Krupkaite Synecek V, Hybler J Neues Jahrbuch fur Mineralogie, Monatshefte 1974 (1974) 541-560 The crystal structures of krupkaite, CuPbBi3S6, and of gladite, CuPbBi5S9, and the classification of superstructures in the bismuthinite-aikinite group, Locality: Krupka, Ore Mountains, NW-Bohemia _database_code_amcsd 0014750 CELL PARAMETERS: 11.1500 11.5100 4.0100 90.000 90.000 90.000 SPACE GROUP: Pb2_1m X-RAY WAVELENGTH: 1.541838 Cell Volume: 514.629 Density (g/cm3): 7.034 MAX. ABS. INTENSITY / VOLUME**2: 88.15117303 RIR: 4.081 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.05 2.89 8.0085 1 1 0 2 15.40 12.69 5.7550 0 2 0 1 15.90 2.40 5.5750 2 0 0 2 17.34 25.89 5.1140 1 2 0 2 22.17 1.12 4.0100 0 0 1 2 22.20 40.47 4.0042 2 2 0 2 23.58 21.58 3.7734 1 0 1 4 23.94 8.72 3.7167 3 0 0 2 24.54 100.00 3.6279 1 3 0 2 24.83 50.14 3.5856 1 1 1 4 25.18 91.54 3.5368 3 1 0 2 27.10 20.25 3.2901 0 2 1 2 28.24 11.64 3.1606 2 3 0 2 28.28 58.64 3.1556 1 2 1 4 28.49 88.42 3.1325 2 1 1 4 28.59 4.44 3.1222 3 2 0 2 31.08 4.16 2.8775 0 4 0 1 31.58 79.17 2.8335 2 2 1 4 32.11 1.90 2.7875 4 0 0 2 32.13 4.32 2.7862 1 4 0 2 32.86 19.81 2.7259 3 0 1 4 33.06 6.62 2.7092 4 1 0 2 33.57 5.74 2.6695 3 3 0 2 33.79 40.87 2.6525 3 1 1 4 35.09 41.45 2.5570 2 4 0 2 35.79 17.32 2.5087 4 2 0 2 36.19 17.81 2.4822 2 3 1 4 36.47 5.17 2.4635 3 2 1 4 38.51 28.25 2.3379 0 4 1 2 39.37 1.15 2.2888 4 0 1 4 39.38 24.89 2.2881 1 4 1 4 39.61 2.16 2.2753 3 4 0 2 39.98 6.41 2.2551 4 3 0 2 40.17 16.51 2.2449 4 1 1 4 40.60 8.61 2.2221 3 3 1 4 41.24 3.03 2.1893 5 1 0 2 41.90 8.97 2.1560 2 4 1 4 42.49 12.14 2.1277 2 5 0 2 42.51 19.58 2.1268 4 2 1 4 43.52 4.58 2.0794 5 2 0 2 45.23 37.89 2.0050 0 0 2 2 45.29 3.22 2.0021 4 4 0 2 45.85 2.18 1.9789 3 4 1 4 46.18 36.54 1.9656 4 3 1 4 46.19 12.81 1.9652 1 5 1 4 46.40 10.02 1.9570 3 5 0 2 46.60 12.66 1.9489 5 0 1 4 47.14 21.02 1.9280 5 3 0 2 47.31 4.23 1.9216 5 1 1 4 47.39 7.66 1.9183 0 6 0 1 48.05 1.24 1.8934 0 2 2 2 48.13 2.45 1.8906 1 6 0 2 48.43 8.71 1.8795 2 5 1 4 48.79 2.98 1.8667 1 2 2 4 49.02 8.16 1.8583 6 0 0 2 49.37 5.80 1.8459 5 2 1 4 49.70 4.30 1.8346 6 1 0 2 50.30 3.02 1.8139 2 6 0 2 50.94 8.21 1.7928 2 2 2 4 50.98 2.00 1.7913 4 4 1 4 51.69 2.55 1.7684 6 2 0 2 51.81 1.92 1.7646 3 0 2 4 51.87 3.38 1.7626 5 4 0 2 52.00 15.80 1.7588 3 5 1 4 52.12 23.04 1.7548 1 3 2 4 52.46 22.22 1.7442 3 1 2 4 52.68 6.90 1.7376 5 3 1 4 52.91 11.13 1.7305 0 6 1 2 53.59 6.52 1.7100 1 6 1 4 53.78 2.39 1.7047 3 6 0 2 54.17 2.96 1.6931 2 3 2 4 54.38 1.28 1.6871 3 2 2 4 54.42 2.15 1.6861 6 0 1 4 55.05 6.49 1.6683 6 1 1 4 55.61 3.01 1.6527 2 6 1 4 55.89 1.36 1.6450 0 4 2 2 56.55 1.55 1.6274 1 4 2 4 56.72 6.66 1.6231 4 5 1 4 57.15 2.55 