Fuloppite Edenharter A, Nowacki W Neues Jahrbuch fur Mineralogie, Monatshefte 1974 (1974) 92-94 Die kristallstruktur von fuloppit Pb3Sb8S15 Locality: Baia Mare, Romania _database_code_amcsd 0014749 CELL PARAMETERS: 13.4350 11.7270 16.9340 90.000 94.700 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2659.019 Density (g/cm3): 5.187 MAX. ABS. INTENSITY / VOLUME**2: 31.79390300 RIR: 1.996 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.48 2.19 8.4385 0 0 2 2 11.06 1.21 7.9975 -1 1 1 4 13.22 1.31 6.6949 2 0 0 2 14.13 64.73 6.2694 -1 1 2 4 14.91 9.27 5.9399 1 1 2 4 16.00 25.36 5.5387 0 2 1 4 17.57 1.67 5.0473 2 0 2 2 18.24 7.80 4.8638 -1 1 3 4 18.43 5.39 4.8152 0 2 2 4 20.13 3.33 4.4110 2 2 0 4 20.53 8.01 4.3251 -2 2 1 4 21.30 14.96 4.1714 3 1 0 4 21.55 4.09 4.1237 -3 1 1 4 21.89 17.45 4.0594 0 2 3 4 22.23 8.17 3.9987 -2 2 2 4 22.34 15.11 3.9792 3 1 1 4 22.87 100.00 3.8889 -1 1 4 4 23.05 2.28 3.8587 -3 1 2 4 23.25 5.40 3.8253 2 2 2 4 23.71 35.37 3.7524 1 3 0 4 23.99 4.29 3.7093 -2 0 4 2 24.18 49.96 3.6809 -1 3 1 4 24.42 21.60 3.6452 1 3 1 4 24.52 52.64 3.6306 3 1 2 4 24.97 14.49 3.5659 -2 2 3 4 25.87 4.75 3.4445 2 0 4 2 26.34 65.15 3.3836 2 2 3 4 26.63 7.75 3.3475 4 0 0 2 27.58 66.32 3.2343 3 1 3 4 27.78 33.90 3.2109 -1 1 5 4 27.86 56.21 3.2028 -4 0 2 2 28.28 8.62 3.1553 -1 3 3 4 28.47 50.30 3.1347 -2 2 4 4 28.83 8.26 3.0972 1 1 5 4 28.90 2.50 3.0891 1 3 3 4 30.09 27.16 2.9699 2 2 4 4 30.40 1.76 2.9406 3 3 0 4 30.49 3.49 2.9318 0 4 0 2 30.58 74.09 2.9238 -3 3 1 4 30.76 4.86 2.9071 4 2 0 4 30.84 15.72 2.8996 -4 2 1 4 30.96 6.48 2.8885 0 4 1 4 31.15 7.15 2.8709 3 3 1 4 31.29 20.74 2.8589 3 1 4 4 31.60 28.84 2.8314 4 2 1 4 31.68 48.81 2.8246 -3 3 2 4 31.81 1.53 2.8128 0 0 6 2 32.33 4.53 2.7694 0 4 2 4 32.52 60.24 2.7533 -2 2 5 4 32.76 5.00 2.7337 -4 0 4 2 32.79 3.34 2.7314 3 3 2 4 32.83 2.78 2.7281 -3 1 5 4 33.30 15.19 2.6902 4 2 2 4 33.36 9.63 2.6855 2 4 0 4 33.62 12.19 2.6658 -3 3 3 4 33.62 12.60 2.6658 -2 4 1 4 33.68 6.27 2.6610 -4 2 3 4 34.31 10.54 2.6134 2 2 5 4 34.35 1.91 2.6108 5 1 0 4 35.16 2.63 2.5524 -5 1 2 4 35.19 3.62 2.5502 3 3 3 4 35.36 3.69 2.5386 -1 3 5 4 35.47 5.90 2.5309 3 1 5 4 35.62 24.49 2.5206 2 0 6 2 35.76 1.92 2.5108 4 2 3 4 36.20 