Munakataite Kampf A R, Mills S J, Housley R M Mineralogical Magazine 74 (2010) 991-998 The crystal structure of munakataite, Pb2Cu2(Se4+O3)(SO4)(OH)4, from Otto Mountain, San Bernardino County, California, USA Locality: Otto Mountain, San Bernardino County, California, USA _database_code_amcsd 0018306 CELL PARAMETERS: 9.8020 5.6750 9.2810 90.000 102.443 90.000 SPACE GROUP: P2_1/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 504.141 Density (g/cm3): 5.303 MAX. ABS. INTENSITY / VOLUME**2: 51.02568422 RIR: 3.133 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.24 19.16 9.5718 1 0 0 2 9.76 2.18 9.0630 0 0 1 2 11.91 4.22 7.4285 -1 0 1 2 14.84 12.20 5.9701 1 0 1 2 18.17 64.74 4.8815 1 1 0 4 18.45 3.06 4.8099 0 1 1 4 18.54 11.78 4.7859 2 0 0 2 19.01 2.36 4.6677 -2 0 1 2 19.79 65.62 4.4866 -1 0 2 2 22.81 7.79 3.8993 2 0 1 2 23.96 7.91 3.7142 -2 0 2 2 24.33 17.35 3.6586 2 1 0 4 25.15 52.90 3.5411 0 1 2 4 25.31 17.78 3.5195 -1 1 2 4 27.76 2.81 3.2138 2 1 1 4 27.96 100.00 3.1906 3 0 0 2 28.31 91.42 3.1528 1 1 2 4 28.73 99.11 3.1078 -2 1 2 4 29.57 3.63 3.0210 0 0 3 2 29.93 15.09 2.9850 2 0 2 2 30.60 1.18 2.9220 -3 0 2 2 31.43 1.72 2.8464 -2 0 3 2 31.53 29.74 2.8375 0 2 0 2 32.19 1.81 2.7812 3 1 0 4 32.92 33.78 2.7205 1 2 0 4 32.96 4.20 2.7177 1 0 3 2 33.11 11.25 2.7053 -1 1 3 4 33.61 5.19 2.6667 0 1 3 4 33.82 1.01 2.6507 -1 2 1 4 33.93 4.62 2.6419 2 1 2 4 34.53 17.00 2.5978 -3 1 2 4 35.01 4.39 2.5628 1 2 1 4 36.66 2.07 2.4512 1 1 3 4 36.82 15.72 2.4408 2 2 0 4 37.39 33.64 2.4049 0 2 2 4 37.50 3.59 2.3981 -1 2 2 4 37.82 1.08 2.3787 3 0 2 2 38.58 21.45 2.3338 -4 0 2 2 38.82 12.68 2.3197 -1 0 4 2 39.27 2.42 2.2943 2 2 1 4 39.67 11.73 2.2718 1 2 2 4 39.72 3.20 2.2695 -3 1 3 4 39.78 6.22 2.2657 0 0 4 2 40.20 7.37 2.2433 -2 0 4 2 40.93 13.23 2.2049 4 1 0 4 41.03 1.30 2.1996 4 0 1 2 41.15 9.61 2.1938 3 1 2 4 41.80 10.20 2.1612 2 1 3 4 41.85 3.58 2.1584 -4 1 2 4 42.08 2.29 2.1472 -1 1 4 4 42.64 17.84 2.1203 3 2 0 4 42.96 6.88 2.1055 1 0 4 2 42.98 6.15 2.1042 0 1 4 4 43.37 3.11 2.0862 -2 1 4 4 43.73 5.05 2.0698 -3 0 4 2 43.77 3.96 2.0682 0 2 3 4 44.03 2.61 2.0566 2 2 2 4 44.51 19.41 2.0356 -3 2 2 4 45.12 1.56 2.0096 -2 2 3 4 45.58 2.27 1.9900 3 0 3 2 45.88 3.24 1.9778 -4 1 3 4 46.26 1.37 1.9627 1 2 3 4 46.71 4.51 1.9445 -3 1 4 4 47.40 2.27 1.9178 -5 0 2 2 47.49 1.39 1.9144 5 0 0 2 47.98 2.62 1.8959 2 0 4 2 48.48 2.91 1.8779 3 1 3 4 49.05 3.14 1.8571 -4 0 4 2 49.09 6.10 1.8558 1 3 0 4 49.43 13.09 1.8439 4 1 2 4 49.81 1.55 1.8308 -2 0 5 2 49.85 12.07 1.8293 4 2 0 4 50.04 8.72 1.8229 3 2 2 4 50.21 17.87 1.8169 -5 1 2 4 50.30 2.49 1.8139 5 1 0 4 50.34 