Lorandite Balic-Zunic T, Makovicky E, Moelo Y Neues Jahrbuch fur Mineralogie, Abhandlungen 168 (1995) 213-235 Contributions to the crystal chemistry of thallium sulphosalts III. The crystal structure of lorandite (TlAsS2) and its relation to weissbergite (TlSbS2) Locality: Crven Dol, Allchar, Republic of Macedonia _database_code_amcsd 0014720 CELL PARAMETERS: 12.2960 11.3130 6.1140 90.000 104.210 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 824.463 Density (g/cm3): 5.533 MAX. ABS. INTENSITY / VOLUME**2: 44.22744957 RIR: 2.603 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.78 9.56 8.2056 1 1 0 4 14.86 14.97 5.9599 2 0 0 2 16.81 22.90 5.2729 2 1 0 4 16.91 20.80 5.2436 -1 1 1 4 17.35 1.15 5.1103 1 2 0 4 18.34 2.83 4.8381 -2 0 1 2 19.91 5.63 4.4602 1 1 1 4 19.96 3.48 4.4484 -2 1 1 4 21.66 4.95 4.1028 2 2 0 4 21.72 11.92 4.0920 0 2 1 4 21.73 29.43 4.0890 -1 2 1 4 23.63 11.48 3.7657 2 0 1 2 23.73 8.32 3.7488 3 1 0 4 24.16 90.23 3.6833 1 2 1 4 24.21 64.15 3.6767 -2 2 1 4 24.76 64.02 3.5954 1 3 0 4 24.92 63.92 3.5730 2 1 1 4 24.99 100.00 3.5629 -3 1 1 4 27.43 3.24 3.2513 3 2 0 4 28.00 1.03 3.1867 2 3 0 4 28.05 41.15 3.1816 0 3 1 4 28.47 7.82 3.1346 2 2 1 4 28.54 5.67 3.1278 -3 2 1 4 29.99 21.81 2.9799 4 0 0 2 30.01 16.91 2.9778 1 3 1 4 30.04 7.76 2.9743 -2 3 1 4 30.08 1.51 2.9711 -4 0 1 2 30.16 41.79 2.9635 0 0 2 2 30.21 10.47 2.9588 -2 0 2 2 30.29 24.07 2.9511 -1 1 2 4 31.03 62.81 2.8816 4 1 0 4 31.04 23.27 2.8811 3 1 1 4 31.20 7.92 2.8667 0 1 2 4 31.25 60.89 2.8626 -2 1 2 4 32.54 80.15 2.7518 1 4 0 4 32.74 8.22 2.7352 3 3 0 4 33.32 8.00 2.6894 -1 2 2 4 33.63 4.48 2.6646 2 3 1 4 33.69 5.13 2.6604 -3 3 1 4 33.85 7.08 2.6480 1 1 2 4 33.94 5.22 2.6414 -3 1 2 4 34.00 16.42 2.6365 4 2 0 4 34.01 5.22 2.6360 3 2 1 4 34.09 21.41 2.6303 -4 2 1 4 34.16 1.55 2.6250 0 2 2 4 34.20 1.32 2.6218 -2 2 2 4 35.17 1.04 2.5518 -1 4 1 4 36.62 1.24 2.4540 1 2 2 4 36.94 6.46 2.4334 4 0 1 2 37.05 16.71 2.4267 2 0 2 2 37.17 9.54 2.4191 -4 0 2 2 37.82 9.97 2.3790 4 1 1 4 37.89 6.20 2.3747 -1 3 2 4 37.91 2.24 2.3736 -5 1 1 4 38.04 14.20 2.3656 -4 1 2 4 38.58 7.97 2.3338 -4 3 1 4 38.60 1.74 2.3327 5 1 0 4 38.64 2.10 2.3301 0 3 2 4 38.68 6.21 2.3278 -2 3 2 4 39.09 43.74 2.3041 3 4 0 4 39.91 1.16 2.2589 -3 4 1 4 40.35 12.88 2.2353 4 2 1 4 40.43 3.21 2.2309 -5 2 1 4 40.45 1.31 2.2301 2 2 2 4 40.58 5.50 2.2229 1 5 0 4 40.87 8.63 2.2080 1 3 2 4 40.95 4.59 2.2041 -3 3 2 4 41.09 9.95 2.1968 5 2 0 4 42.75 3.71 2.1153 2 5 0 4 42.78 6.33 2.1138 0 5 1 4 42.79 3.55 2.1134 -1 5 1 4 43.07 10.04 2.1002 3 1 2 4 43.21 3.11 2.0936 -5 1 2 4 43.60 45.12 2.0760 -1 4 2 4 44.15 3.08 2.0512 3 4 1 4 44.16 4.95 2.0507 1 5 1 4 44.19 5.93 2.0495 -2 5 1 4 44.30 1.38 2.0447 4 3 1 4 44.38 7.25 2.0413 -5 3 1 4 44.39 10.07 2.0406 2 3 2 4 44.39 10.65 2.0406 -6 0 1 2 44.99 8.26 2.0151 5 3 0 4 45.15 1.15 2.0082 -6 1 1 4 45.36 2.97 1.9994 3 2 2 4 45.36 9.87 1.9992 -1 1 3 4 45.94 5.33 1.9756 0 0 3 2 46.17 7.58 1.9662 3 5 0 4 46.34 8.25 1.9592 -3 4 2 4 46.41 1.27 1.9567 6 1 0 4 46.67 8.07 1.9462 0 1 3 4 46.75 5.32 1.9432 -3 1 3 4 46.84 5.47 1.9394 2 5 1 4 46.88 1.17 1.9378 -3 5 1 4 47.59 8.26 1.9107 -2 2 3 4 48.50 5.06 1.8770 -6 0 2 2 48.64 4.14 1.8718 -4 0 3 2 48.83 3.21 1.8652 0 2 3 4 48.90 2.70 1.8626 -3 2 3 4 48.99 6.73 1.8594 3 3 2 4 49.05 1.68 1.8573 4 1 2 4 49.12 18.30 1.8549 -5 3 2 4 49.21 5.56 1.8516 -6 1 2 4 49.35 1.75 1.8467 -4 1 3 4 49.48 2.12 1.8421 -5 4 1 4 49.59 1.00 1.8383 -4 4 2 4 50.16 2.96 1.8186 -1 5 2 4 50.66 1.99 1.8019 3 5 1 4 50.72 6.37 1.8001 -4 5 1 4 50.79 4.15 1.7975 5 3 1 4 50.80 4.91 1.7973 -2 5 2 4 50.82 3.31 1.7968 0 6 1 4 50.82 5.51 1.7965 -1 6 1 4 50.88 7.74 1.7947 -6 3 1 4 51.10 1.66 1.7875 -2 3 3 4 51.13 5.12 1.7865 4 2 2 4 51.28 1.01 1.7814 -6 2 2 4 51.31 1.34 1.7808 1 2 3 4 51.42 1.48 1.7770 -4 2 3 4 52.02 12.79 1.7581 6 0 1 2 52.03 4.46 1.7575 1 6 1 4 52.06 7.06 1.7568 -2 6 1 4 52.23 1.63 1.7513 2 0 3 2 52.27 3.32 1.7500 0 3 3 4 52.59 3.31 1.7404 1 5 2 4 52.65 2.50 1.7385 -3 5 2 4 52.79 6.62 1.7342 -7 1 1 4 53.06 1.29 1.7259 -5 1 3 4 53.76 4.70 1.7052 3 