Izoklakeite Makovicky E, Mumme W G Neues Jahrbuch fur Mineralogie, Abhandlungen 153 (1986) 121-145 The crystal structure of izoklakeite, Pb51.3Sb20.4Bi19.5Ag1.2Cu2.9Fe0.7S114. The kobellite homologous series and its derivatives Locality: Vena, Sweden _database_code_amcsd 0018392 CELL PARAMETERS: 34.0700 37.9800 4.0720 90.000 90.000 90.000 SPACE GROUP: Pnnm X-RAY WAVELENGTH: 1.541838 Cell Volume: 5269.081 Density (g/cm3): 6.681 MAX. ABS. INTENSITY / VOLUME**2: 48.47816488 RIR: 2.363 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 3.48 47.91 25.3612 1 1 0 4 4.65 1.38 18.9900 0 2 0 2 10.39 1.91 8.5175 4 0 0 2 10.46 1.45 8.4537 3 3 0 4 13.20 3.44 6.7069 5 1 0 4 13.97 2.10 6.3403 4 4 0 4 15.61 2.99 5.6783 6 0 0 2 19.14 2.18 4.6377 5 6 0 4 19.52 2.38 4.5480 6 5 0 4 20.51 2.48 4.3313 7 4 0 4 20.86 11.29 4.2587 8 0 0 2 20.99 1.98 4.2322 8 1 0 4 21.02 1.18 4.2269 6 6 0 4 21.70 3.40 4.0962 2 9 0 4 21.95 1.91 4.0488 0 1 1 4 21.98 2.14 4.0432 1 0 1 4 22.48 2.88 3.9557 3 9 0 4 22.48 2.34 3.9546 1 2 1 8 22.57 6.85 3.9391 2 1 1 8 22.67 2.04 3.9228 6 7 0 4 22.83 13.92 3.8953 5 8 0 4 22.89 1.61 3.8858 8 4 0 4 23.21 17.87 3.8331 3 0 1 4 23.42 1.48 3.7980 0 10 0 2 23.53 31.40 3.7813 4 9 0 4 23.62 18.99 3.7669 9 1 0 4 23.68 1.58 3.7573 3 2 1 8 23.92 4.65 3.7200 1 4 1 8 23.97 3.11 3.7125 9 2 0 4 24.34 12.04 3.6567 4 1 1 8 24.35 9.74 3.6552 2 4 1 8 24.72 37.64 3.6019 3 10 0 4 24.95 13.65 3.5691 1 5 1 8 25.05 19.82 3.5544 3 4 1 8 25.20 1.58 3.5335 8 6 0 4 25.33 2.43 3.5164 9 4 0 4 25.36 5.69 3.5118 2 5 1 8 25.48 6.53 3.4954 5 0 1 4 25.59 1.57 3.4807 5 1 1 8 25.68 28.37 3.4688 4 10 0 4 26.01 10.00 3.4262 4 4 1 8 26.04 63.21 3.4220 3 5 1 8 26.15 3.54 3.4074 1 6 1 8 26.16 96.46 3.4070 10 0 0 2 26.22 4.38 3.3985 7 8 0 4 26.31 82.39 3.3871 6 9 0 4 26.34 6.20 3.3839 2 11 0 4 26.45 2.52 3.3694 5 3 1 8 26.87 5.85 3.3175 5 10 0 4 26.96 45.26 3.3073 4 5 1 8 26.99 9.92 3.3034 3 11 0 4 27.20 10.79 3.2788 3 6 1 8 27.82 1.07 3.2068 10 4 0 4 27.98 6.29 3.1884 7 9 0 4 28.08 3.77 3.1774 4 6 1 8 28.15 1.42 3.1701 8 8 0 4 28.20 1.19 3.1650 0 12 0 2 28.27 32.93 3.1569 6 10 0 4 28.57 4.92 3.1248 6 4 1 8 28.58 14.33 3.1231 7 0 