F2 Ga3 H10.5 N1.5 O12.5 P3 Loiseau T, Taulelle F, Ferey G Microporous Materials 9 (1997) 83-93 Crystal structure and solid-state nuclear magnetic resonance characterization of an oxyfluorinated three-dimensional framework gallophosphate with ULM-4 structural type. Structural relationships with (Ga As O4)-2 _cod_database_code 1000458 _database_code_amcsd 0014402 CELL PARAMETERS: 8.6740 10.1900 16.8260 90.000 94.210 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 1483.204 Density (g/cm3): 2.633 MAX. ABS. INTENSITY / VOLUME**2: 22.20841102 RIR: 2.746 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.16 18.83 8.7099 0 1 1 4 10.54 88.16 8.3903 0 0 2 2 11.16 100.00 7.9298 -1 0 1 2 13.43 50.06 6.5947 1 1 0 4 16.63 8.02 5.3318 -1 1 2 4 17.41 9.02 5.0950 0 2 0 2 17.56 1.07 5.0494 1 1 2 4 18.09 1.29 4.9034 0 1 3 4 18.20 1.19 4.8752 0 2 1 4 18.24 7.21 4.8627 -1 0 3 2 19.52 8.02 4.5474 1 0 3 2 20.23 1.96 4.3901 1 2 0 4 20.23 3.73 4.3886 -1 1 3 4 20.39 10.68 4.3549 0 2 2 4 20.72 7.08 4.2865 -1 2 1 4 21.18 1.74 4.1951 0 0 4 2 21.40 3.82 4.1526 1 1 3 4 22.33 1.64 3.9815 2 1 0 4 22.42 8.49 3.9649 -2 0 2 2 22.50 5.11 3.9508 -1 2 2 4 22.60 2.94 3.9341 -2 1 1 4 22.93 6.21 3.8793 0 1 4 4 23.31 6.85 3.8164 2 1 1 4 24.08 1.55 3.6950 -2 1 2 4 24.50 10.21 3.6329 -1 1 4 4 25.80 6.45 3.4532 1 1 4 4 26.59 2.38 3.3525 -2 1 3 4 26.78 1.96 3.3291 0 3 1 4 27.27 3.03 3.2703 -2 2 1 4 27.80 4.06 3.2094 -1 0 5 2 27.99 3.52 3.1877 0 1 5 4 28.23 29.11 3.1617 1 3 0 4 28.38 18.96 3.1448 2 1 3 4 28.53 5.71 3.1283 -2 0 4 2 29.93 3.07 2.9851 -1 3 2 4 30.56 3.34 2.9256 1 1 5 4 30.69 7.59 2.9127 -2 2 3 4 30.76 4.74 2.9066 2 0 4 2 30.80 1.69 2.9033 0 3 3 4 31.08 6.71 2.8774 -3 0 1 2 31.87 2.77 2.8077 3 0 1 2 32.00 2.92 2.7968 0 0 6 2 32.26 1.96 2.7746 3 1 0 4 32.33 3.04 2.7691 -3 1 1 4 33.22 6.15 2.6970 0 1 6 4 33.29 2.13 2.6916 -3 1 2 4 33.91 4.44 2.6433 -3 0 3 2 34.11 1.80 2.6282 -1 1 6 4 34.23 3.69 2.6198 2 3 1 4 35.07 3.87 2.5586 -3 1 3 4 35.08 3.60 2.5581 -1 3 4 4 35.23 3.64 2.5475 0 4 0 2 36.03 5.64 2.4930 1 3 4 4 36.08 2.91 2.4897 3 0 3 2 36.54 1.97 2.4590 3 2 1 4 36.61 2.21 2.4543 -2 3 3 4 36.65 1.07 2.4517 0 2 6 4 36.87 3.18 2.4376 0 4 2 4 37.07 3.02 2.4254 -1 4 1 4 37.68 6.31 2.3873 0 3 5 4 37.98 7.44 2.3692 2 3 3 4 38.82 1.09 2.3199 1 2 6 4 39.75 2.91 2.2677 1 0 7 2 40.21 1.28 2.2425 3 1 4 4 41.90 1.55 2.1563 -3 3 2 4 42.58 6.09 2.1233 -1 3 6 4 42.69 1.12 2.1179 -4 1 1 4 44.08 1.08 2.0545 0 1 8 4 44.28 2.20 2.0454 2 3 5 4 44.70 2.48 2.0275 -4 1 3 4 47.08 1.79 1.9301 -3 2 6 4 47.46 1.44 1.9158 2 4 4 4 48.39 1.46 1.8809 -3 1 7 4 49.64 1.29 1.8367 4 2 3 4 49.71 2.88 1.8343 -3 4 3 4 49.95 2.65 1.8258 -4 3 1 4 50.85 4.63 1.7957 1 0 9 2 51.31 4.40 1.7805 3 4 3 4 51.74 6.99 1.7669 -4 3 3 4 51.99 2.34 1.7589 -2 4 6 4 52.24 1.33 1.7509 0 2 9 4 52.43 1.20 1.7453 2 3 7 4 53.65 1.42 1.7082 5 0 1 2 53.99 3.55 1.6983 0 6 0 2 54.16 1.30 1.6936 1 2 9 4 55.18 1.50 1.6646 0 6 2 4 55.25 1.36 1.6625 -3 2 8 4 55.59 1.10 1.6531 4 0 6 2 55.82 1.74 1.6471 0 5 6 4 55.84 1.21 1.6463 2 1 9 4 57.07 1.39 1.6137 -3 4 6 4 58.11 2.13 1.5873 -1 2 10 4 58.12 1.14 1.5873 5 2 2 4 58.20 1.75 1.5851 -4 2 7 4 58.94 1.05 1.5671 -5 1 5 4 59.32 1.27 1.5579 4 4 3 4 61.97 2.06 1.4974 2 3 9 4 63.37 1.13 1.4677 1 4 9 4 63.68 1.18 1.4614 0 2 11 4 64.65 1.12 1.4418 6 0 0 2 64.96 1.11 1.4355 1 7 0 4 65.31 1.14 1.4288 -3 6 3 4 65.90 1.32 1.4173 5 3 4 4 66.33 2.15 1.4092 -4 2 9 4 66.66 1.76 1.4030 3 6 3 4 66.99 1.19 1.3969 5 4 2 4 67.07 1.25 1.3954 -4 4 7 4 69.82 1.47 1.3470 -1 2 12 4 70.71 2.01 1.3323 2 7 3 4 71.83 2.99 1.3143 5 3 6 4 72.06 1.23 1.3107 -6 1 6 4 74.85 1.02 1.2686 -3 5 9 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.