Kraisslite Cooper M A, Hawthorne F C Mineralogical Magazine 76 (2012) 2819-2836 Crystal structure of kraisslite, Zn3(Mn,Mg)25(Fe3+,Al)(As3+O3)2[(Si,As5+)O4]10(OH)16, from the Sterling Hill mine, Ogdensburg, Sussex County, New Jersey, USA Locality: the Sterling Hill mine, Ogdensburg, Sussex County, New Jersey, USA _database_code_amcsd 0019752 CELL PARAMETERS: 8.1821 14.1946 43.9103 90.000 90.000 90.000 SPACE GROUP: C222_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 5099.814 Density (g/cm3): 4.089 MAX. ABS. INTENSITY / VOLUME**2: 11.64768311 RIR: 0.928 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.05 4.99 10.9776 0 0 4 2 12.09 1.72 7.3184 0 0 6 2 12.63 2.10 7.0064 0 2 1 4 12.65 1.07 6.9981 1 1 1 4 13.12 1.09 6.7458 1 1 2 4 13.88 2.00 6.3799 1 1 3 4 16.07 1.81 5.5160 1 1 5 4 18.88 2.38 4.7002 0 2 7 4 18.89 3.69 4.6977 1 1 7 4 20.22 9.57 4.3910 0 0 10 2 20.45 6.54 4.3419 0 2 8 4 20.46 6.34 4.3399 1 1 8 4 21.70 20.86 4.0960 1 3 0 4 21.72 3.70 4.0911 2 0 0 2 21.79 2.30 4.0783 1 3 1 4 21.82 5.58 4.0734 2 0 1 4 22.08 3.43 4.0265 1 3 2 4 22.12 1.94 4.0190 1 1 9 4 22.54 8.46 3.9444 1 3 3 4 22.57 5.53 3.9400 2 0 3 4 23.18 5.99 3.8375 1 3 4 4 23.20 5.55 3.8335 2 0 4 4 23.84 3.60 3.7329 1 1 10 4 23.97 1.33 3.7121 1 3 5 4 24.00 3.67 3.7084 2 0 5 4 24.32 6.03 3.6592 0 0 12 2 24.91 3.03 3.5742 1 3 6 4 24.93 2.49 3.5710 2 0 6 4 25.43 1.88 3.5032 0 4 2 4 25.60 6.94 3.4793 0 2 11 4 25.61 8.20 3.4783 1 1 11 4 25.86 1.55 3.4448 2 2 3 4 25.98 5.19 3.4296 1 3 7 4 26.00 5.93 3.4267 2 0 7 4 26.40 1.46 3.3766 0 4 4 4 27.13 2.69 3.2868 2 2 5 4 27.16 17.28 3.2827 1 3 8 4 27.19 22.48 3.2802 2 0 8 4 27.43 5.92 3.2515 1 1 12 4 27.94 3.47 3.1931 0 4 6 4 28.45 29.08 3.1370 1 3 9 4 28.46 3.07 3.1365 0 0 14 2 28.47 6.17 3.1348 2 0 9 4 28.91 2.63 3.0887 0 4 7 4 28.93 8.91 3.0858 2 2 7 4 29.83 85.25 2.9952 1 3 10 4 29.85 40.40 2.9932 2 0 10 4 29.98 7.70 2.9801 0 4 8 4 30.01 8.94 2.9775 2 2 8 4 31.19 100.00 2.8676 2 2 9 4 31.29 4.80 2.8588 1 3 11 4 32.44 34.59 2.7600 0 4 10 4 32.63 9.44 2.7444 0 0 16 2 32.82 10.38 2.7288 1 3 12 4 33.11 1.40 2.7057 1 1 15 4 