1 4 28.69 2.39 3.1117 2 12 0 4 28.92 3.29 3.0870 11 1 0 4 28.99 1.38 3.0799 5 11 0 4 29.01 1.41 3.0782 1 8 1 8 29.21 1.02 3.0569 11 2 0 4 29.37 13.50 3.0412 2 8 1 8 29.44 37.76 3.0337 6 5 1 8 29.69 2.62 3.0085 11 3 0 4 29.84 23.28 2.9942 7 10 0 4 30.12 12.41 2.9668 7 4 1 8 30.30 1.41 2.9502 6 11 0 4 30.46 12.30 2.9343 8 1 1 8 30.48 31.48 2.9326 6 6 1 8 30.62 17.75 2.9195 1 9 1 8 30.72 1.32 2.9109 1 13 0 4 30.74 1.12 2.9084 8 2 1 8 30.96 85.30 2.8885 7 5 1 8 31.06 1.80 2.8795 2 13 0 4 31.20 1.24 2.8667 8 3 1 8 31.51 9.84 2.8392 12 0 0 2 31.53 45.08 2.8373 3 9 1 8 31.67 3.36 2.8251 6 7 1 8 31.78 9.84 2.8161 7 11 0 4 31.83 3.38 2.8112 8 4 1 8 31.95 32.96 2.8008 7 6 1 8 32.34 1.77 2.7682 1 10 1 8 32.63 5.78 2.7443 8 5 1 8 32.64 1.99 2.7434 9 2 1 8 32.67 23.71 2.7412 2 10 1 8 32.93 1.06 2.7202 12 4 0 4 33.00 5.14 2.7147 6 8 1 8 33.28 1.24 2.6919 5 9 1 8 33.41 4.64 2.6820 8 11 0 4 33.95 6.63 2.6406 4 10 1 8 34.30 2.67 2.6146 13 1 0 4 34.37 1.11 2.6092 7 8 1 8 34.43 8.36 2.6045 9 5 1 8 34.58 1.02 2.5940 11 8 0 4 35.34 3.28 2.5396 9 6 1 8 35.39 1.65 2.5361 10 10 0 4 35.55 1.38 2.5250 1 15 0 4 35.90 5.36 2.5015 8 8 1 8 36.04 2.12 2.4922 1 12 1 8 36.34 2.44 2.4725 2 12 1 8 36.45 1.98 2.4652 11 0 1 4 38.21 1.28 2.3557 12 9 0 4 38.39 4.04 2.3448 11 5 1 8 38.70 4.76 2.3264 8 10 1 8 38.87 16.07 2.3172 9 9 1 8 39.22 3.18 2.2971 11 6 1 8 39.27 1.83 2.2944 13 8 0 4 39.36 6.12 2.2892 10 8 1 8 39.85 4.72 2.2619 12 4 1 8 40.02 10.82 2.2528 1 14 1 8 40.30 1.29 2.2381 2 14 1 8 40.46 4.66 2.2293 1 17 0 4 40.52 1.04 2.2264 13 9 0 4 41.02 1.86 2.2001 13 1 1 8 41.16 3.22 2.1930 12 11 0 4 41.88 14.32 2.1571 13 10 0 4 41.92 1.72 2.1553 8 12 1 8 41.97 5.23 2.1527 10 10 1 8 42.02 39.73 2.1502 0 15 1 4 42.09 22.27 2.1467 13 4 1 8 42.11 1.87 2.1459 1 15 1 8 42.36 2.33 2.1335 7 13 1 8 42.37 1.49 2.1333 2 15 1 8 42.45 1.44 2.1294 16 0 0 2 42.47 1.47 2.1286 11 9 1 8 42.72 23.66 2.1165 13 5 1 8 42.79 1.40 2.1134 12 12 0 4 42.80 1.52 2.1127 3 15 1 8 42.86 7.26 2.1100 0 18 0 2 42.98 1.25 2.1046 9 15 0 4 43.34 7.99 2.0875 13 11 0 4 43.38 1.56 2.0858 14 1 1 8 43.40 1.58 2.0848 4 15 1 8 43.48 2.75 2.0813 13 6 1 8 44.20 9.27 2.0490 