Aschamalmite Callegari A M, Boiocchi M Mineralogical Magazine 73 (2009) 83-94 Aschamalmite (Pb6Bi2S9): crystal structure and ordering scheme for Pb and Bi atoms Locality: Susa Valley, Piedmont, Italy _database_code_amcsd 0014588 CELL PARAMETERS: 13.7190 4.1320 31.4190 90.000 90.940 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 1780.806 Density (g/cm3): 7.276 MAX. ABS. INTENSITY / VOLUME**2: 60.15520081 RIR: 2.692 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.63 15.81 15.7074 0 0 2 2 11.27 3.46 7.8537 0 0 4 2 16.93 1.63 5.2358 0 0 6 2 19.00 4.44 4.6712 -2 0 5 2 19.31 2.63 4.5955 2 0 5 2 22.47 1.14 3.9564 1 1 0 4 22.64 5.74 3.9277 -1 1 1 4 22.67 5.97 3.9231 1 1 1 4 23.16 2.55 3.8409 -1 1 2 4 23.21 1.64 3.8323 1 1 2 4 23.51 39.00 3.7839 -2 0 7 2 23.87 40.71 3.7274 2 0 7 2 24.01 9.37 3.7068 -1 1 3 4 24.08 9.00 3.6953 1 1 3 4 25.16 60.59 3.5401 -1 1 4 4 25.25 56.45 3.5267 1 1 4 4 25.96 100.00 3.4322 -2 0 8 2 25.98 22.43 3.4293 4 0 0 2 26.09 32.21 3.4151 -4 0 1 2 26.19 40.72 3.4030 4 0 1 2 26.34 92.54 3.3840 2 0 8 2 26.51 16.73 3.3619 -4 0 2 2 26.57 59.97 3.3551 -1 1 5 4 26.68 66.14 3.3408 1 1 5 4 26.70 15.03 3.3390 4 0 2 2 27.23 3.96 3.2749 -4 0 3 2 27.50 1.18 3.2433 4 0 3 2 28.21 6.05 3.1638 -1 1 6 4 28.34 6.68 3.1494 1 1 6 4 28.41 2.50 3.1415 0 0 10 2 28.50 20.45 3.1317 -2 0 9 2 28.89 27.48 3.0904 2 0 9 2 29.13 11.62 3.0657 3 1 0 4 29.63 30.38 3.0151 -3 1 2 4 29.75 48.32 3.0027 3 1 2 4 30.18 2.06 2.9608 1 1 7 4 30.29 85.32 2.9509 -3 1 3 4 30.47 88.28 2.9335 3 1 3 4 31.12 24.64 2.8740 -2 0 10 2 31.20 63.91 2.8665 -3 1 4 4 31.44 43.46 2.8452 3 1 4 4 31.52 23.45 2.8386 2 0 10 2 32.35 2.05 2.7672 -3 1 5 4 33.72 6.18 2.6583 -3 1 6 4 33.80 3.95 2.6519 -2 0 11 2 34.05 4.57 2.6329 3 1 6 4 34.21 1.94 2.6212 2 0 11 2 34.25 2.22 2.6179 0 0 12 2 34.34 2.04 2.6113 1 1 9 4 37.00 1.58 2.4295 -3 1 8 4 38.80 4.03 2.3208 -1 1 11 4 38.98 8.91 2.3104 1 1 11 4 39.49 1.18 2.2818 -5 1 1 4 40.19 3.93 2.2439 0 0 14 2 40.27 1.94 2.2394 -5 1 3 4 40.51 1.90 2.2266 5 1 3 4 41.26 42.73 2.1880 -1 1 12 4 41.45 38.28 2.1785 1 1 12 4 41.87 9.93 2.1573 -5 1 5 4 42.26 15.74 2.1385 5 1 5 4 42.29 4.11 2.1371 6 0 5 2 42.91 18.91 2.1079 -6 0 6 2 42.96 35.64 2.1052 -5 1 6 4 43.05 1.98 2.1012 -3 1 11 4 43.42 33.00 2.0842 5 1 6 4 43.45 18.13 2.0827 6 0 6 2 43.55 1.67 2.0783 3 1 11 4 43.81 25.12 2.0666 -1 1 13 4 43.82 64.24 2.0660 0 2 0 2 44.00 18.51 2.0579 1 1 13 4 44.16 16.29 2.0508 -6 0 7 2 44.23 19.69 2.0480 -5 1 7 4 44.74 17.72 2.0255 5 1 7 4 44.78 11.14 2.0237 6 0 7 2 45.57 1.22 1.9908 -4 0 13 