Crocoite Knight K S Mineralogical Magazine 64 (2000) 291-300 A high temperature structural phase transition in crocoite (PbCrO4) at 1068 K: crystal structure refinement at 1073 K and thermal expansion tensor determination at 1000 K Sample: the high temperature form at T = 1073 K Locality: Dundas, Tasmania _database_code_amcsd 0014540 CELL PARAMETERS: 8.7986 5.7342 7.2740 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 366.997 Density (g/cm3): 5.849 MAX. ABS. INTENSITY / VOLUME**2: 59.76380735 RIR: 3.327 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 15.81 2.14 5.6062 1 0 1 4 19.71 59.39 4.5032 0 1 1 4 20.18 16.02 4.3993 2 0 0 2 22.18 51.74 4.0087 1 1 1 8 23.63 18.33 3.7644 2 0 1 4 24.48 29.81 3.6370 0 0 2 2 25.52 100.00 3.4904 2 1 0 4 26.52 63.48 3.3612 1 0 2 4 28.36 92.01 3.1469 2 1 1 8 30.84 47.95 2.8997 1 1 2 8 31.20 47.02 2.8671 0 2 0 2 32.93 8.52 2.7201 3 0 1 4 35.65 15.17 2.5183 2 1 2 8 36.56 1.76 2.4576 3 1 1 8 37.44 7.65 2.4020 2 2 0 4 38.51 1.52 2.3375 1 0 3 4 39.51 14.21 2.2809 2 2 1 8 40.04 4.64 2.2516 0 2 2 4 41.39 28.44 2.1813 1 2 2 8 41.73 23.55 2.1646 1 1 3 8 42.62 17.96 2.1211 3 1 2 8 42.96 21.88 2.1055 4 0 1 4 44.09 6.33 2.0537 4 1 0 4 45.99 4.34 1.9733 3 2 1 8 48.73 9.17 1.8687 3 0 3 4 49.29 1.71 1.8486 0 3 1 4 50.17 1.09 1.8185 0 0 4 2 50.44 1.64 1.8091 1 3 1 8 51.30 3.41 1.7809 1 0 4 4 51.43 3.70 1.7768 3 1 3 8 52.18 4.45 1.7531 2 3 0 4 53.79 5.01 1.7043 2 3 1 8 53.91 3.24 1.7007 1 1 4 8 54.04 8.63 1.6970 4 2 1 8 55.29 3.42 1.6615 1 3 2 8 56.11 1.10 1.6390 5 1 1 8 58.44 1.15 1.5792 2 3 2 8 59.00 6.09 1.5656 3 2 3 8 60.65 1.44 1.5269 5 1 2 8 61.27 3.01 1.5128 1 2 4 8 62.80 1.79 1.4797 1 3 3 8 63.47 1.45 1.4656 3 3 2 8 65.06 1.52 1.4336 0 4 0 2 67.13 1.73 1.3944 6 1 1 8 67.80 1.55 1.3822 5 1 3 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.