Nagashimalite Matsubara S Mineralogical Journal 10 (1980) 131-142 The crystal structure of nagashimalite, Ba4(V(3+),Ti)4[(O,OH)2|Cl|Si8B2O27] Locality: Mogurazawa mine, Kirya City, Gumma Prefecture, Japan _database_code_amcsd 0014423 CELL PARAMETERS: 13.9370 12.1220 7.1160 90.000 90.000 90.000 SPACE GROUP: Pmmn X-RAY WAVELENGTH: 1.541838 Cell Volume: 1202.208 Density (g/cm3): 4.116 MAX. ABS. INTENSITY / VOLUME**2: 19.00353234 RIR: 1.503 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.70 17.29 6.9685 2 0 0 2 13.97 11.56 6.3377 1 0 1 4 14.61 27.42 6.0610 0 2 0 2 15.78 7.43 5.6164 1 1 1 8 17.82 1.67 4.9788 2 0 1 4 19.24 1.36 4.6141 0 2 1 4 19.27 4.46 4.6055 2 1 1 8 20.27 10.77 4.3803 1 2 1 8 20.47 3.18 4.3380 3 1 0 4 22.86 3.40 3.8901 3 0 1 4 23.12 83.96 3.8472 2 2 1 8 24.03 27.73 3.7040 3 1 1 8 25.03 2.71 3.5580 0 0 2 2 25.35 4.10 3.5137 0 3 1 4 25.57 13.30 3.4843 4 0 0 2 26.89 65.95 3.3159 1 1 2 8 27.24 13.58 3.2738 3 2 1 8 28.16 58.95 3.1688 2 0 2 4 28.45 7.27 3.1374 2 3 1 8 28.52 7.35 3.1293 4 0 1 4 29.10 50.60 3.0684 0 2 2 4 29.13 5.01 3.0658 2 1 2 8 29.29 1.74 3.0488 3 3 0 4 29.47 41.23 3.0305 0 4 0 2 29.48 15.70 3.0299 4 1 1 8 29.57 100.00 3.0207 4 2 0 4 31.87 6.93 2.8082 2 2 2 8 31.93 11.14 2.8024 3 3 1 8 32.10 21.93 2.7882 0 4 1 4 32.19 14.73 2.7805 4 2 1 8 32.21 15.26 2.7791 2 4 0 4 32.55 6.24 2.7510 3 1 2 8 32.76 1.04 2.7340 1 4 1 8 32.97 10.20 2.7165 5 1 0 4 33.56 2.06 2.6703 0 3 2 4 34.19 18.87 2.6226 1 3 2 8 34.56 4.65 2.5954 5 0 1 4 34.65 63.39 2.5887 2 4 1 8 35.37 4.23 2.5379 5 1 1 8 36.02 2.02 2.4935 2 3 2 8 36.08 39.39 2.4894 4 0 2 4 37.62 18.03 2.3907 3 4 1 8 37.70 5.62 2.3859 5 2 1 8 38.50 3.31 2.3384 1 0 3 4 38.68 3.47 2.3279 0 1 3 4 38.90 11.59 2.3151 3 3 2 8 39.12 5.39 2.3027 4 2 2 8 39.27 2.74 2.2944 5 3 0 4 39.41 4.77 2.2866 4 4 0 4 39.60 3.12 2.2761 1 4 2 8 40.16 6.43 2.2455 2 0 3 4 40.85 4.75 2.2089 0 2 3 4 40.87 2.40 2.2082 6 0 1 4 40.87 5.82 2.2079 2 1 3 8 41.14 2.13 2.1942 5 0 2 4 41.22 5.08 2.1902 2 4 2 8 41.35 1.60 2.1837 5 3 1 8 41.43 2.67 2.1797 2 5 1 8 41.48 11.20 2.1770 4 