2 46.24 20.14 1.9634 0 0 16 2 47.16 1.56 1.9270 -6 0 9 2 47.66 13.61 1.9080 -3 1 13 4 47.87 3.35 1.9002 5 1 9 4 47.92 2.88 1.8983 6 0 9 2 48.21 14.35 1.8877 3 1 13 4 48.87 2.44 1.8637 4 0 14 2 48.89 2.69 1.8631 -6 0 10 2 48.96 3.60 1.8603 -5 1 10 4 49.65 7.94 1.8363 5 1 10 4 49.71 4.00 1.8343 6 0 10 2 50.11 8.57 1.8203 -3 1 14 4 50.32 8.94 1.8133 -2 2 7 4 50.51 9.71 1.8070 2 2 7 4 50.68 10.66 1.8013 3 1 14 4 50.70 10.72 1.8005 -4 0 15 2 50.74 3.57 1.7992 -6 0 11 2 50.82 13.23 1.7965 -5 1 11 4 51.50 11.32 1.7745 4 0 15 2 51.56 7.25 1.7727 5 1 11 4 51.62 2.97 1.7706 6 0 11 2 51.62 3.27 1.7706 7 1 0 4 51.64 28.08 1.7701 -2 2 8 4 51.65 6.68 1.7697 4 2 0 4 51.66 6.26 1.7692 -7 1 1 4 51.71 9.23 1.7677 -4 2 1 4 51.76 11.11 1.7663 7 1 1 4 51.77 11.74 1.7660 4 2 1 4 51.85 26.81 1.7633 2 2 8 4 51.88 6.55 1.7623 -7 1 2 4 51.95 5.11 1.7602 -4 2 2 4 52.05 4.49 1.7569 4 2 2 4 52.07 5.77 1.7565 7 1 2 4 52.27 4.94 1.7501 -7 1 3 4 52.36 1.45 1.7473 -4 2 3 4 52.43 4.81 1.7453 0 0 18 2 52.55 1.25 1.7416 7 1 3 4 52.72 1.56 1.7362 -6 0 12 2 52.81 4.78 1.7335 -5 1 12 4 53.11 5.63 1.7245 -2 2 9 4 53.34 7.68 1.7175 2 2 9 4 53.39 5.80 1.7161 -4 0 16 2 53.44 1.51 1.7146 8 0 0 2 53.59 2.43 1.7102 5 1 12 4 53.68 3.56 1.7075 -8 0 2 2 53.88 7.32 1.7015 8 0 2 2 54.05 6.40 1.6966 -8 0 3 2 54.21 3.94 1.6920 4 0 16 2 54.36 6.56 1.6877 8 0 3 2 54.60 3.73 1.6809 -8 0 4 2 54.72 8.96 1.6775 -2 2 10 4 54.97 8.44 1.6704 2 2 10 4 55.00 1.62 1.6695 8 0 4 2 56.46 1.74 1.6298 -2 2 11 4 58.99 3.40 1.5658 -4 0 18 2 59.86 4.00 1.5452 4 0 18 2 60.82 1.57 1.5230 1 1 19 4 60.96 1.88 1.5199 0 2 14 4 61.90 4.19 1.4990 -4 0 19 2 62.53 2.32 1.4854 6 2 5 4 62.79 4.29 1.4799 4 0 19 2 63.00 10.17 1.4755 -6 2 6 4 63.42 9.99 1.4667 6 2 6 4 63.63 2.30 1.4623 -1 1 20 4 63.65 3.09 1.4620 -3 1 19 4 63.87 1.81 1.4575 1 1 20 4 63.97 9.31 1.4555 -6 2 7 4 64.31 3.89 1.4486 3 1 19 4 64.45 6.59 1.4457 6 2 7 4 65.59 12.36 1.4232 0 2 16 4 66.32 1.49 1.4093 -8 0 13 2 66.60 6.96 1.4042 -3 1 20 4 66.75 5.25 1.4015 -1 1 21 4 66.82 1.84 1.4001 -7 1 14 4 66.94 1.85 1.3978 6 2 9 4 66.98 7.30 1.3971 1 1 21 4 67.27 4.36 1.3917 3 1 20 4 67.50 2.13 1.3877 8 0 13 2 67.71 1.58 1.3838 4 2 14 4 67.72 1.75 1.3836 -6 2 10 4 67.92 2.40 1.3801 7 1 14 4 68.30 2.78 1.3733 -8 0 14 2 68.39 2.62 1.3717 6 2 10 4 68.57 4.20 1.3686 -9 1 7 4 68.94 5.41 1.3621 -7 1 15 4 69.21 7.18 1.3574 -4 2 15 4 69.25 2.63 1.3568 -6 2 11 4 69.27 3.17 1.3564 9 1 7 4 69.54 2.25 1.3518 8 0 14 2 69.62 2.81 1.3504 -1 3 4 4 69.63 5.15 1.3503 -9 1 8 4 69.67 2.64 1.3497 1 3 4 4 69.79 1.23 