1.05 2.4813 1 3 5 4 36.28 1.47 2.4760 -3 3 4 4 36.96 19.90 2.4319 -2 2 6 4 37.16 1.09 2.4196 -3 1 6 4 37.35 6.22 2.4076 0 4 4 4 39.18 4.37 2.2991 5 1 3 4 39.27 9.40 2.2944 1 1 7 4 39.44 6.89 2.2846 -4 2 5 4 39.60 1.35 2.2759 -1 3 6 4 40.40 5.20 2.2326 2 4 4 4 40.63 1.14 2.2203 1 5 2 4 40.77 20.81 2.2134 0 4 5 4 40.83 15.06 2.2099 -5 3 1 4 40.85 4.40 2.2093 5 3 0 4 40.92 2.44 2.2055 4 4 0 4 41.55 7.19 2.1735 -5 3 2 4 41.58 1.22 2.1719 4 4 1 4 41.71 3.00 2.1654 -2 2 7 4 41.77 1.41 2.1626 -4 4 2 4 41.82 3.06 2.1602 3 3 5 4 42.03 1.79 2.1499 -5 1 5 4 42.51 61.83 2.1265 1 5 3 4 42.75 3.72 2.1151 6 0 2 2 42.94 2.56 2.1062 4 4 2 4 42.96 5.07 2.1054 -5 3 3 4 43.02 1.29 2.1027 5 3 2 4 43.13 1.79 2.0974 -4 2 6 4 43.25 5.90 2.0921 -4 4 3 4 43.30 3.29 2.0898 -3 3 6 4 43.30 1.37 2.0895 -6 2 1 4 43.59 3.20 2.0762 3 5 0 4 43.75 10.90 2.0691 2 2 7 4 43.93 5.55 2.0611 -2 0 8 2 44.16 27.88 2.0509 6 2 1 4 44.18 3.39 2.0499 -1 3 7 4 44.44 8.26 2.0385 -1 5 4 4 44.64 6.81 2.0297 0 4 6 4 44.70 22.93 2.0272 1 1 8 4 44.95 11.36 2.0167 4 4 3 4 45.16 5.13 2.0075 1 3 7 4 45.38 9.57 1.9985 3 5 2 4 45.47 25.54 1.9946 -5 1 6 4 45.59 1.49 1.9896 5 1 5 4 45.60 15.03 1.9896 6 2 2 4 45.83 4.92 1.9800 3 3 6 4 45.95 3.80 1.9751 -2 4 6 4 46.02 3.00 1.9724 -3 5 3 4 46.46 1.19 1.9545 0 6 0 2 46.72 2.31 1.9445 -2 2 8 4 46.74 4.03 1.9435 -3 1 8 4 46.79 1.31 1.9415 0 6 1 4 47.54 1.07 1.9126 4 4 4 4 47.63 9.36 1.9091 6 0 4 2 47.65 3.62 1.9086 -5 3 5 4 48.04 1.39 1.8940 1 5 5 4 48.05 9.15 1.8937 -4 4 5 4 48.06 4.74 1.8932 -7 1 1 4 48.10 2.09 1.8917 -3 5 4 4 48.20 8.71 1.8879 7 1 0 4 48.52 2.56 1.8762 2 6 0 4 48.56 3.34 1.8749 -7 1 2 4 48.71 16.14 1.8694 -2 6 1 4 48.85 2.36 1.8644 2 2 8 4 48.91 6.87 1.8622 0 4 7 4 48.98 1.04 1.8596 7 1 1 4 49.05 2.14 1.8572 -1 3 8 4 49.36 10.01 1.8463 -5 1 7 4 49.49 11.32 1.8416 5 1 6 4 49.53 9.08 1.8404 -2 6 2 4 49.59 2.82 1.8384 -6 2 5 4 49.68 2.11 1.8351 -7 1 3 4 50.04 1.15 1.8226 2 6 2 4 50.05 1.77 1.8225 -6 0 6 2 50.21 2.57 1.8170 3 3 7 4 50.29 6.55 1.8144 1 1 9 4 50.74 9.70 1.7993 -3 5 5 4 50.78 2.62 1.7978 -1 5 6 4 50.80 1.27 1.7975 -5 3 6 4 50.90 1.17 1.7941 4 2 7 4 50.91 7.39 1.7938 5 3 5 4 51.24 5.21 1.7830 -4 4 6 4 51.53 1.00 1.7735 0 6 4 4 51.55 2.85 1.7730 