33.41 2.13 2.6821 1 5 0 4 33.43 18.53 2.6807 2 4 0 4 33.46 1.95 2.6784 3 1 0 4 33.47 18.99 2.6771 1 5 1 4 33.49 2.17 2.6757 2 4 1 4 33.52 21.47 2.6734 3 1 1 4 33.66 1.40 2.6623 1 5 2 4 33.68 2.93 2.6609 2 4 2 4 33.71 1.15 2.6587 3 1 2 4 33.82 6.21 2.6504 2 2 11 4 33.98 5.50 2.6381 1 5 3 4 34.00 4.09 2.6368 2 4 3 4 34.03 2.59 2.6346 3 1 3 4 34.41 1.76 2.6059 1 3 13 4 34.42 1.50 2.6054 1 5 4 4 34.43 1.53 2.6047 2 0 13 4 34.98 3.99 2.5651 1 5 5 4 35.00 1.01 2.5639 2 4 5 4 35.03 1.89 2.5619 3 1 5 4 35.06 1.97 2.5593 1 1 16 4 35.25 1.18 2.5459 2 2 12 4 35.67 1.02 2.5171 2 4 6 4 36.07 3.48 2.4902 1 3 14 4 36.43 7.36 2.4661 1 5 7 4 36.45 5.13 2.4650 2 4 7 4 36.48 4.71 2.4632 3 1 7 4 36.84 7.98 2.4395 0 0 18 2 37.04 3.88 2.4272 0 2 17 4 37.04 3.83 2.4269 1 1 17 4 37.32 12.12 2.4098 1 5 8 4 37.36 13.62 2.4071 3 1 8 4 38.04 11.56 2.3658 0 6 0 2 38.08 13.20 2.3629 3 3 0 4 38.14 8.02 2.3595 3 3 1 4 38.30 35.69 2.3503 1 5 9 4 38.31 34.04 2.3494 2 4 9 4 38.34 27.09 2.3479 3 1 9 4 38.94 1.29 2.3127 0 6 4 4 38.99 1.75 2.3100 3 3 4 4 39.05 1.28 2.3067 1 1 18 4 39.37 3.74 2.2889 1 5 10 4 39.38 7.15 2.2880 2 4 10 4 39.41 3.14 2.2866 3 1 10 4 39.49 1.98 2.2818 3 3 5 4 39.53 2.62 2.2799 1 3 16 4 39.94 1.50 2.2571 2 2 15 4 40.52 3.91 2.2262 1 5 11 4 40.54 3.66 2.2254 2 4 11 4 40.56 2.63 2.2241 3 1 11 4 40.76 1.65 2.2136 0 6 7 4 40.81 1.62 2.2112 3 3 7 4 41.11 7.63 2.1955 0 0 20 2 41.32 6.54 2.1848 1 3 17 4 41.34 4.83 2.1841 2 0 17 4 41.61 1.44 2.1703 3 3 8 4 41.76 3.77 2.1632 1 5 12 4 41.79 2.89 2.1613 3 1 12 4 42.51 4.27 2.1266 3 3 9 4 43.45 3.57 2.0827 0 6 10 4 43.49 4.96 2.0808 3 3 10 4 44.52 1.22 2.0352 0 6 11 4 45.71 1.16 1.9850 3 3 12 4 45.89 2.94 1.9775 1 5 15 4 45.92 3.23 1.9761 3 1 15 4 46.02 1.12 1.9722 2 6 6 4 46.17 1.22 1.9663 1 7 1 4 46.23 2.01 1.9636 4 2 1 4 46.35 2.54 1.9589 3 5 2 4 46.38 1.01 1.9577 4 2 2 4 46.65 1.61 1.9469 2 6 7 4 46.71 1.40 1.9447 4 0 7 4 47.41 3.01 1.9177 2 4 16 4 48.19 1.10 1.8884 2 6 9 4 48.22 1.27 1.8873 3 3 14 4 48.24 1.26 1.8864 4 0 9 4 48.96 6.52 1.8605 1 5 17 4 48.97 4.01 1.8600 2 4 17 4 48.99 7.85 1.8592 3 1 17 