Holtite Hoskins B F, Mumme W G, Pryce M W Mineralogical Magazine 53 (1989) 457-463 Holtite, (Si2.25Sb0.75)B[Al6(Al0.43 Ta0.27[]0.30)O15(O,OH)2.25]: crystal structure and crystal chemistry Locality: Greenbrushes, Australia _database_code_amcsd 0014489 CELL PARAMETERS: 4.6914 11.8960 20.3830 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 1137.553 Density (g/cm3): 3.875 MAX. ABS. INTENSITY / VOLUME**2: 12.41035731 RIR: 1.043 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.61 100.00 10.2742 0 1 1 4 8.68 33.02 10.1915 0 0 2 2 14.89 9.28 5.9480 0 2 0 2 15.02 14.54 5.8999 0 1 3 4 17.26 19.12 5.1371 0 2 2 4 17.40 10.76 5.0957 0 0 4 2 20.81 6.04 4.2676 1 1 1 8 20.84 2.99 4.2616 1 0 2 4 22.16 2.31 4.0119 1 1 2 8 22.85 5.72 3.8924 0 3 1 4 22.98 5.29 3.8698 0 2 4 4 23.06 5.41 3.8564 0 1 5 4 24.56 6.30 3.6248 1 2 1 8 25.72 35.56 3.4642 1 2 2 8 25.81 20.56 3.4514 1 0 4 4 26.02 4.91 3.4247 0 3 3 4 26.23 1.41 3.3972 0 0 6 2 26.90 11.84 3.3147 1 1 4 8 27.54 47.28 3.2382 1 2 3 8 29.02 30.31 3.0772 1 0 5 4 29.83 6.99 2.9956 1 3 1 8 29.93 3.96 2.9852 1 2 4 8 29.99 5.62 2.9791 1 1 5 8 30.05 11.00 2.9740 0 4 0 2 30.30 29.46 2.9499 0 2 6 4 30.80 42.24 2.9030 1 3 2 8 31.33 2.16 2.8549 0 4 2 4 31.47 6.57 2.8424 0 3 5 4 31.63 3.37 2.8284 0 1 7 4 32.37 5.41 2.7661 1 3 3 8 32.54 1.60 2.7515 1 0 6 4 32.77 4.87 2.7331 1 2 5 8 33.43 18.76 2.6807 1 1 6 8 34.45 2.39 2.6034 1 3 4 8 34.93 5.89 2.5686 0 4 4 4 35.22 2.53 2.5479 0 0 8 2 36.03 9.25 2.4930 1 4 1 8 36.31 3.97 2.4740 1 0 7 4 36.85 5.48 2.4388 1 4 2 8 36.98 7.44 2.4310 1 3 5 8 37.12 5.91 2.4222 1 1 7 8 38.08 11.43 2.3632 0 5 1 4 38.20 5.05 2.3560 1 4 3 8 38.35 11.99 2.3470 0 3 7 4 38.37 3.33 2.3457 2 0 0 2 38.44 11.14 2.3420 0 2 8 4 38.64 2.78 2.3303 2 0 1 4 39.40 1.31 2.2869 2 1 1 8 39.42 1.01 2.2859 2 0 2 4 40.02 4.16 2.2530 1 4 4 8 40.17 1.17 2.2449 2 1 2 8 40.28 3.02 2.2390 1 0 8 4 40.30 1.63 2.2377 0 4 6 4 40.55 1.23 2.2248 0 1 9 4 41.02 3.04 2.2004 1 1 8 8 41.38 1.92 2.1821 2 2 0 4 41.42 3.24 2.1797 2 1 3 8 41.62 1.42 2.1697 2 2 1 8 42.26 3.25 2.1385 1 4 5 8 42.85 12.18 2.1105 1 5 1 8 43.10 10.27 2.0990 1 3 7 8 43.13 5.16 2.0974 2 1 4 8 43.17 11.63 2.0954 1 2 8 8 43.56 5.39 2.0776 2 2 3 8 43.57 2.67 2.0774 1 5 2 8 44.57 3.63 2.0331 2 0 5 4 44.74 1.76 2.0254 1 5 3 8 44.88 1.10 2.0197 1 4 6 8 44.90 6.77 2.0189 2 3 0 4 45.10 1.95 2.0102 1 1 9 8 45.13 2.88 2.0091 2 3 1 8 45.20 2.15 2.0060 2 2 4 8 45.25 3.33 2.0041 2 1 5 8 45.76 3.25 1.9827 0 6 0 2 45.82 9.97 1.9804 2 3 2 8 46.16 3.16 1.9666 0 3 9 4 46.67 4.10 1.9462 0 6 2 4 46.95 2.93 1.9353 2 3 3 8 46.96 3.23 1.9349 0 4 8 4 47.10 2.91 1.9293 1 2 9 8 47.13 1.92 1.9282 0 2 10 4 47.25 8.21 1.9239 2 2 5 8 47.73 6.96 1.9053 2 1 6 