data_global _chemical_name_mineral 'Jordanite' loop_ _publ_author_name 'Biagioni C' 'Dini A' 'Orlandi P' 'Moelo Y' 'Pasero M' 'Zaccarini F' _journal_name_full 'Minerals' _journal_volume 6 _journal_year 2016 _journal_page_first _journal_page_last doi:10.3390 _publ_section_title ; Lead-antimony sulfosalts from Tuscany (Italy). XX. Members of the jordanite-geocronite series from the Pollone mine, Valdicastello Carducci: Occurrence and crystal structures Note: Sb-rich jordanite ; _database_code_amcsd 0020594 _chemical_compound_source 'Pollone mine, Valdicastello Carducci, Pietrasanta, Tuscany, Italy' _chemical_formula_sum 'Pb4.667 Sb.933 As1.067 S7.667' _cell_length_a 8.9554 _cell_length_b 31.9228 _cell_length_c 8.4937 _cell_angle_alpha 90 _cell_angle_beta 117.981 _cell_angle_gamma 90 _cell_volume 2144.344 _exptl_crystal_density_diffrn 6.534 _symmetry_space_group_name_H-M 'P 1 21/m 1' loop_ _space_group_symop_operation_xyz 'x,y,z' 'x,1/2-y,z' '-x,1/2+y,-z' '-x,-y,-z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_U_iso_or_equiv Pb1 0.44554 0.05466 0.35035 1.00000 0.01831 Pb2 0.43630 0.05516 0.83760 0.50000 0.01620 Sb2 0.44290 0.04539 0.84880 0.50000 0.01620 Pb3 0.90383 0.04265 0.32253 1.00000 0.01895 Sb4 0.92046 0.04881 0.83364 0.83900 0.01330 As4 0.92046 0.04881 0.83364 0.16100 0.01330 Pb5 0.26238 0.14343 0.00029 1.00000 0.02525 As6 0.27310 0.14349 0.50870 0.94000 0.01560 Sb6 0.27310 0.14349 0.50870 0.06000 0.01560 Pb7 0.78992 0.15103 0.01984 1.00000 0.01812 Pb8 0.79132 0.15072 0.51607 1.00000 0.01749 Pb9 0.12014 0.25000 0.17379 1.00000 0.02140 Pb10 0.12050 0.25000 0.69057 1.00000 0.02120 As11 0.61430 0.22587 0.17880 0.50000 0.01360 Pb12 0.55032 0.25000 0.64347 1.00000 0.03260 S1 0.30680 0.00310 0.01370 1.00000 0.01610 S2 0.30660 0.00470 0.54650 1.00000 0.01660 S3 0.05130 0.08729 0.11580 1.00000 0.01390 S4 0.05500 0.08654 0.68170 1.00000 0.01460 S5 0.65060 0.09790 0.20310 1.00000 0.01570 S6 0.66510 0.09175 0.70400 1.00000 0.01340 S7 0.40370 0.17803 0.37500 1.00000 0.02040 S8 0.40050 0.17848 0.76990 1.00000 0.01900 S9 0.02750 0.18020 0.38480 1.00000 0.01400 S10 0.99040 0.19309 0.86950 1.00000 0.01500 S11 0.37380 0.26170 0.05910 0.50000 0.01130 S12 0.75020 0.25000 0.03530 1.00000 0.02000 S13 0.74870 0.25000 0.45590 1.00000 0.02220 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pb1 0.01700 0.01940 0.01880 0.00160 0.00860 0.00080 Pb2 0.01470 0.01830 0.01760 -0.00030 0.00940 -0.00120 Sb2 0.01470 0.01830 0.01760 -0.00030 0.00940 -0.00120 Pb3 0.01460 0.02150 0.02010 0.00220 0.00760 0.00050 Sb4 0.01200 0.01420 0.01580 -0.00070 0.00820 -0.00100 As4 0.01200 0.01420 0.01580 -0.00070 0.00820 -0.00100 Pb5 0.02040 0.03520 0.02160 0.00850 0.01100 0.00540 As6 0.01350 0.01630 0.01840 0.00220 0.00860 0.00090 Sb6 0.01350 0.01630 0.01840 0.00220 0.00860 0.00090 Pb7 0.01880 0.01960 0.01880 0.00030 0.01120 -0.00020 Pb8 0.01830 0.01830 0.01740 -0.00100 0.00970 -0.00070 Pb9 0.02120 0.02480 0.01870 0.00000 0.00980 0.00000 Pb10 0.02160 0.02350 0.02370 0.00000 0.01490 0.00000 As11 0.01030 0.00880 0.01990 -0.00030 0.00560 -0.00100 Pb12 0.03410 0.02190 0.04140 0.00000 0.01750 0.00000 S1 0.01070 0.01890 0.01920 0.00100 0.00750 -0.00320 S2 0.01370 0.01690 0.02150 0.00190 0.01010 0.00180 S3 0.01250 0.01620 0.01440 -0.00040 0.00750 0.00010 S4 0.01220 0.01730 0.01600 0.00150 0.00810 -0.00080 S5 0.01600 0.01570 0.01760 -0.00140 0.00970 -0.00060 S6 0.01140 0.01380 0.01600 0.00010 0.00720 -0.00070 S7 0.01360 0.02600 0.02300 -0.00050 0.01070 -0.00140 S8 0.01260 0.02500 0.01870 0.00020 0.00680 -0.00220 S9 0.00720 0.01970 0.01700 -0.00010 0.00720 -0.00050 S10 0.01710 0.01340 0.01750 -0.00420 0.01070 -0.00220 S11 0.01000 0.01900 0.01000 0.00700 0.01000 0.00400 S12 0.00800 0.03000 0.02200 0.00000 0.00700 0.00000 S13 0.00700 0.03200 0.02400 0.00000 0.00400 0.00000