4 49.08 1.40 1.8560 2 6 10 4 49.18 2.05 1.8527 1 7 8 4 49.21 1.07 1.8515 3 5 8 4 49.24 2.92 1.8505 4 2 8 4 49.97 1.14 1.8253 1 7 9 4 50.00 1.53 1.8242 3 5 9 4 50.03 1.78 1.8231 4 2 9 4 50.58 4.56 1.8046 1 5 18 4 50.59 26.08 1.8042 2 4 18 4 50.61 4.56 1.8035 3 1 18 4 50.67 1.23 1.8015 0 4 21 4 50.69 1.19 1.8009 2 2 21 4 50.84 1.34 1.7961 1 7 10 4 50.87 1.60 1.7950 3 5 10 4 51.16 1.30 1.7855 4 0 12 4 51.55 1.26 1.7729 0 8 1 4 51.57 3.33 1.7722 4 4 0 4 51.62 2.38 1.7707 4 4 1 4 51.82 2.57 1.7643 3 5 11 4 51.85 1.62 1.7634 4 2 11 4 51.98 1.10 1.7593 4 4 3 4 52.25 21.78 1.7508 1 5 19 4 52.26 4.30 1.7504 2 4 19 4 52.28 19.41 1.7497 3 1 19 4 52.63 1.27 1.7391 2 2 22 4 52.81 2.07 1.7334 1 7 12 4 53.68 1.18 1.7073 0 8 7 4 53.75 2.75 1.7054 4 4 7 4 53.98 5.03 1.6985 2 4 20 4 53.99 3.86 1.6983 0 6 18 4 54.03 4.85 1.6973 3 3 18 4 54.34 1.26 1.6883 0 8 8 4 54.40 1.63 1.6865 4 4 8 4 55.63 6.51 1.6522 3 3 19 4 55.74 6.75 1.6490 1 5 21 4 55.76 2.22 1.6487 2 4 21 4 55.78 7.39 1.6482 3 1 21 4 55.89 1.99 1.6451 0 8 10 4 55.95 5.78 1.6434 4 4 10 4 56.54 2.97 1.6278 2 8 0 4 56.55 1.09 1.6273 3 7 0 4 56.58 1.26 1.6267 2 8 1 4 56.60 1.84 1.6262 3 7 1 4 56.61 1.08 1.6258 2 2 24 4 56.62 1.06 1.6257 5 1 0 4 56.66 1.53 1.6245 5 1 1 4 56.78 1.40 1.6214 0 8 11 4 56.84 2.77 1.6197 4 4 11 4 57.00 1.10 1.6157 5 1 3 4 57.25 2.23 1.6093 0 6 20 4 57.28 2.09 1.6084 3 3 20 4 57.42 1.37 1.6048 2 6 17 4 57.57 1.55 1.6009 2 4 22 4 58.20 2.40 1.5851 1 1 27 4 58.59 2.50 1.5756 2 8 7 4 58.61 1.54 1.5752 3 7 7 4 58.66 1.34 1.5738 2 2 25 4 58.67 1.74 1.5737 5 1 7 4 59.06 1.36 1.5642 4 2 17 4 59.20 1.33 1.5606 2 8 8 4 59.71 10.26 1.5487 1 9 0 4 59.75 7.34 1.5477 1 9 1 4 59.77 18.25 1.5473 4 6 0 4 59.80 6.16 1.5465 5 3 0 4 59.84 10.75 1.5456 5 3 1 4 59.87 1.33 1.5448 1 9 2 4 59.90 9.99 1.5441 2 8 9 4 59.92 9.91 1.5437 3 7 9 4 59.93 5.66 1.5435 4 6 2 4 59.96 3.07 1.5427 5 3 2 4 59.98 11.85 1.5423 5 1 9 4 60.08 2.94 1.5401 1 9 3 4 60.17 1.79 1.5380 5 3 3 4 60.46 1.13 1.5313 0 2 28 4 60.46 1.16 1.5312 1 1 28 4 60.67 1.20 1.5263 2 8 10 4 60.75 1.89 1.5246 2 2 26 4 60.82 1.06 1.5231 5 3 