Argyrodite Eulenberger G Monatshefte fur Chemie 108 (1977) 901-913 Die kristallstrukture der tieftemperaturmodifikation von Ag8GeS6 Locality: synthetic Note: z-coordinate of Ag6 altered to reproduce reported bond lengths _database_code_amcsd 0014663 CELL PARAMETERS: 15.1490 7.4760 10.5890 90.000 90.000 90.000 SPACE GROUP: Pna2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1199.246 Density (g/cm3): 6.247 MAX. ABS. INTENSITY / VOLUME**2: 47.07675263 RIR: 2.454 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.38 10.24 6.1606 2 0 1 2 14.50 18.54 6.1073 0 1 1 2 15.64 5.81 5.6643 1 1 1 4 21.39 1.06 4.1550 1 1 2 4 22.85 5.81 3.8917 3 1 1 4 23.49 1.14 3.7873 4 0 0 2 23.71 7.71 3.7530 2 1 2 4 24.53 5.58 3.6292 1 2 0 4 24.97 2.54 3.5660 4 0 1 2 25.95 2.67 3.4331 1 2 1 4 26.38 1.73 3.3785 4 1 0 4 27.72 29.82 3.2186 4 1 1 4 27.89 12.24 3.1993 2 0 3 2 27.92 1.91 3.1957 2 2 1 4 27.95 7.53 3.1918 0 1 3 2 28.58 17.28 3.1232 1 1 3 4 28.99 34.23 3.0803 4 0 2 2 29.25 100.00 3.0536 0 2 2 2 29.74 11.48 3.0044 3 2 0 4 29.85 20.61 2.9934 1 2 2 4 30.39 5.09 2.9413 2 1 3 4 31.41 7.75 2.8480 4 1 2 4 31.59 5.73 2.8321 2 2 2 4 31.87 23.54 2.8080 5 1 0 4 33.00 7.69 2.7142 5 1 1 4 33.21 60.45 2.6980 3 1 3 4 33.69 13.65 2.6604 4 2 0 4 33.86 8.25 2.6472 0 0 4 1 34.32 21.81 2.6130 3 2 2 4 34.74 9.93 2.5821 4 0 3 2 34.77 8.35 2.5802 4 2 1 4 35.48 10.80 2.5303 1 2 3 4 35.56 15.33 2.5248 6 0 0 2 35.94 6.49 2.4990 2 0 4 2 36.21 27.90 2.4807 5 1 2 4 36.49 19.10 2.4622 1 1 4 4 36.59 3.58 2.4560 6 0 1 2 36.83 17.42 2.4406 4 1 3 4 36.98 7.55 2.4306 2 2 3 4 37.06 15.07 2.4257 0 3 1 2 37.55 9.41 2.3952 1 3 1 4 37.96 6.18 2.3701 2 1 4 4 38.01 12.96 2.3672 2 3 0 4 38.24 3.57 2.3537 5 2 0 4 38.59 14.50 2.3333 6 1 1 4 38.99 3.95 2.3102 2 3 1 4 39.21 4.34 2.2976 5 2 1 4 39.38 1.67 2.2878 3 2 3 4 40.31 2.13 2.2372 3 1 4 4 40.45 8.19 2.2302 1 3 2 4 41.08 6.42 2.1974 5 1 3 4 41.29 9.07 2.1865 3 3 1 4 41.42 3.82 2.1799 6 1 2 4 41.81 4.68 2.1604 0 2 4 2 42.01 3.69 2.1508 5 2 2 4 43.43 2.83 2.0838 4 1 4 4 43.47 3.82 2.0818 4 3 0 4 43.54 1.03 2.0788 7 1 0 4 43.56 1.77 2.0775 2 2 4 4 44.10 8.76 2.0535 6 0 3 2 44.12 17.34 2.0526 6 2 1 4 44.35 2.28 2.0427 4 3 1 4 44.42 7.95 2.0396 2 0 5 2 44.51 4.20 2.0358 0 3 3 2 44.88 3.22 2.0194 1 1 5 4 45.68 1.75 1.9862 