8 48.50 11.92 1.8770 2 3 4 8 49.35 1.35 1.8468 1 1 10 8 49.93 10.55 1.8267 2 0 7 4 50.15 2.25 1.8190 1 6 1 8 50.73 1.04 1.7997 1 5 6 8 51.40 15.28 1.7776 2 4 3 8 52.40 4.27 1.7462 2 2 7 8 52.74 3.81 1.7356 2 3 6 8 52.86 1.61 1.7321 2 4 4 8 54.16 1.13 1.6936 0 7 1 4 54.58 2.50 1.6813 0 4 10 4 54.69 5.37 1.6784 2 4 5 8 54.97 2.16 1.6704 2 5 0 4 55.10 1.94 1.6667 1 6 5 8 55.17 3.42 1.6648 2 5 1 8 55.38 4.27 1.6591 2 3 7 8 55.44 4.31 1.6574 2 2 8 8 55.51 2.86 1.6553 1 2 11 8 55.77 1.31 1.6484 2 5 2 8 56.43 4.02 1.6305 1 5 8 8 56.48 3.63 1.6293 2 0 9 4 56.75 2.50 1.6221 2 5 3 8 56.87 2.99 1.6191 2 4 6 8 57.05 1.95 1.6142 2 1 9 8 57.27 2.05 1.6086 1 6 6 8 58.11 3.97 1.5873 2 5 4 8 58.47 3.47 1.5785 1 7 2 8 58.87 4.69 1.5686 0 7 5 4 59.03 4.29 1.5647 0 6 8 4 59.42 1.10 1.5554 1 7 3 8 59.46 6.58 1.5545 0 1 13 4 59.72 1.82 1.5485 1 5 9 8 59.77 4.53 1.5472 1 6 7 8 59.97 1.61 1.5425 1 2 12 8 60.69 2.58 1.5259 2 1 10 8 61.40 1.06 1.5101 2 6 1 8 61.90 3.68 1.4990 2 5 6 8 62.04 1.10 1.4960 3 2 2 8 62.45 2.51 1.4871 1 0 13 4 62.46 3.85 1.4870 0 8 0 2 62.71 4.62 1.4815 1 3 12 8 62.88 2.78 1.4780 2 6 3 8 63.02 6.24 1.4750 0 4 12 4 63.26 6.58 1.4700 1 5 10 8 64.04 1.46 1.4540 2 0 11 4 64.18 4.64 1.4511 3 3 1 8 64.24 4.57 1.4499 3 2 4 8 64.28 5.22 1.4492 3 1 5 8 64.44 1.91 1.4459 1 7 6 8 64.60 1.54 1.4427 1 2 13 8 65.02 3.64 1.4344 2 3 10 8 65.30 4.06 1.4289 2 4 9 8 65.79 3.28 1.4195 2 6 5 8 66.07 1.28 1.4141 1 8 1 8 66.16 5.13 1.4125 2 2 11 8 66.61 1.25 1.4040 1 8 2 8 66.99 3.65 1.3969 2 5 8 8 67.50 2.43 1.3876 1 8 3 8 68.05 1.31 1.3777 3 0 7 4 68.40 1.35 1.3715 3 4 2 8 68.48 1.73 1.3701 3 3 5 8 68.69 1.36 1.3665 2 4 10 8 68.84 4.14 1.3638 2 7 2 8 68.93 2.59 1.3622 0 8 6 4 69.10 2.42 1.3593 0 7 9 4 69.28 1.76 1.3563 3 4 3 8 69.64 1.89 1.3501 0 1 15 4 70.50 8.78 1.3357 3 4 4 8 70.68 4.64 1.3328 3 0 8 4 72.15 1.31 1.3092 0 5 13 4 72.34 1.23 1.3063 2 4 11 8 72.41 2.66 1.3052 1 0 15 4 73.02 1.11 1.2958 2 1 13 8 73.27 2.36 1.2920 2 5 10 8 74.41 2.04 1.2749 1 2 15 8 74.44 3.33 1.2745 1 8 7 8 74.52 1.62 1.2733 2 2 13 8 75.62 2.12 1.2575 1 7 10 8 76.56 2.17 1.2444 3 5 5 8 76.83 1.08 1.2407 3 0 10 4 77.25 2.15 1.2350 2 8 3 8 79.66 1.04 1.2036 0 9 7 4 80.64 1.14 1.1914 1 9 6 8 80.79 2.44 1.1896 0 10 0 2 81.45 1.81 1.1816 0 10 2 4 81.51 1.00 1.1809 2 3 14 8 81.59 4.97 1.1800 0 5 15 4 82.13 2.51 1.1735 0 6 14 4 82.19 1.38 1.1729 4 0 0 2 82.22 1.43 1.1725 2 6 11 8 82.35 1.34 1.1710 0 4 16 4 82.84 2.03 1.1653 4 1 1 8 82.85 1.23 1.1652 4 0 2 4 83.34 1.45 1.1596 4 1 2 8 83.88 2.08 1.1535 2 2 15 8 85.05 1.83 1.1406 2 7 10 8 85.86 1.35 1.1319 3 5 9 8 86.68 1.68 1.1232 2 9 4 8 89.17 1.06 1.0983 4 3 4 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.