4 1 8 41.57 3.76 2.1724 6 1 1 8 41.84 24.00 2.1591 5 1 2 8 42.04 1.02 2.1493 3 5 0 4 42.95 10.20 2.1056 2 2 3 8 43.48 7.71 2.0812 3 1 3 8 43.62 7.44 2.0748 6 2 1 8 43.81 4.60 2.0663 3 4 2 8 44.01 10.84 2.0575 3 5 1 8 44.28 4.91 2.0456 0 3 3 4 44.86 2.72 2.0203 0 6 0 2 45.47 2.64 1.9949 3 2 3 8 45.75 14.07 1.9831 1 5 2 8 46.21 1.90 1.9647 7 1 0 4 46.25 1.18 1.9628 2 3 3 8 46.70 5.59 1.9450 6 0 2 4 46.94 2.51 1.9356 4 1 3 8 47.13 21.21 1.9283 5 3 2 8 47.22 2.46 1.9249 1 6 1 8 47.33 3.67 1.9205 6 1 2 8 47.42 3.91 1.9174 7 0 1 4 47.44 2.38 1.9165 4 5 1 8 48.04 8.16 1.8938 7 1 1 8 48.63 1.42 1.8721 3 3 3 8 48.64 12.76 1.8721 2 6 1 8 48.75 3.62 1.8679 0 4 3 4 49.20 2.99 1.8520 6 2 2 8 49.44 4.48 1.8436 6 4 0 4 49.85 1.19 1.8293 5 5 0 4 50.59 24.44 1.8042 2 4 3 8 51.15 3.36 1.7860 7 3 0 4 51.19 17.11 1.7847 6 4 1 8 51.36 11.78 1.7790 0 0 4 2 51.83 3.18 1.7640 4 3 3 8 52.06 5.85 1.7569 0 6 2 4 52.35 12.88 1.7478 4 6 0 4 52.53 10.41 1.7421 8 0 0 2 52.85 7.91 1.7322 7 3 1 8 53.70 2.88 1.7070 0 2 4 4 53.71 1.50 1.7065 2 1 4 8 53.81 1.28 1.7036 2 6 2 8 54.03 3.66 1.6973 4 6 1 8 54.09 1.04 1.6955 0 5 3 4 54.54 2.20 1.6826 0 7 1 4 55.29 1.43 1.6614 3 0 4 4 55.36 1.16 1.6596 6 0 3 4 55.74 2.31 1.6491 5 3 3 8 55.85 10.00 1.6462 4 4 3 8 55.92 4.12 1.6443 6 1 3 8 56.19 1.83 1.6369 6 4 2 8 56.36 2.45 1.6325 6 5 1 8 56.57 7.19 1.6269 5 5 2 8 57.52 1.11 1.6023 3 2 4 8 57.58 6.23 1.6007 6 2 3 8 57.84 1.16 1.5942 5 6 1 8 57.90 1.49 1.5927 3 5 3 8 58.23 6.93 1.5844 4 0 4 4 59.76 2.90 1.5475 1 7 2 8 60.16 3.36 1.5380 0 6 3 4 60.25 1.05 1.5361 9 1 0 4 60.33 3.24 1.5342 0 4 4 4 60.39 13.07 1.5329 4 2 4 8 60.73 1.24 1.5250 7 0 3 4 60.73 1.87 1.5250 1 4 4 8 60.75 6.48 1.5246 4 5 3 8 60.76 1.14 1.5244 6 6 0 4 61.16 12.60 1.5152 0 8 0 2 61.18 2.62 1.5150 8 2 2 8 61.26 2.54 1.5131 7 1 3 8 61.38 1.79 1.5103 8 4 0 4 61.68 2.54 1.5039 7 5 1 8 61.77 3.82 1.5019 2 6 3 8 61.93 3.17 1.4983 2 4 4 8 62.29 1.91 1.4906 6 6 1 8 62.91 4.15 1.4774 8 4 1 8 62.96 1.48 1.4764 3 7 2 8 63.08 1.45 1.4737 1 8 1 8 63.96 5.04 1.4556 6 4 3 8 64.44 1.21 1.4460 9 3 0 