3 2 4 4 46.13 4.06 1.9677 2 1 5 4 46.17 2.62 1.9660 2 3 3 4 46.37 8.27 1.9583 5 2 3 4 46.68 1.45 1.9458 6 2 2 4 47.23 3.18 1.9246 5 3 0 4 48.05 3.42 1.8936 8 0 0 2 48.05 5.27 1.8936 5 3 1 4 48.16 2.76 1.8896 3 1 5 4 48.20 1.08 1.8881 3 3 3 4 48.51 32.04 1.8765 4 2 4 4 48.72 3.11 1.8690 0 4 0 2 48.86 1.92 1.8641 8 0 1 2 49.67 1.85 1.8357 8 1 0 4 49.91 3.80 1.8271 1 4 1 4 50.28 2.44 1.8146 2 4 0 4 50.45 1.46 1.8088 5 3 2 4 50.46 7.78 1.8087 8 1 1 4 50.72 1.33 1.7998 6 2 3 4 50.89 5.19 1.7944 4 1 5 4 50.93 3.61 1.7931 4 3 3 4 51.01 2.94 1.7904 2 2 5 4 51.07 4.07 1.7885 2 4 1 4 51.49 3.02 1.7748 6 1 4 4 51.78 1.16 1.7657 7 2 2 4 51.80 3.30 1.7648 0 0 6 1 52.26 1.21 1.7506 1 4 2 4 53.30 1.41 1.7188 2 0 6 2 53.71 4.19 1.7067 1 1 6 4 54.25 1.08 1.6908 5 1 5 4 54.29 3.17 1.6898 5 3 3 4 55.03 1.55 1.6687 8 0 3 2 55.20 3.01 1.6640 3 4 2 4 55.46 1.18 1.6569 4 2 5 4 56.00 2.47 1.6421 9 1 0 4 56.00 1.17 1.6420 1 4 3 4 56.02 2.01 1.6415 6 2 4 4 56.51 2.40 1.6286 8 1 3 4 56.60 1.22 1.6261 3 1 6 4 57.07 3.28 1.6138 0 3 5 2 57.62 3.57 1.5997 4 0 6 2 57.69 6.87 1.5979 4 4 2 4 57.77 2.17 1.5959 0 2 6 2 58.12 1.01 1.5871 1 2 6 4 58.18 1.44 1.5857 6 1 5 4 58.22 4.39 1.5848 6 3 3 4 58.48 1.06 1.5783 2 3 5 4 58.88 3.49 1.5684 9 1 2 4 59.37 1.94 1.5567 5 3 4 4 60.07 2.37 1.5402 8 0 4 2 60.65 5.13 1.5268 0 4 4 2 60.88 5.01 1.5217 3 2 6 4 62.00 1.36 1.4967 2 4 4 4 62.19 3.57 1.4927 8 3 1 4 62.37 2.08 1.4889 9 1 3 4 62.41 1.56 1.4880 1 5 0 4 62.44 2.28 1.4873 6 4 1 4 62.57 1.25 1.4846 4 3 5 4 62.99 1.23 1.4756 1 1 7 4 63.06 1.34 1.4741 9 2 2 4 63.09 2.25 1.4735 1 5 1 4 63.67 1.17 1.4615 3 4 4 4 64.09 1.20 1.4530 2 5 1 4 64.41 2.10 1.4465 6 0 6 2 65.05 1.47 1.4338 1 3 6 4 65.27 1.16 1.4296 10 1 2 4 65.54 1.22 1.4243 5 3 5 4 65.73 1.38 1.4207 3 5 1 4 65.97 1.78 1.4161 4 4 4 4 66.42 1.20 1.4075 9 2 3 4 67.25 1.14 1.3921 10 0 3 2 67.56 3.72 1.3865 8 3 3 4 69.87 1.11 1.3462 4 3 6 4 70.04 1.53 1.3434 11 1 1 4 70.74 1.47 1.3318 5 1 7 4 72.32 1.31 1.3065 6 4 4 4 72.45 1.19 1.3046 10 2 3 4 73.14 1.05 1.2939 4 5 3 4 76.08 1.41 1.2510 6 3 6 4 77.46 1.52 1.2321 10 0 5 2 78.36 1.84 1.2203 8 2 6 4 78.74 1.27 1.2153 4 4 6 4 81.64 1.24 1.1793 3 6 2 4 82.66 1.39 1.1674 8 1 7 4 82.75 2.15 1.1663 8 5 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.