4 2 4 54.42 2.67 1.6860 2 6 1 4 54.49 1.58 1.6839 7 1 0 4 54.62 3.36 1.6803 -6 3 2 4 54.64 6.85 1.6798 1 3 3 4 54.67 1.25 1.6789 6 2 1 4 54.75 5.31 1.6766 -4 3 3 4 54.77 3.74 1.6761 -7 2 1 4 55.04 5.47 1.6686 -5 2 3 4 55.45 20.63 1.6571 5 4 1 4 55.52 2.03 1.6552 -5 5 1 4 55.53 6.98 1.6549 2 5 2 4 55.69 2.52 1.6504 5 1 2 4 55.72 4.12 1.6498 -1 4 3 4 56.43 6.86 1.6305 7 2 0 4 56.91 3.40 1.6179 -3 4 3 4 57.11 1.48 1.6127 -6 0 3 2 57.55 5.05 1.6015 3 1 3 4 57.74 3.72 1.5966 -6 1 3 4 57.87 3.32 1.5933 4 6 0 4 57.88 2.09 1.5932 3 6 1 4 57.96 1.62 1.5911 -7 3 1 4 57.97 1.21 1.5908 0 6 2 4 58.07 4.23 1.5884 2 3 3 4 59.24 5.27 1.5598 2 7 0 4 59.27 2.76 1.5590 -1 7 1 4 59.49 1.18 1.5537 3 5 2 4 59.61 7.90 1.5511 -5 5 2 4 59.61 1.32 1.5509 -6 2 3 4 59.64 4.23 1.5503 1 6 2 4 60.37 1.23 1.5334 1 7 1 4 60.39 1.34 1.5329 -2 7 1 4 60.58 2.22 1.5285 -2 0 4 2 60.82 3.53 1.5230 -8 1 1 4 61.08 2.31 1.5171 5 5 1 4 61.16 4.50 1.5154 -6 5 1 4 61.71 1.23 1.5032 -1 1 4 4 62.26 3.16 1.4912 -7 4 1 4 62.29 1.28 1.4904 4 6 1 4 62.36 6.17 1.4891 -5 6 1 4 62.40 1.01 1.4882 0 5 3 4 62.45 2.84 1.4871 4 0 3 2 62.47 4.05 1.4867 3 3 3 4 62.51 1.46 1.4859 -5 4 3 4 62.52 1.55 1.4856 -8 0 2 2 62.53 1.47 1.4854 7 2 1 4 62.58 2.30 1.4844 -3 7 1 4 62.63 1.50 1.4832 -8 2 1 4 62.70 1.55 1.4817 0 0 4 2 62.81 5.51 1.4794 -4 0 4 2 62.84 1.14 1.4789 5 6 0 4 62.99 1.29 1.4756 -2 2 4 4 63.05 5.91 1.4744 4 1 3 4 63.27 2.92 1.4697 -7 1 3 4 63.30 2.37 1.4692 0 1 4 4 63.56 2.42 1.4638 -3 2 4 4 64.52 3.22 1.4442 1 5 3 4 64.62 4.39 1.4422 -4 5 3 4 64.70 2.55 1.4408 8 2 0 4 64.71 2.81 1.4405 6 2 2 4 64.90 1.13 1.4368 -8 2 2 4 65.05 2.92 1.4339 -7 2 3 4 65.07 2.85 1.4334 0 2 4 4 65.49 3.27 1.4252 7 3 1 4 65.73 4.13 1.4207 4 7 0 4 65.73 1.02 1.4206 3 7 1 4 65.82 1.48 1.4189 0 7 2 4 65.85 3.86 1.4184 -2 7 2 4 65.93 1.96 1.4169 1 1 4 4 66.07 6.93 1.4141 0 8 0 2 66.08 1.04 1.4139 3 6 2 4 66.19 1.03 1.4119 -5 6 2 4 66.49 3.26 1.4062 -3 3 4 4 67.47 1.42 1.3883 6 5 1 4 67.55 1.08 1.3867 -7 5 1 4 67.60 2.52 1.3857 8 3 0 4 67.62 1.20 