1.6116 4 1 2 4 57.48 2.05 1.6032 3 3 2 4 57.54 1.02 1.6017 5 5 0 2 58.40 1.94 1.5803 4 6 0 2 58.50 2.94 1.5778 7 1 0 2 58.50 16.12 1.5778 2 4 2 4 58.53 1.36 1.5771 2 7 0 2 58.87 1.86 1.5688 3 6 1 4 58.97 6.85 1.5662 4 2 2 4 59.19 3.71 1.5611 6 4 0 2 60.29 2.85 1.5351 7 2 0 2 61.52 11.02 1.5074 1 7 1 4 61.66 1.01 1.5043 3 4 2 4 61.69 5.89 1.5037 3 7 0 2 61.93 3.04 1.4984 4 3 2 4 62.43 2.74 1.4874 5 5 1 4 62.85 1.50 1.4786 5 1 2 4 63.34 2.16 1.4683 7 1 1 4 63.37 3.09 1.4677 2 7 1 4 63.78 6.20 1.4592 2 5 2 4 64.00 4.92 1.4547 6 4 1 4 64.02 2.06 1.4543 5 6 0 2 64.44 1.38 1.4460 6 5 0 2 64.57 2.40 1.4433 5 2 2 4 65.06 11.24 1.4337 7 2 1 4 65.40 1.92 1.4269 1 8 0 2 65.93 1.81 1.4167 4 4 2 4 65.96 2.44 1.4162 4 7 0 2 66.80 5.81 1.4005 3 5 2 4 67.20 1.33 1.3931 2 8 0 2 67.38 12.33 1.3897 5 3 2 4 67.58 4.58 1.3861 0 6 2 2 67.86 4.91 1.3811 7 3 1 4 68.18 1.49 1.3755 1 6 2 4 68.65 4.82 1.3671 5 6 1 4 68.89 5.04 1.3629 6 0 2 4 69.05 1.86 1.3602 6 5 1 4 69.38 1.74 1.3546 8 2 0 2 69.44 2.71 1.3535 6 1 2 4 69.94 1.92 1.3451 2 6 2 4 70.56 2.79 1.3347 6 6 0 2 71.08 1.69 1.3263 6 2 2 4 71.23 2.25 1.3238 5 4 2 4 71.26 1.25 1.3234 5 7 0 2 71.57 2.08 1.3184 1 1 3 4 71.69 1.18 1.3165 8 0 1 4 71.70 7.00 1.3164 7 4 1 4 71.72 5.59 1.3160 2 8 1 4 72.23 3.07 1.3080 8 1 1 4 72.83 1.67 1.2987 3 6 2 4 73.19 3.08 1.2932 1 2 3 4 73.29 4.46 1.2916 2 1 3 4 74.71 3.18 1.2706 1 9 0 2 74.89 4.81 1.2679 2 2 3 4 75.00 1.57 1.2664 6 6 1 4 75.60 1.26 1.2578 3 0 3 4 75.67 6.12 1.2567 5 7 1 4 75.84 2.12 1.2544 8 4 0 2 76.13 2.81 1.2504 3 1 3 4 76.80 1.49 1.2411 4 6 2 4 76.89 2.27 1.2399 7 1 2 4 76.91 1.05 1.2396 2 7 2 4 77.49 2.22 1.2318 9 1 0 2 77.49 2.90 1.2318 6 4 2 4 77.54 1.41 1.2311 2 3 3 4 78.47 2.29 1.2189 7 2 2 4 78.53 3.81 1.2181 4 8 1 4 78.98 2.59 1.2123 0 4 3 2 79.06 1.03 1.2112 1 9 1 4 79.54 2.38 1.2052 1 4 3 4 79.71 4.88 1.2030 3 7 2 4 80.05 1.65 1.1987 4 1 3 4 81.28 1.10 1.1837 9 0 1 4 81.61 2.16 1.1797 4 2 3 4 81.80 1.87 1.1775 9 1 1 4 81.82 1.79 1.1772 5 6 2 4 81.82 2.09 1.1772 6 7 1 4 82.19 1.18 1.1728 6 5 2 4 83.08 1.68 1.1626 1 8 2 4 83.09 2.68 1.1624 4 9 0 2 83.50 2.41 1.1578 3 9 1 4 83.52 2.25 1.1575 5 8 1 4 83.59 2.21 1.1568 4 7 2 4 84.20 4.79 1.1499 4 3 3 4 84.21 1.67 1.1498 1 5 3 4 84.51 1.69 1.1465 5 0 3 4 84.65 1.05 1.1449 1 10 0 2 84.73 1.22 1.1441 2 8 2 4 85.86 1.26 1.1319 2 5 3 4 85.93 2.24 1.1311 9 3 1 4 86.76 1.65 1.1224 8 2 2 4 87.34 1.68 1.1164 4 9 1 4 87.87 2.76 1.1111 6 6 2 4 88.35 3.20 1.1063 0 10 1 2 88.53 1.26 1.1045 5 7 2 4 88.60 2.63 1.1038 3 5 3 4 89.14 1.20 1.0985 5 3 3 4 89.33 1.97 1.0967 0 6 3 2 89.88 1.16 1.0914 1 6 3 4 89.93 2.07 1.0909 9 5 0 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.