5 4 61.33 4.61 1.5115 1 3 27 4 61.52 1.62 1.5073 2 8 11 4 61.60 1.42 1.5056 5 1 11 4 61.69 1.95 1.5035 1 9 7 4 62.87 1.72 1.4781 2 2 27 4 62.97 2.19 1.4761 1 9 9 4 63.29 2.24 1.4694 1 5 25 4 63.30 3.29 1.4691 2 4 25 4 63.32 2.51 1.4688 3 1 25 4 63.52 5.24 1.4646 1 3 28 4 63.53 3.81 1.4643 2 0 28 4 63.62 1.16 1.4625 0 8 17 4 63.68 3.10 1.4613 4 4 17 4 63.77 1.33 1.4594 4 6 10 4 65.02 2.18 1.4344 0 4 28 4 65.05 1.56 1.4338 4 4 18 4 65.07 1.08 1.4334 1 1 30 4 65.29 2.42 1.4291 1 5 26 4 65.30 3.41 1.4289 2 4 26 4 65.32 1.85 1.4286 3 1 26 4 65.49 1.92 1.4252 4 6 12 4 65.53 1.24 1.4245 5 3 12 4 67.24 3.05 1.3924 2 2 29 4 67.33 1.45 1.3906 1 5 27 4 67.36 1.65 1.3901 3 1 27 4 68.75 1.16 1.3653 3 9 0 4 69.41 1.13 1.3540 2 8 18 4 69.42 1.57 1.3538 1 5 28 4 69.45 1.58 1.3533 3 1 28 4 69.77 2.68 1.3479 4 6 16 4 69.80 1.35 1.3473 5 3 16 4 70.22 1.58 1.3403 4 8 0 4 70.32 1.07 1.3387 1 3 31 4 70.33 1.38 1.3385 2 10 2 4 70.44 1.46 1.3367 6 2 2 4 71.56 1.06 1.3185 1 5 29 4 71.57 2.11 1.3184 2 4 29 4 71.79 1.43 1.3148 3 9 9 4 72.26 1.30 1.3075 1 9 18 4 72.31 2.02 1.3067 4 6 18 4 72.50 4.94 1.3038 3 9 10 4 72.59 1.16 1.3023 6 0 10 4 73.30 1.89 1.2914 6 2 9 4 73.63 1.71 1.2865 1 9 19 4 73.71 3.13 1.2853 5 3 19 4 73.94 1.06 1.2819 4 8 10 4 74.00 1.32 1.2809 4 2 26 4 74.12 1.16 1.2792 3 9 12 4 74.47 1.09 1.2741 1 11 1 4 74.55 1.01 1.2729 5 7 1 4 75.92 1.05 1.2533 3 5 27 4 77.38 2.31 1.2333 1 11 9 4 77.46 1.58 1.2322 5 7 9 4 77.50 1.55 1.2317 6 4 9 4 78.18 1.46 1.2226 4 4 26 4 78.40 2.28 1.2197 0 0 36 2 82.00 1.04 1.1750 0 8 28 4 82.03 1.11 1.1747 4 8 18 4 82.06 2.12 1.1744 4 4 28 4 83.41 1.38 1.1587 6 2 19 4 83.70 1.80 1.1555 0 0 38 2 83.74 1.36 1.1550 6 6 8 4 84.16 2.16 1.1503 3 7 27 4 84.21 2.14 1.1497 5 1 27 4 84.69 1.06 1.1444 2 10 20 4 84.80 1.11 1.1433 6 2 20 4 86.19 1.12 1.1284 4 8 21 4 87.37 1.37 1.1162 1 11 19 4 88.11 1.55 1.1087 2 8 29 4 88.13 1.04 1.1085 3 7 29 4 88.18 1.18 1.1080 5 1 29 4 88.33 1.05 1.1065 4 4 31 4 88.98 1.15 1.1001 2 12 10 4 89.05 1.00 1.0994 5 9 10 4 89.13 1.31 1.0987 7 3 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.