Leguernite Garavelli A, Pinto D, Mitolo D, Bindi L Mineralogical Magazine 78 (2014) 1629-1645 Leguernite, Bi12.67O14(SO4)5, a new Bi oxysulfate from the fumarole deposit of La Fossa crater, Vulcano, Aeolian Islands, Italy Note: O17 y-coordinate changed to reproduce reported bond lengths Locality: La Fossa crater, Vulcano, Aeolian Islands, Italy _database_code_amcsd 0020607 CELL PARAMETERS: 11.2486 5.6568 11.9139 90.000 99.177 90.000 SPACE GROUP: P2 X-RAY WAVELENGTH: 1.541838 Cell Volume: 748.391 Density (g/cm3): 7.435 MAX. ABS. INTENSITY / VOLUME**2: 173.0515273 RIR: 7.579 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.52 34.20 11.7614 0 0 1 2 7.96 19.47 11.1046 1 0 0 2 10.05 5.04 8.8058 -1 0 1 2 15.07 6.45 5.8807 0 0 2 2 15.96 3.25 5.5523 2 0 0 2 16.53 4.12 5.3619 -2 0 1 2 17.40 6.39 5.0978 0 1 1 2 17.60 11.92 5.0405 1 1 0 2 19.66 1.89 4.5161 1 1 1 2 20.17 1.68 4.4029 -2 0 2 2 21.80 2.09 4.0768 0 1 2 2 22.44 4.22 3.9625 2 1 0 2 22.82 4.69 3.8971 -1 0 3 2 22.85 3.10 3.8915 -2 1 1 2 24.07 3.05 3.6971 1 1 2 2 24.51 1.17 3.6321 2 1 1 2 25.64 1.18 3.4745 -2 1 2 2 25.64 2.80 3.4743 -2 0 3 2 26.32 1.63 3.3855 -3 0 2 2 26.37 1.91 3.3798 3 0 1 2 27.68 100.00 3.2223 0 1 3 2 27.80 2.75 3.2092 -1 1 3 2 28.56 3.08 3.1254 2 1 2 2 28.81 90.78 3.0988 -3 1 1 2 28.82 22.81 3.0974 3 1 0 2 29.87 14.70 2.9914 1 1 3 2 30.45 5.40 2.9353 -3 0 3 2 30.52 27.48 2.9291 3 0 2 2 30.78 1.60 2.9050 -3 1 2 2 30.82 2.62 2.9014 3 1 1 2 31.63 31.22 2.8284 0 2 0 1 31.92 1.02 2.8037 -4 0 1 2 32.09 5.86 2.7889 -2 0 4 2 32.56 2.83 2.7500 0 2 1 2 32.67 2.33 2.7409 1 2 0 2 33.27 2.20 2.6929 -1 2 1 2 33.95 1.76 2.6407 2 1 3 2 34.37 5.07 2.6090 0 1 4 2 35.21 2.74 2.5489 0 2 2 2 35.62 2.29 2.5202 2 2 0 2 35.85 20.02 2.5051 -3 0 4 2 35.90 1.05 2.5017 -2 2 1 2 35.92 7.96 2.4998 3 0 3 2 37.80 1.49 2.3797 -2 2 2 2 37.98 2.42 2.3689 4 0 2 2 39.36 3.79 2.2891 -1 2 3 2 40.10 2.67 2.2487 -5 0 1 2 40.44 1.17 2.2302 1 0 5 2 40.91 1.88 2.2059 1 2 3 2 41.15 5.44 2.1934 -2 2 3 2 41.32 1.29 2.1850 4 1 2 2 41.58 2.03 2.1720 0 1 5 2 41.61 2.17 2.1706 -3 2 2 2 41.64 1.94 2.1691 3 2 1 2 42.40 1.86 2.1320 -2 1 5 2 43.30 1.72 2.0897 -5 1 1 2 43.62 1.16 2.0748 1 1 5 2 44.10 1.16 2.0534 2 2 3 2 44.14 1.15 2.0516 2 0 5 2 44.14 2.54 2.0516 -4 1 4 2 44.48 4.03 2.0367 -3 2 3 