1.3855 6 3 2 4 67.65 2.55 1.3849 2 5 3 4 67.66 1.70 1.3847 1 2 4 4 67.84 1.24 1.3815 -2 6 3 4 68.15 1.12 1.3759 2 8 0 4 68.61 3.68 1.3678 8 0 1 2 68.89 1.52 1.3630 -3 6 3 4 69.03 1.29 1.3606 7 5 0 4 69.53 1.27 1.3521 2 1 4 4 69.73 2.42 1.3485 -6 1 4 4 69.87 3.32 1.3463 4 7 1 4 70.01 1.66 1.3438 -4 7 2 4 70.45 5.87 1.3366 -1 4 4 4 70.67 3.27 1.3330 -5 3 4 4 70.85 1.14 1.3299 1 6 3 4 70.95 2.91 1.3284 -9 1 2 4 71.02 1.11 1.3273 5 2 3 4 71.27 4.07 1.3232 -8 2 3 4 71.72 2.24 1.3160 3 5 3 4 71.76 1.49 1.3154 9 1 0 4 72.43 2.69 1.3049 7 2 2 4 73.76 1.07 1.2846 -7 6 1 4 73.99 3.32 1.2812 -5 6 3 4 74.23 1.14 1.2776 4 8 0 4 74.32 3.56 1.2763 0 8 2 4 74.57 1.91 1.2726 -5 4 4 4 74.99 1.07 1.2666 -2 5 4 4 75.12 2.30 1.2647 -1 7 3 4 75.18 1.70 1.2637 7 6 0 4 75.46 1.41 1.2598 -1 5 4 4 75.51 1.26 1.2591 -3 5 4 4 75.70 1.68 1.2564 3 2 4 4 76.33 1.06 1.2476 6 1 3 4 76.56 2.46 1.2444 8 5 0 4 77.63 3.13 1.2299 -9 4 1 4 77.65 4.69 1.2296 5 4 3 4 77.90 1.13 1.2263 4 7 2 4 78.24 2.20 1.2218 2 8 2 4 78.25 1.02 1.2218 -9 2 3 4 78.27 1.63 1.2214 -2 0 5 2 78.29 2.07 1.2211 -10 1 1 4 78.32 2.34 1.2208 -4 8 2 4 79.22 3.15 1.2092 -9 4 2 4 80.47 1.54 1.1935 -3 2 5 4 80.57 1.70 1.1923 2 9 1 4 80.60 2.35 1.1920 -3 9 1 4 80.97 1.60 1.1874 -2 6 4 4 81.67 1.14 1.1789 0 1 5 4 82.45 3.44 1.1698 -7 4 4 4 82.50 1.23 1.1693 9 3 1 4 82.52 1.76 1.1690 8 6 0 4 82.53 1.74 1.1689 6 6 2 4 82.71 1.71 1.1668 2 5 4 4 82.75 1.13 1.1664 10 2 0 4 83.10 1.80 1.1623 -6 8 1 4 83.23 1.45 1.1608 5 7 2 4 83.46 1.13 1.1582 4 9 0 4 83.46 1.43 1.1581 3 9 1 4 83.57 1.64 1.1569 -2 9 2 4 83.88 1.40 1.1535 -10 0 3 2 84.10 1.41 1.1510 7 1 3 4 84.71 1.94 1.1443 -9 4 3 4 86.09 1.33 1.1294 -6 8 2 4 86.24 3.20 1.1279 9 4 1 4 86.36 1.16 1.1266 -6 2 5 4 87.80 2.21 1.1118 -1 4 5 4 87.84 1.62 1.1114 10 1 1 4 87.93 1.20 1.1105 -2 7 4 4 88.63 1.31 1.1036 -7 1 5 4 88.63 2.30 1.1035 -8 6 3 4 88.79 2.25 1.1019 6 8 1 4 88.81 1.30 1.1018 1 10 1 4 88.97 1.12 1.1002 2 8 3 4 89.58 1.29 1.0943 4 7 3 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.