Dolerophanite Effenberger H Monatshefte fur Chemie 116 (1985) 927-931 Cu2O(SO4), dolerophanite: Refinement of the crystal structure with a comparison of [OCu(II)4] tetrahedra in inorganic compounds Locality: synthetic _database_code_amcsd 0014667 CELL PARAMETERS: 9.3700 6.3190 7.6390 90.000 122.340 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 382.141 Density (g/cm3): 4.156 MAX. ABS. INTENSITY / VOLUME**2: 30.10979127 RIR: 2.359 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.72 82.18 6.4541 0 0 1 2 17.96 7.06 4.9387 1 1 0 4 18.63 23.44 4.7637 -1 1 1 4 19.02 8.08 4.6650 -2 0 1 2 22.46 1.45 3.9583 2 0 0 2 24.56 87.20 3.6252 -2 0 2 2 26.12 9.19 3.4110 1 1 1 4 27.64 4.04 3.2271 0 0 2 2 28.25 10.34 3.1595 0 2 0 2 31.53 18.08 2.8377 0 2 1 4 32.24 42.44 2.7766 2 0 1 2 32.26 1.55 2.7753 -3 1 1 4 33.41 4.00 2.6818 -3 1 2 4 34.28 100.00 2.6160 -2 2 1 4 35.25 26.90 2.5462 -2 0 3 2 36.38 11.72 2.4693 2 2 0 4 36.91 1.38 2.4351 3 1 0 4 37.77 6.85 2.3818 -2 2 2 4 38.06 3.08 2.3642 1 1 2 4 38.60 3.98 2.3325 -4 0 2 2 39.73 2.80 2.2690 -1 1 3 4 39.86 15.88 2.2614 -4 0 1 2 39.93 28.93 2.2576 0 2 2 4 39.94 16.23 2.2573 -3 1 3 4 42.00 2.92 2.1514 0 0 3 2 44.51 6.28 2.0355 1 3 0 4 44.73 18.63 2.0261 2 0 2 2 44.81 2.02 2.0227 -1 3 1 4 45.85 2.12 1.9792 4 0 0 2 45.87 7.30 1.9785 3 1 1 4 48.72 1.14 1.8689 1 3 1 4 49.55 1.67 1.8396 -1 3 2 4 50.08 5.41 1.8213 -3 1 4 4 50.34 1.12 1.8126 -4 0 4 2 50.89 1.86 1.7944 -5 1 2 4 51.38 6.24 1.7783 0 2 3 4 51.70 2.56 1.7681 1 1 3 4 51.73 21.15 1.7671 -4 2 3 4 53.70 1.56 1.7068 -5 1 1 4 54.73 13.29 1.6773 4 2 0 4 55.85 2.28 1.6462 3 3 0 4 56.69 3.72 1.6238 1 3 2 4 56.80 2.37 1.6210 -2 2 4 4 57.08 9.58 1.6135 0 0 4 2 57.50 6.75 1.6028 -5 1 4 4 57.58 4.14 1.6006 3 1 2 4 58.09 3.52 1.5879 -3 3 3 4 58.42 13.52 1.5797 0 4 0 2 58.73 11.33 1.5722 -4 2 4 4 59.44 1.78 1.5550 -6 0 3 2 60.26 1.16 1.5358 5 1 0 4 60.32 2.87 1.5345 0 4 1 4 61.25 2.22 1.5133 -4 0 5 2 62.64 1.07 1.4830 -3 1 5 4 62.73 1.85 1.4812 3 3 1 4 62.74 3.10 1.4809 -6 0 4 2 63.30 10.50 1.4693 4 2 1 4 64.33 5.44 1.4482 -2 4 2 4 66.49 5.85 1.4062 2 2 3 4 66.72 2.16 1.4018 1 1 4 4 67.50 15.13 1.3876 -6 2 2 4 67.56 1.02 1.3864 1 3 3 4 68.31 7.48 1.3731 2 4 1 4 68.76 4.48 1.3653 -1 1 5 4 69.48 1.06 1.3528 -6 0 5 2 69.93 1.33 1.3452 5 1 1 4 70.09 3.84 1.3426 -2 2 5 4 70.10 5.75 1.3424 -2 4 3 4 71.40 2.75 1.3211 -6 2 1 4 71.50 2.04 1.3194 6 0 0 2 72.23 2.45 1.3080 -4 4 2 4 72.59 1.31 1.3023 -5 3 4 4 72.67 3.41 1.3012 3 3 2 4 73.07 4.91 1.2951 -4 4 1 4 73.34 1.69 1.2908 0 0 5 2 76.46 3.64 1.2458 2 4 2 4 76.62 1.15 1.2436 -6 2 5 4 80.97 2.21 1.1874 1 3 4 4 82.87 2.33 1.1650 -1 3 5 4 86.15 3.09 1.1288 0 4 4 4 89.73 1.42 1.0928 -4 4 5 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.