2 44.53 21.59 2.0347 3 2 2 2 45.27 1.43 2.0032 3 1 4 2 45.56 2.06 1.9912 -4 2 1 2 45.69 3.54 1.9859 -2 2 4 2 45.70 1.04 1.9854 -1 0 6 2 46.32 8.19 1.9602 0 0 6 2 47.12 1.49 1.9287 2 1 5 2 48.42 4.95 1.8797 1 0 6 2 48.55 15.39 1.8753 -3 2 4 2 48.56 6.98 1.8748 -6 0 1 2 48.60 1.50 1.8733 -1 1 6 2 48.61 5.45 1.8731 3 2 3 2 48.92 1.31 1.8618 0 3 1 2 49.00 2.21 1.8590 1 3 0 2 49.20 6.09 1.8520 -6 0 2 2 49.47 2.98 1.8423 -2 1 6 2 50.03 4.38 1.8233 -5 1 4 2 50.24 1.76 1.8161 4 2 2 2 50.85 1.14 1.7956 0 3 2 2 51.16 1.62 1.7854 2 3 0 2 51.85 7.21 1.7634 3 1 5 2 51.98 1.45 1.7591 1 3 2 2 51.99 1.37 1.7590 6 1 0 2 52.69 1.12 1.7372 -4 2 4 2 53.68 1.12 1.7076 3 2 4 2 53.85 5.67 1.7023 6 1 1 2 53.96 8.26 1.6993 0 3 3 2 54.03 1.47 1.6974 -1 3 3 2 54.20 1.07 1.6924 4 2 3 2 54.58 1.65 1.6815 -5 1 5 2 54.62 8.24 1.6804 -3 3 1 2 54.62 1.84 1.6802 3 3 0 2 55.25 1.25 1.6626 1 3 3 2 55.81 1.42 1.6473 -3 3 2 2 55.83 1.54 1.6467 3 3 1 2 56.64 1.32 1.6250 -1 2 6 2 56.77 5.02 1.6217 -6 1 4 2 56.84 1.45 1.6199 5 2 2 2 56.86 8.22 1.6192 6 1 2 2 57.05 5.52 1.6143 -2 1 7 2 57.17 5.06 1.6111 0 2 6 2 57.61 3.65 1.6001 4 1 5 2 57.83 1.12 1.5943 2 3 3 2 58.93 6.68 1.5672 -3 1 7 2 59.00 3.59 1.5655 1 2 6 2 59.04 3.32 1.5647 3 1 6 2 59.12 5.02 1.5627 -6 2 1 2 59.68 4.48 1.5494 -6 2 2 2 60.78 5.29 1.5238 -6 1 5 2 61.36 1.41 1.5109 -6 2 3 2 63.92 1.74 1.4564 -5 0 7 2 64.56 1.89 1.4436 4 1 6 2 65.14 1.14 1.4321 -4 3 4 2 65.45 1.08 1.4261 7 1 2 2 66.01 1.01 1.4153 3 3 4 2 66.07 2.03 1.4142 0 4 0 1 67.46 1.06 1.3883 2 3 5 2 69.45 1.74 1.3534 6 0 5 2 71.30 1.47 1.3227 3 3 5 2 71.42 1.08 1.3208 6 3 0 2 72.45 1.13 1.3046 3 4 1 2 72.98 1.15 1.2963 6 3 1 2 73.08 1.39 1.2948 -5 2 7 2 74.51 1.09 1.2735 3 4 2 2 74.52 1.22 1.2733 0 1 9 2 75.47 1.15 1.2596 -6 3 4 2 75.55 1.78 1.2585 6 3 2 2 75.72 1.13 1.2562 -2 3 7 2 76.64 3.00 1.2433 1 1 9 2 77.36 1.52 1.2336 -3 3 7 2 77.51 1.28 1.2315 -3 4 4 2 78.32 1.64 1.2208 6 2 5 2 78.47 3.54 1.2189 -9 1 2 2 78.99 1.35 1.2121 -6 3 5 2 79.37 1.71 1.2073 9 0 1 2 80.78 1.46 1.1897 -2 0 10 2 82.19 1.15 1.1728 -8 2 5 2 82.24 1.33 1.1723 -9 0 5 2 84.62 1.12 1.1453 -6 2 8 2 86.88 1.19 1.1211 4 2 8 2 87.94 2.14 1.1104 9 2 1 2 89.33 1.84 1.0967 -2 2 10 2 89.56 1.36 1.0945 -5 1 10 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.