Magnanelliite Biagioni C, Bindi L, Kampf A R Minerals 9 (2019) 779 Crystal-chemistry of sulfates from the Apuan Alps (Tuscany, Italy). VII. Magnanelliite, K3Fe3+2(SO4)4 (OH)(H2O)2, a new sulfate from the Monte Arsiccio mine Locality: Monte Arsiccio mine, Apuan Alps, Italy _database_code_amcsd 0020909 CELL PARAMETERS: 7.5491 16.8652 12.1574 90.000 94.064 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1543.953 Density (g/cm3): 2.847 MAX. ABS. INTENSITY / VOLUME**2: 8.073058908 RIR: 0.923 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.49 4.93 8.4326 0 2 0 2 12.79 69.54 6.9233 0 2 1 4 12.87 15.66 6.8759 1 1 0 4 14.39 11.75 6.1547 -1 1 1 4 14.61 2.48 6.0634 0 0 2 2 15.22 4.88 5.8219 1 1 1 4 18.02 39.61 4.9229 0 2 2 4 18.88 33.66 4.7012 -1 1 2 4 20.14 2.17 4.4084 1 1 2 4 21.33 4.67 4.1656 1 3 1 4 24.11 12.08 3.6917 -1 3 2 4 24.42 18.46 3.6451 0 2 3 4 24.82 30.78 3.5876 -1 1 3 4 25.12 3.90 3.5448 1 3 2 4 25.74 3.33 3.4616 0 4 2 4 25.92 20.70 3.4379 2 2 0 4 26.29 2.40 3.3902 1 1 3 4 26.49 9.15 3.3652 -2 2 1 4 26.98 27.59 3.3053 -2 0 2 2 27.42 6.00 3.2528 2 2 1 4 28.78 100.00 3.1016 2 0 2 2 29.01 41.83 3.0783 1 5 0 4 29.05 41.07 3.0741 -1 3 3 4 29.46 26.00 3.0317 0 0 4 2 29.74 60.64 3.0045 -1 5 1 4 30.16 5.43 2.9633 1 5 1 4 31.47 17.73 2.8428 -1 1 4 4 31.84 1.42 2.8109 0 6 0 2 31.87 2.17 2.8083 2 4 0 4 32.23 3.78 2.7775 -1 5 2 4 32.34 6.31 2.7683 -2 4 1 4 32.70 5.59 2.7383 0 6 1 4 33.01 27.92 2.7133 1 5 2 4 33.05 3.99 2.7100 1 1 4 4 33.10 15.78 2.7067 -2 2 3 4 33.12 1.57 2.7047 2 4 1 4 34.48 35.19 2.6013 -2 4 2 4 34.97 4.68 2.5661 -1 3 4 4 35.19 3.00 2.5502 0 6 2 4 35.35 3.53 2.5390 2 2 3 4 35.95 2.22 2.4984 2 4 2 4 36.18 2.66 2.4827 3 1 0 4 36.42 1.18 2.4672 1 3 4 4 36.43 4.70 2.4665 -3 1 1 4 37.22 36.83 2.4155 1 5 3 4 38.20 1.29 2.3562 -3 1 2 4 38.29 5.11 2.3506 -2 2 4 4 38.55 1.01 2.3351 -1 1 5 4 38.63 5.09 2.3309 0 2 5 4 39.31 2.09 2.2920 3 3 0 4 40.03 6.45 2.2524 2 6 0 4 40.20 3.70 2.2431 3 1 2 4 40.22 7.26 2.2422 1 1 5 4 40.42 5.84 2.2316 -2 6 1 4 40.53 1.37 2.2260 3 3 1 4 40.94 5.26 2.2042 2 2 4 4 42.20 1.69 2.1413 -2 6 2 4 42.45 1.48 2.1294 1 5 4 4 42.90 5.44 2.1082 0 8 0 2 43.09 1.77 2.0994 3 3 2 4 43.10 6.63 2.0987 1 3 5 4 43.58 3.36 2.0770 0 8 1 4 44.13 2.02 2.0524 3 1 3 4 45.00 11.64 2.0144 -1 7 3 4 45.02 1.42 2.0137 3 5 0 4 45.25 1.29 2.0040 -2 6 3 4 45.57 1.75 1.9904 -3 1 4 4 46.11 10.37 1.9685 3 5 1 4 46.81 6.31 1.9406 3 3 3 4 47.02 19.91 1.9325 -1 5 5 4 47.24 3.26 1.9240 2 2 5 4 47.72 2.66 1.9060 1 1 6 4 48.35 4.12 1.8825 4 0 0 2 48.44 5.06 1.8793 3 5 2 4 48.71 1.05 1.8692 0 