1 5 6 4 51.91 7.71 1.7615 -3 1 9 4 51.95 10.06 1.7603 -2 2 9 4 52.35 4.05 1.7477 7 1 3 4 52.43 12.84 1.7451 5 5 1 4 52.59 7.50 1.7403 -6 2 6 4 53.06 9.74 1.7260 -6 4 3 4 53.18 1.45 1.7222 4 0 8 2 53.38 1.42 1.7165 6 2 5 4 53.42 3.18 1.7153 6 4 2 4 53.51 4.65 1.7124 0 4 8 4 53.64 1.21 1.7087 5 5 2 4 53.65 1.67 1.7084 -7 3 2 4 53.94 1.11 1.6999 2 6 4 4 54.17 1.23 1.6932 2 2 9 4 54.17 4.79 1.6930 -1 3 9 4 54.22 9.70 1.6918 4 4 6 4 54.23 3.71 1.6914 0 6 5 4 54.36 2.68 1.6877 0 0 10 2 54.40 1.27 1.6866 -5 3 7 4 54.70 6.96 1.6781 -7 3 3 4 54.76 2.93 1.6762 -6 4 4 4 54.88 1.26 1.6729 -4 4 7 4 54.92 1.72 1.6719 3 3 8 4 55.04 1.35 1.6684 -4 6 2 4 55.05 5.49 1.6680 -8 0 2 2 55.26 1.91 1.6623 1 7 0 4 55.26 2.30 1.6622 1 3 9 4 55.41 1.16 1.6582 5 5 3 4 55.49 1.68 1.6560 -1 7 1 4 55.61 2.01 1.6527 1 7 1 4 55.62 1.40 1.6524 4 2 8 4 56.03 1.12 1.6414 1 1 10 4 56.94 2.70 1.6172 6 2 6 4 57.24 1.73 1.6094 8 2 0 4 57.30 2.28 1.6079 -3 1 10 4 57.40 1.38 1.6055 -2 2 10 4 57.41 1.30 1.6051 0 6 6 4 57.55 8.61 1.6014 -8 0 4 2 58.20 6.62 1.5853 4 4 7 4 58.38 1.59 1.5806 -8 2 3 4 58.55 2.03 1.5766 5 3 7 4 58.88 2.13 1.5684 3 7 0 4 58.93 1.04 1.5673 -4 4 8 4 59.57 3.11 1.5519 7 3 4 4 59.65 3.54 1.5501 -3 7 2 4 59.72 1.12 1.5484 -7 1 7 4 59.78 1.21 1.5470 1 5 8 4 59.88 1.54 1.5445 2 6 6 4 59.89 1.79 1.5444 3 5 7 4 60.02 3.48 1.5413 1 7 4 4 60.64 2.49 1.5271 4 2 9 4 60.86 2.48 1.5222 -3 7 3 4 61.03 1.91 1.5183 0 6 7 4 61.95 2.31 1.4980 1 1 11 4 62.43 3.43 1.4876 7 3 5 4 62.54 2.21 1.4853 4 6 5 4 62.67 2.13 1.4823 7 5 0 4 62.79 2.10 1.4799 -5 3 9 4 62.97 1.56 1.4761 -7 5 2 4 63.25 2.60 1.4703 6 6 0 4 63.33 2.24 1.4685 5 1 9 4 63.34 6.81 1.4683 -4 4 9 4 63.45 2.72 1.4661 -1 5 9 4 63.76 2.62 1.4597 4 0 10 2 64.52 1.91 1.4442 0 8 2 4 64.65 5.09 1.4417 -6 6 3 4 64.76 2.35 1.4394 8 4 1 4 65.05 2.41 1.4338 0 6 8 4 65.20 1.82 1.4308 3 3 10 4 65.68 2.92 1.4216 4 6 6 4 65.86 1.90 1.4182 -2 6 8 4 65.95 1.57 1.4165 4 2 10 4 66.17 3.41 1.4123 -6 6 4 4 66.25 4.89 1.4106 -5 7 2 4 66.38 1.09 1.4083 2 4 10 4 66.41 3.42 1.4077 2 8 2 4 66.48 5.93 1.4064 0 0 12 2 66.69 1.05 1.4025 -6 0 10 2 67.12 2.34 1.3946 -9 1 5 4 67.29 2.23 1.3914 -3 3 11 4 67.33 1.02 1.3907 5 7 2 4 67.41 1.19 1.3892 8 0 6 2 67.54 2.73 