4.83 1.8126 0 0 5 2 50.64 1.04 1.8025 -4 2 2 4 50.77 1.66 1.7982 2 1 4 4 50.83 1.68 1.7964 5 0 1 2 50.84 23.07 1.7959 -1 2 4 4 51.84 3.13 1.7637 -1 1 5 4 51.96 1.05 1.7598 -2 2 4 4 51.98 2.29 1.7592 2 3 0 4 52.41 2.89 1.7458 -3 0 5 2 52.41 5.24 1.7457 0 3 2 4 52.50 1.38 1.7431 -1 3 2 4 52.52 3.27 1.7424 -2 1 5 4 52.65 3.89 1.7384 4 2 1 4 53.50 2.76 1.7126 5 1 1 4 53.75 1.88 1.7054 4 0 3 2 54.19 10.22 1.6927 1 3 2 4 54.43 12.53 1.6856 -2 3 2 4 55.79 3.33 1.6478 -5 0 4 2 56.03 4.82 1.6414 1 1 5 4 56.03 3.12 1.6412 5 0 2 2 56.48 4.10 1.6293 3 2 3 4 56.91 1.07 1.6179 -6 0 2 2 57.05 2.11 1.6144 3 1 4 4 57.16 2.09 1.6116 -1 3 3 4 57.34 5.87 1.6069 4 2 2 4 57.48 1.29 1.6033 0 3 3 4 57.80 5.60 1.5953 6 0 0 2 58.09 3.78 1.5879 -3 3 2 4 58.13 6.90 1.5870 5 2 0 4 58.31 2.58 1.5824 -5 1 4 4 58.55 7.54 1.5764 2 2 4 4 59.21 1.10 1.5604 -4 1 5 4 59.40 1.71 1.5559 -6 1 2 4 59.49 15.21 1.5539 -4 2 4 4 60.15 1.57 1.5384 -2 2 5 4 60.26 1.28 1.5358 6 1 0 4 60.62 3.19 1.5275 0 2 5 4 60.64 1.79 1.5272 2 1 5 4 61.38 1.65 1.5105 0 0 6 2 62.20 2.39 1.4925 4 0 4 2 62.32 1.82 1.4900 -1 1 6 4 62.46 3.09 1.4869 -3 2 5 4 62.60 3.24 1.4840 4 3 0 4 62.76 1.74 1.4806 3 3 2 4 63.24 2.60 1.4704 2 3 3 4 63.38 1.82 1.4675 1 2 5 4 63.70 1.40 1.4610 -6 0 4 2 63.76 2.35 1.4597 0 1 6 4 64.13 1.68 1.4521 0 3 4 4 64.35 2.17 1.4477 3 0 5 2 64.43 4.05 1.4462 -3 1 6 4 65.17 2.16 1.4315 5 1 3 4 65.83 8.08 1.4188 0 4 0 2 66.03 1.77 1.4148 -6 1 4 4 66.53 4.09 1.4055 -6 2 2 4 67.10 1.73 1.3949 -7 0 2 2 67.34 2.90 1.3906 6 2 0 4 67.90 1.73 1.3805 -4 1 6 4 68.45 1.09 1.3706 6 1 2 4 69.20 3.70 1.3576 4 3 2 4 69.49 3.10 1.3527 -1 4 2 4 69.49 1.22 1.3527 -2 2 6 4 69.84 5.82 1.3468 -5 3 2 4 70.89 1.85 1.3293 7 1 0 4 71.38 1.34 1.3214 -1 0 7 2 71.75 1.05 1.3156 -2 3 5 4 72.98 7.77 1.2964 3 4 0 4 73.43 1.58 1.2896 3 2 5 4 73.45 2.84 1.2891 -2 1 7 4 73.97 2.00 1.2814 2 4 2 4 74.00 3.35 1.2810 4 1 5 4 74.72 1.60 1.2704 1 3 5 4 77.49 1.64 1.2318 7 2 0 4 78.42 1.27 1.2194 -6 2 5 4 78.48 2.31 1.2187 1 1 7 4 78.97 2.69 1.2123 -4 4 2 4 79.13 1.65 1.2103 -1 4 4 4 79.18 2.39 1.2096 -6 1 6 4 79.23 1.31 1.2090 7 1 2 4 79.39 1.11 1.2071 -5 2 6 4 79.72 1.60 1.2028 5 2 4 4 80.02 1.73 1.1991 -2 4 4 4 80.12 1.50 1.1979 -1 2 7 4 80.25 2.75 1.1962 -8 1 2 4 80.74 1.03 1.1902 7 2 1 4 81.00 1.39 1.1870 2 0 7 2 81.35 4.67 1.1828 -7 2 4 4 81.44 1.90 1.1817 6 2 3 4 81.87 1.50 1.1766 1 4 4 4 82.16 1.69 1.1732 -3 3 6 4 82.16 1.78 1.1731 -5 1 7 4 82.70 1.16 1.1669 -8 0 4 2 85.64 1.23 1.1343 7 2 2 4 87.27 1.33 1.1172 0 4 5 4 88.74 1.49 1.1025 8 2 0 4 89.50 1.38 1.0950 2 2 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.