8 3 4 49.03 2.25 1.8580 3 1 4 4 49.37 2.25 1.8459 -2 6 4 4 49.40 10.23 1.8448 -3 5 3 4 49.66 11.83 1.8358 -2 0 6 2 49.67 2.51 1.8355 -4 2 1 4 50.17 2.58 1.8184 1 9 0 4 50.44 1.46 1.8094 2 8 1 4 50.77 1.39 1.7982 4 2 1 4 51.41 1.37 1.7774 -2 8 2 4 51.52 2.46 1.7739 3 3 4 4 52.27 1.32 1.7501 -1 9 2 4 52.48 3.26 1.7435 2 8 2 4 52.81 1.42 1.7337 1 9 2 4 52.90 3.68 1.7308 0 8 4 4 53.15 4.30 1.7231 -3 5 4 4 53.18 3.04 1.7224 -3 3 5 4 53.29 17.36 1.7190 4 4 0 4 53.34 1.53 1.7175 -4 4 1 4 53.51 4.96 1.7124 -1 5 6 4 54.39 1.58 1.6869 4 4 1 4 54.40 1.99 1.6865 -2 6 5 4 54.52 2.03 1.6832 -2 4 6 4 55.61 2.81 1.6526 -4 0 4 2 55.74 1.23 1.6492 1 7 5 4 55.79 1.84 1.6479 1 9 3 4 56.04 3.90 1.6410 0 6 6 4 56.26 5.04 1.6351 3 5 4 4 57.58 2.98 1.6008 2 4 6 4 57.96 1.82 1.5911 0 8 5 4 58.85 4.78 1.5691 3 7 3 4 58.94 1.39 1.5671 -3 3 6 4 59.11 1.28 1.5630 -4 6 1 4 59.38 2.29 1.5565 0 10 3 4 59.62 4.94 1.5508 4 0 4 2 60.09 2.34 1.5398 4 6 1 4 60.12 1.28 1.5392 2 10 0 4 60.41 2.61 1.5325 -2 10 1 4 61.14 11.58 1.5159 0 0 8 2 61.47 1.30 1.5084 2 2 7 4 61.50 4.30 1.5077 3 5 5 4 61.75 3.29 1.5023 -2 10 2 4 62.25 5.61 1.4914 1 5 7 4 62.39 1.81 1.4884 1 11 1 4 62.66 2.96 1.4826 3 9 1 4 62.97 1.25 1.4761 5 1 1 4 63.03 1.28 1.4748 0 6 7 4 63.08 2.54 1.4738 0 10 4 4 63.31 4.65 1.4689 -3 5 6 4 64.00 1.28 1.4547 5 3 0 4 64.11 5.74 1.4525 -2 10 3 4 64.39 3.35 1.4468 -3 7 5 4 65.10 1.48 1.4328 5 3 1 4 65.10 1.70 1.4328 5 1 2 4 65.37 3.56 1.4275 -3 9 3 4 66.03 1.92 1.4148 -1 11 3 4 67.44 1.69 1.3888 -2 10 4 4 67.66 3.14 1.3847 0 10 5 4 68.12 2.73 1.3764 -5 5 1 4 68.16 2.67 1.3758 -1 5 8 4 69.05 2.27 1.3602 -5 5 2 4 69.26 2.50 1.3566 2 10 4 4 69.54 2.36 1.3518 -3 5 7 4 69.89 1.01 1.3459 2 6 7 4 69.97 1.20 1.3446 1 5 8 4 70.39 1.27 1.3375 2 8 6 4 70.82 1.50 1.3305 0 2 9 4 73.80 2.47 1.2840 -5 5 4 4 73.87 4.25 1.2829 2 10 5 4 74.27 2.62 1.2769 5 5 3 4 74.81 1.27 1.2692 1 11 5 4 75.29 1.16 1.2622 5 7 1 4 75.72 1.38 1.2562 4 10 0 4 75.76 2.07 1.2556 -4 10 1 4 75.93 2.50 1.2532 3 9 5 4 76.32 1.72 1.2477 -1 5 9 4 76.40 4.58 1.2466 -6 0 2 2 76.63 1.63 1.2435 4 10 1 4 76.89 1.15 1.2399 2 8 7 4 77.55 2.16 1.2309 -5 5 5 4 78.16 1.53 1.2229 5 5 4 4 79.00 1.61 1.2120 6 0 2 2 79.33 2.17 1.2078 2 10 6 4 81.68 1.57 1.1789 -2 0 10 2 81.98 2.98 1.1753 -4 4 8 4 82.88 1.21 1.1649 6 4 2 4 83.37 1.34 1.1593 -3 9 7 4 85.53 1.87 1.1354 -2 4 10 4 85.62 1.78 1.1344 2 10 7 4 85.93 2.10 1.1311 2 0 10 2 86.71 1.15 1.1229 2 14 2 4 86.83 1.04 1.1217 -6 6 3 4 87.26 1.21 1.1173 1 5 10 4 90.00 1.21 1.0903 -4 10 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.