4 65.41 3.52 1.4268 7 3 3 8 65.60 1.25 1.4232 0 0 5 2 65.92 1.27 1.4170 9 3 1 8 66.28 9.37 1.4103 9 1 2 8 66.51 1.12 1.4059 5 3 4 8 66.60 1.75 1.4041 8 0 3 4 66.60 1.34 1.4041 4 4 4 8 66.76 1.26 1.4012 6 6 2 8 66.90 1.35 1.3986 0 7 3 4 67.35 2.18 1.3903 8 4 2 8 67.39 3.95 1.3895 4 8 0 4 67.99 1.41 1.3787 1 2 5 8 68.52 1.23 1.3695 6 5 3 8 68.66 6.50 1.3670 2 8 2 8 69.10 7.29 1.3594 5 7 2 8 69.12 2.02 1.3589 2 2 5 8 69.43 2.71 1.3538 9 4 1 8 70.27 7.40 1.3396 9 3 2 8 70.54 2.45 1.3352 0 6 4 4 71.08 1.88 1.3263 8 3 3 8 71.55 1.53 1.3187 7 1 4 8 71.59 1.26 1.3181 2 3 5 8 72.31 1.47 1.3066 7 7 0 4 72.89 1.81 1.2977 10 0 2 4 73.11 6.67 1.2943 4 8 2 8 73.34 1.48 1.2909 7 5 3 8 73.44 1.22 1.2893 9 1 3 8 73.52 7.06 1.2882 0 4 5 4 73.57 5.00 1.2875 4 2 5 8 73.72 2.99 1.2851 7 7 1 8 73.90 2.75 1.2824 6 6 3 8 74.38 1.36 1.2753 5 5 4 8 74.56 1.08 1.2728 3 9 1 8 74.97 3.76 1.2668 2 4 5 8 75.01 5.11 1.2662 10 4 0 4 75.42 1.23 1.2604 7 3 4 8 75.44 1.46 1.2601 11 1 0 4 75.83 2.17 1.2545 1 9 2 8 76.15 1.14 1.2501 5 7 3 8 76.39 3.14 1.2468 4 6 4 8 76.40 1.75 1.2466 10 4 1 8 76.54 4.40 1.2447 8 0 4 4 76.82 2.32 1.2408 11 1 1 8 77.09 2.77 1.2372 4 9 1 8 77.98 5.21 1.2252 9 5 2 8 78.75 1.21 1.2153 7 4 4 8 78.98 1.09 1.2122 0 10 0 2 80.32 2.62 1.1953 6 8 2 8 80.60 1.42 1.1919 11 3 1 8 80.85 1.02 1.1888 7 8 1 8 81.77 1.38 1.1778 2 10 1 8 81.91 1.08 1.1762 1 1 6 8 82.49 1.38 1.1694 5 4 5 8 82.50 1.58 1.1692 2 0 6 4 82.97 1.23 1.1638 2 1 6 8 83.07 1.32 1.1626 9 1 4 8 83.87 3.44 1.1535 0 8 4 4 83.96 1.71 1.1526 7 1 5 8 84.07 1.77 1.1514 8 4 4 8 84.37 1.10 1.1480 2 2 6 8 84.38 1.49 1.1479 5 9 2 8 84.41 1.17 1.1476 2 6 5 8 84.42 1.51 1.1474 0 10 2 4 84.53 1.37 1.1463 12 0 1 4 84.65 2.05 1.1449 4 10 0 4 84.69 1.01 1.1445 7 7 3 8 84.80 2.64 1.1433 8 8 0 4 85.83 1.42 1.1322 2 10 2 8 87.28 1.16 1.1170 10 4 3 8 87.68 1.65 1.1130 7 3 5 8 87.70 1.03 1.1128 11 1 3 8 87.96 1.24 1.1102 4 9 3 8 88.06 1.75 1.1092 11 5 1 8 88.62 2.53 1.1036 4 6 5 8 89.19 2.81 1.0980 9 7 2 8 89.49 4.14 1.0951 4 8 4 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.