1.3475 10 0 4 2 69.88 7.83 1.3461 4 2 15 4 69.93 2.19 1.3452 -1 1 22 4 69.96 2.36 1.3448 -10 0 5 2 69.98 2.16 1.3444 6 2 11 4 70.10 7.81 1.3423 7 1 15 4 70.18 2.62 1.3411 1 1 22 4 70.28 3.30 1.3394 -1 3 5 4 70.33 3.47 1.3385 1 3 5 4 70.42 8.26 1.3370 9 1 8 4 70.51 1.78 1.3356 10 0 5 2 70.52 1.16 1.3354 2 0 23 2 70.65 3.78 1.3332 0 2 18 4 70.82 1.23 1.3304 -9 1 9 4 70.90 1.26 1.3292 -6 2 12 4 71.18 2.23 1.3247 -7 1 16 4 71.46 4.26 1.3201 -4 2 16 4 71.50 1.03 1.3194 8 2 0 4 71.71 2.57 1.3162 -8 2 2 4 71.71 3.59 1.3161 9 1 9 4 71.80 1.84 1.3147 -3 3 2 4 71.87 3.01 1.3137 3 3 2 4 71.88 5.28 1.3134 8 2 2 4 72.03 4.67 1.3111 -8 2 3 4 72.15 4.99 1.3092 -3 3 3 4 72.16 6.64 1.3091 -9 1 10 4 72.16 3.06 1.3090 4 2 16 4 72.25 5.28 1.3077 3 3 3 4 72.29 4.75 1.3070 8 2 3 4 72.40 2.51 1.3053 7 1 16 4 72.49 2.94 1.3039 -8 2 4 4 72.64 4.22 1.3016 -3 3 4 4 72.77 3.00 1.2996 3 3 4 4 72.84 1.30 1.2985 8 2 4 4 73.14 2.72 1.2940 9 1 10 4 73.20 1.74 1.2930 -1 1 23 4 73.42 2.02 1.2896 -2 0 24 2 73.63 1.81 1.2866 -9 1 11 4 73.94 1.52 1.2819 2 0 24 2 75.99 3.31 1.2523 -7 1 18 4 76.31 2.87 1.2479 -4 2 18 4 77.07 3.29 1.2374 4 2 18 4 77.34 2.84 1.2338 7 1 18 4 78.13 1.62 1.2233 -10 0 12 2 78.49 1.37 1.2185 -5 1 22 4 78.58 5.82 1.2175 -7 1 19 4 78.77 4.70 1.2150 -1 3 12 4 78.90 4.36 1.2133 1 3 12 4 78.90 3.80 1.2133 -4 2 19 4 79.18 1.13 1.2096 -5 3 5 4 79.40 2.05 1.2069 10 0 12 2 79.45 1.83 1.2063 5 3 5 4 79.66 2.18 1.2036 5 1 22 4 79.70 3.90 1.2031 4 2 19 4 79.76 1.02 1.2023 6 0 22 2 79.83 1.22 1.2014 -10 0 13 2 79.93 4.33 1.2002 -5 3 6 4 79.98 3.56 1.1996 7 1 19 4 80.25 3.94 1.1963 5 3 6 4 80.44 13.96 1.1938 11 1 0 4 80.49 2.84 1.1933 -2 0 26 2 80.52 3.26 1.1929 -1 3 13 4 80.61 1.30 1.1918 -11 1 2 4 80.65 2.58 1.1912 1 3 13 4 80.81 2.78 1.1893 -5 3 7 4 81.03 3.32 1.1866 2 0 26 2 81.18 2.51 1.1849 5 3 7 4 81.49 1.25 1.1811 -6 0 23 2 81.62 1.17 1.1796 -5 1 23 4 82.82 1.86 1.1655 5 1 23 4 82.93 1.39 1.1643 -8 2 13 4 83.31 2.00 1.1599 -3 3 13 4 83.71 2.14 1.1553 3 3 13 4 84.01 2.04 1.1520 8 2 13 4 84.29 1.23 1.1489 8 0 20 2 84.76 2.69 1.1437 -8 2 14 4 84.81 1.28 1.1432 5 3 10 4 85.16 1.62 1.1393 -3 3 14 4 85.60 1.86 1.1346 3 3 14 4 85.71 2.27 1.1334 -5 3 11 4 85.93 2.29 1.1312 8 2 14 4 86.16 1.28 1.1287 10 2 4 4 86.29 1.35 1.1274 5 3 11 4 86.32 2.35 1.1270 -10 2 5 4 86.37 1.14 1.1265 -7 3 1 4 86.44 2.07 1.1257 7 3 1 4 86.54 1.11 1.1247 -7 3 2 4 86.69 1.03 1.1232 7 3 2 4 86.84 1.81 1.1216 10 2 5 4 86.85 1.16 1.1215 2 2 23 4 89.61 2.16 1.0940 -2 2 24 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.