67.01 4.77 1.3965 3 6 1 4 67.71 3.96 1.3839 4 3 0 4 67.81 3.73 1.3821 2 5 3 4 67.92 3.46 1.3800 -4 3 4 4 68.02 3.36 1.3782 -2 5 5 4 68.06 1.60 1.3776 -3 8 1 4 68.10 3.50 1.3768 -3 8 2 4 68.19 2.15 1.3753 1 10 1 4 68.23 1.09 1.3746 -1 10 2 4 68.42 1.98 1.3712 -1 5 5 4 68.71 2.20 1.3661 3 4 2 4 68.83 1.13 1.3641 0 10 2 4 68.92 2.24 1.3625 -4 5 1 4 69.02 3.82 1.3606 -4 5 3 4 70.24 1.19 1.3401 -1 8 4 4 71.57 5.91 1.3184 -3 7 4 4 71.98 2.36 1.3118 4 1 1 4 72.03 4.20 1.3111 2 0 4 2 72.29 3.24 1.3070 -2 0 6 2 72.42 1.17 1.3050 -1 11 1 4 72.97 1.16 1.2965 4 2 1 4 73.28 2.02 1.2918 -4 2 5 4 73.34 1.56 1.2909 2 2 4 4 73.56 2.02 1.2876 0 8 4 4 73.60 2.11 1.2870 -2 2 6 4 73.70 1.69 1.2854 -3 9 1 4 75.17 3.64 1.2640 -1 11 2 4 75.33 1.97 1.2616 -1 2 6 4 75.73 1.57 1.2560 0 10 3 4 75.73 4.02 1.2559 2 7 3 4 75.74 1.15 1.2558 0 11 2 4 75.94 3.82 1.2530 -2 7 5 4 76.01 1.95 1.2520 2 10 1 4 76.11 1.42 1.2506 -3 2 6 4 76.12 1.82 1.2506 -2 10 3 4 76.27 2.59 1.2484 3 8 1 4 76.32 1.12 1.2478 -1 7 5 4 76.50 1.19 1.2453 -3 9 3 4 76.62 1.61 1.2436 2 9 2 4 76.77 1.67 1.2415 -2 9 4 4 76.80 2.83 1.2412 -4 7 1 4 76.81 3.31 1.2410 1 3 5 4 76.86 1.82 1.2402 4 4 1 4 76.90 3.20 1.2398 -4 7 3 4 77.17 2.00 1.2361 -4 4 5 4 77.38 2.09 1.2333 3 3 3 4 77.43 3.80 1.2326 -2 11 1 4 77.75 2.68 1.2283 0 12 0 2 78.59 2.01 1.2172 -5 0 1 2 78.92 3.34 1.2130 -5 3 3 4 79.05 1.07 1.2114 1 4 5 4 79.10 2.23 1.2107 -5 1 4 4 79.19 2.33 1.2096 -1 4 6 4 79.86 1.26 1.2011 -3 10 2 4 79.87 1.36 1.2010 -5 2 1 4 79.96 2.77 1.1999 -3 4 6 4 80.06 1.62 1.1986 -5 2 4 4 81.00 1.87 1.1870 1 8 4 4 81.08 1.64 1.1860 -5 4 2 4 81.58 1.61 1.1800 -4 8 1 4 82.43 1.14 1.1700 0 11 3 4 82.48 3.18 1.1694 1 12 1 4 82.56 1.45 1.1685 -3 10 3 4 82.81 1.38 1.1656 -3 5 6 4 86.12 1.20 1.1291 4 4 2 4 86.48 1.60 1.1254 -1 9 5 4 87.81 1.23 1.1117 -1 12 3 4 88.49 1.74 1.1049 -1 11 4 4 89.05 2.06 1.0994 3 11 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.