1.3870 -3 7 6 4 67.66 3.69 1.3847 0 8 4 4 68.11 2.57 1.3766 -4 4 10 4 68.20 1.67 1.3751 -1 7 7 4 68.23 1.71 1.3746 -9 3 3 4 68.37 1.14 1.3721 -1 5 10 4 68.58 1.15 1.3684 5 1 10 4 68.67 1.02 1.3669 -8 0 8 2 68.79 1.74 1.3647 -3 1 12 4 68.83 2.24 1.3641 -6 2 10 4 68.87 1.91 1.3633 -2 8 4 4 69.11 3.88 1.3591 9 1 4 4 69.45 2.51 1.3534 3 7 6 4 69.94 1.81 1.3451 8 4 4 4 70.56 1.45 1.3347 -3 5 10 4 70.78 1.85 1.3311 3 3 11 4 71.03 2.40 1.3270 -1 3 12 4 71.07 2.26 1.3264 9 3 3 4 71.51 6.24 1.3194 4 8 2 4 71.55 1.42 1.3187 4 2 11 4 71.86 1.81 1.3137 2 4 11 4 71.96 2.04 1.3122 -1 7 8 4 72.13 1.75 1.3096 -10 2 1 4 72.31 1.07 1.3067 4 4 10 4 72.36 1.49 1.3060 10 0 2 2 72.73 3.86 1.3001 -7 5 7 4 72.89 2.46 1.2978 3 7 7 4 73.24 1.64 1.2924 8 2 7 4 73.25 1.30 1.2923 1 9 1 4 73.26 1.21 1.2922 4 6 8 4 73.67 1.60 1.2859 -8 4 7 4 73.82 3.78 1.2837 -6 2 11 4 74.09 1.35 1.2797 7 1 9 4 74.40 1.06 1.2751 6 6 6 4 74.88 1.35 1.2681 0 4 12 4 75.23 1.05 1.2631 -2 4 12 4 75.32 1.92 1.2618 8 6 1 4 75.49 3.96 1.2593 -9 5 1 4 75.56 2.06 1.2583 -9 1 8 4 76.20 3.37 1.2493 6 4 9 4 76.32 1.11 1.2477 -5 7 7 4 76.36 1.57 1.2471 10 0 4 2 76.41 4.23 1.2465 9 5 1 4 76.50 1.17 1.2453 3 9 1 4 76.82 2.20 1.2408 -7 1 11 4 76.83 1.93 1.2407 2 6 10 4 76.97 2.19 1.2388 -8 4 8 4 76.98 1.29 1.2387 -8 6 4 4 77.20 1.92 1.2357 -1 3 13 4 77.36 2.13 1.2336 8 2 8 4 77.85 1.09 1.2270 -3 9 3 4 78.17 1.35 1.2228 7 3 9 4 78.47 1.24 1.2189 -4 6 10 4 78.72 2.23 1.2156 9 1 7 4 78.88 1.54 1.2135 3 1 13 4 79.56 1.27 1.2048 6 8 2 4 80.75 1.72 1.1901 7 7 4 4 80.76 1.76 1.1900 -5 5 11 4 81.66 1.12 1.1792 -2 2 14 4 82.04 2.18 1.1746 2 6 11 4 82.07 1.19 1.1743 -7 1 12 4 82.10 1.34 1.1739 -10 4 5 4 82.20 1.13 1.1727 0 10 0 2 82.76 1.19 1.1662 -5 9 2 4 82.86 2.18 1.1650 -4 0 14 2 83.27 2.74 1.1603 7 7 5 4 83.39 1.15 1.1590 8 4 8 4 83.73 1.05 1.1552 4 2 13 4 83.87 2.36 1.1535 -2 10 1 4 84.01 1.76 1.1520 -10 2 8 4 84.87 1.37 1.1425 -7 7 7 4 85.29 1.46 1.1380 -2 6 12 4 85.36 1.20 1.1372 -3 3 14 4 85.82 1.08 1.1323 8 6 6 4 86.24 1.06 1.1279 6 6 9 4 86.38 3.16 1.1264 -11 3 5 4 86.98 1.13 1.1201 -8 6 8 4 88.71 1.49 1.1027 8 8 0 4 88.99 1.40 1.1000 3 9 7 4 89.16 1.50 1.0984 -12 2 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.