14 10 0 4 44.22 1.01 2.0481 4 18 0 4 44.25 9.25 2.0470 1 16 1 8 44.40 3.40 2.0402 14 4 1 8 44.50 3.19 2.0360 2 16 1 8 44.50 55.28 2.0360 0 0 2 2 45.01 13.12 2.0142 14 5 1 8 45.45 2.35 1.9955 1 19 0 4 45.47 1.05 1.9947 8 14 1 8 45.70 2.47 1.9854 12 10 1 8 45.74 6.89 1.9836 15 0 1 4 45.78 1.09 1.9822 16 7 0 4 46.11 3.06 1.9687 3 19 0 4 46.15 1.44 1.9668 7 15 1 8 46.44 2.47 1.9555 1 17 1 8 46.49 8.53 1.9535 13 9 1 8 46.63 1.63 1.9477 10 13 1 8 46.85 4.67 1.9390 9 14 1 8 47.36 1.26 1.9194 8 15 1 8 47.56 2.45 1.9120 14 8 1 8 47.85 13.45 1.9011 16 9 0 4 48.07 1.52 1.8928 18 0 0 2 48.13 2.31 1.8907 8 18 0 4 48.22 1.12 1.8873 2 20 0 4 48.29 1.04 1.8846 16 1 1 8 48.36 1.68 1.8820 10 14 1 8 48.53 1.46 1.8758 12 12 1 8 48.61 6.54 1.8730 3 20 0 4 49.05 5.14 1.8574 16 10 0 4 49.16 1.03 1.8535 4 20 0 4 49.23 1.11 1.8508 16 4 1 8 49.28 2.50 1.8491 7 19 0 4 49.30 10.41 1.8484 3 18 1 8 49.32 2.33 1.8477 8 16 1 8 49.63 1.87 1.8369 8 0 2 4 49.79 2.63 1.8313 16 5 1 8 49.82 3.11 1.8304 14 10 1 8 49.99 2.96 1.8244 11 14 1 8 50.17 24.64 1.8184 10 15 1 8 50.36 1.73 1.8119 11 17 0 4 50.41 1.37 1.8103 17 9 0 4 50.47 5.12 1.8083 16 6 1 8 50.59 2.49 1.8044 5 8 2 8 50.62 2.94 1.8032 9 16 1 8 50.69 1.20 1.8010 6 20 0 4 50.86 2.26 1.7952 15 9 1 8 50.90 4.02 1.7938 10 18 0 4 50.94 5.79 1.7927 4 9 2 8 50.99 3.77 1.7912 19 1 0 4 50.99 3.92 1.7911 9 1 2 8 51.26 1.45 1.7822 16 7 1 8 51.34 2.79 1.7795 8 17 1 8 51.56 8.24 1.7724 3 10 2 8 51.67 1.22 1.7691 4 21 0 4 51.67 4.88 1.7691 7 20 0 4 51.89 1.00 1.7620 19 4 0 4 52.05 1.09 1.7570 10 16 1 8 52.09 6.32 1.7559 4 10 2 8 52.28 6.98 1.7498 17 5 1 8 52.33 5.58 1.7484 7 18 1 8 52.35 21.61 1.7477 10 0 2 4 52.44 18.70 1.7450 6 9 2 8 52.45 1.18 1.7446 2 11 2 8 52.61 1.24 1.7396 9 17 1 8 52.75 1.46 1.7353 5 10 2 8 52.78 1.29 1.7344 8 20 0 4 52.82 2.48 1.7332 3 11 2 8 52.94 3.22 1.7297 17 6 1 8 53.02 2.10 1.7270 18 9 0 4 53.15 2.81 1.7233 6 21 0 4 53.39 1.51 1.7160 7 9 2 8 53.44 1.81 1.7147 18 1 1 8 53.56 8.18 1.7110 6 10 2 8 53.81 6.81 1.7035 20 0 0 2 54.10 2.39 1.6953 7 21 0 4 54.16 3.72 1.6935 12 18 0 4 54.50 6.08 1.6836 7 10 2 8 54.65 1.28 1.6795 11 19 0 4 54.66 1.41 1.6791 9 18 1 8 55.54 2.83 1.6545 12 0 2 4 55.71 2.96 1.6499 7 11 2 8 56.04 1.26 1.6411 19 0 1 4 56.77 1.41 1.6217 8 11 2 8 56.87 1.60 1.6189 11 20 0 4 60.18 2.49 1.5377 13 20 0 4 61.70 1.87 1.5034 1 17 2 8 61.99 1.08 1.4971 14 20 0 4 62.22 1.34 1.4921 12 11 2 8 62.75 6.48 1.4806 13 10 2 8 63.50 3.31 1.4651 0 18 2 4 63.86 3.67 1.4575 13 11 2 8 64.07 1.04 1.4534 4 24 1 8 64.47 2.26 1.4452 15 18 1 8 64.52 4.51 1.4443 14 10 2 8 64.66 1.01 1.4416 16 17 1 8 65.37 1.12 1.4276 6 24 1 8 65.50 1.15 1.4251 1 19 2 8 65.72 1.79 1.4207 18 15 1 8 65.80 2.99 1.4194 21 9 1 8 66.01 1.70 1.4153 3 19 2 8 66.17 1.68 1.4123 3 25 1 8 66.60 2.24 1.4042 19 14 1 8 66.61 4.01 1.4039 4 25 1 8 67.40 6.84 1.3895 16 9 2 8 67.62 1.28 1.3854 8 18 2 8 67.89 3.46 1.3807 6 25 1 8 68.01 3.43 1.3784 3 20 2 8 68.07 3.78 1.3773 23 4 1 8 68.36 2.82 1.3722 16 10 2 8 68.46 2.91 1.3705 2 26 1 8 68.53 2.45 1.3693 23 5 1 8 68.55 1.42 1.3688 7 19 2 8 68.71 1.40 1.3661 7 25 1 8 68.99 1.08 1.3613 23 11 0 4 69.65 1.28 1.3499 19 16 1 8 69.89 2.24 1.3460 10 18 2 8 69.95 2.16 1.3448 19 1 2 8 70.52 2.78 1.3354 7 20 2 8 70.53 7.80 1.3352 20 15 1 8 71.03 1.98 1.3270 3 5 3 8 71.27 1.01 1.3232 7 26 1 8 71.43 1.14 1.3206 3 27 1 8 71.47 1.69 1.3200 4 5 3 8 71.66 1.26 1.3170 18 9 2 8 71.76 1.75 1.3154 6 21 2 8 72.08 1.23 1.3104 20 16 1 8 72.20 1.48 1.3085 8 26 1 8 72.32 4.15 1.3065 20 0 2 4 72.56 1.52 1.3028 7 21 2 8 72.61 2.26 1.3020 12 18 2 8 72.70 1.49 1.3006 6 5 3 8 73.24 1.29 1.2923 6 6 3 8 73.50 4.02 1.2885 7 5 3 8 73.71 1.17 1.2854 20 17 1 8 73.81 2.07 1.2839 3 9 3 8 74.04 1.52 1.2804 7 6 3 8 74.43 1.25 1.2746 2 10 3 8 74.95 1.09 1.2672 11 20 2 8 75.03 1.36 1.2660 0 30 0 2 75.84 1.26 1.2544 9 27 1 8 76.10 1.26 1.2508 13 25 1 8 76.27 1.07 1.2485 22 18 0 4 77.73 3.05 1.2286 14 25 1 8 77.84 1.73 1.2271 13 20 2 8 78.09 1.16 1.2239 26 6 1 8 78.16 1.11 1.2229 9 9 3 8 80.25 3.06 1.1963 0 15 3 4 80.29 1.94 1.1957 13 4 3 8 80.73 2.02 1.1904 13 5 3 8 81.03 1.59 1.1867 10 30 0 4 81.31 1.07 1.1833 16 25 1 8 81.79 1.00 1.1776 1 16 3 8 82.33 1.30 1.1712 14 5 3 8 85.49 1.16 1.1358 3 18 3 8 86.16 2.75 1.1287 10 15 3 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.