O49 W18 Lamire M, Labbe P, Goreaud M, Raveau B Revue de Chimie Minerale 24 (1987) 369-381 Refinement et nouvelle analyse de la structure de W18 O49 _cod_database_code 1001678 _database_code_amcsd 0015402 CELL PARAMETERS: 18.3182 3.7828 14.0280 90.000 115.211 90.000 SPACE GROUP: P2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 879.464 Density (g/cm3): 7.727 MAX. ABS. INTENSITY / VOLUME**2: 196.1307801 RIR: 8.265 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.73 4.61 13.1321 -1 0 1 2 6.96 25.97 12.6918 0 0 1 2 10.43 2.77 8.4823 1 0 1 2 10.68 5.56 8.2866 2 0 0 2 13.49 1.42 6.5661 -2 0 2 2 14.51 2.78 6.1057 -3 0 1 2 16.96 2.42 5.2290 1 0 2 2 19.32 2.91 4.5949 -1 0 3 2 19.50 2.54 4.5521 -4 0 1 2 19.99 2.68 4.4419 -4 0 2 2 20.08 2.29 4.4227 3 0 1 2 20.29 1.56 4.3774 -3 0 3 2 22.76 1.37 3.9066 -4 0 3 2 23.52 100.00 3.7828 0 1 0 2 23.82 38.77 3.7355 1 0 3 2 24.43 30.52 3.6430 -5 0 2 2 24.56 2.06 3.6252 0 1 1 4 24.70 1.25 3.6043 -5 0 1 2 25.49 1.31 3.4943 3 0 2 2 25.89 1.03 3.4412 2 1 0 4 26.15 16.98 3.4072 -5 0 3 2 26.25 19.50 3.3948 -1 0 4 2 26.90 1.59 3.3147 5 0 0 2 27.45 4.24 3.2490 2 0 3 2 28.12 8.41 3.1729 0 0 4 2 29.25 3.98 3.0529 -6 0 2 2 29.54 3.91 3.0241 -5 0 4 2 30.04 1.88 2.9752 -6 0 1 2 30.18 6.50 2.9613 -6 0 3 2 30.38 7.35 2.9427 4 0 2 2 30.61 1.49 2.9205 -1 1 3 4 30.64 15.61 2.9176 5 0 1 2 30.73 1.14 2.9094 -4 1 1 4 31.05 1.17 2.8800 -4 1 2 4 31.11 1.13 2.8747 3 1 1 4 31.92 3.92 2.8037 -3 0 5 2 32.18 1.51 2.7814 -2 0 5 2 32.41 8.42 2.7622 6 0 0 2 32.59 12.91 2.7477 -4 0 5 2 32.68 2.21 2.7401 -6 0 4 2 33.72 22.43 2.6580 1 1 3 4 34.17 18.01 2.6240 -5 1 2 4 34.30 1.04 2.6145 2 0 4 2 35.46 10.96 2.5317 -5 1 3 4 35.53 12.48 2.5266 -1 1 4 4 36.03 1.14 2.4930 5 1 0 4 36.45 2.71 2.4647 2 1 3 4 36.98 5.76 2.4310 0 1 4 4 37.87 2.85 2.3757 -6 1 2 4 38.10 2.63 2.3621 -5 1 4 4 38.50 1.31 2.3385 -6 1 1 4 38.61 4.62 2.3318 -6 1 3 4 38.77 5.57 2.3227 4 1 2 4 38.99 11.19 2.3103 5 1 1 4 40.03 2.78 2.2525 -3 1 5 4 40.25 1.23 2.2409 -2 1 5 4 40.43 6.30 2.2308 6 1 0 4 40.58 9.70 2.2231 -4 1 5 4 40.66 1.67 2.2191 -6 1 4 4 45.19 3.53 2.0063 -9 0 4 2 45.48 1.78 1.9943 1 0 6 2 46.29 1.26 1.9614 7 0 2 2 46.73 1.72 1.9438 -9 0 1 2 46.78 3.05 1.9420 -6 0 7 2 47.35 1.87 1.9197 5 0 4 2 48.11 19.03 1.8914 0 2 0 2 48.53 1.47 1.8760 -7 0 7 2 48.76 5.48 1.8678 2 0 6 2 50.33 4.74 1.8131 0 0 7 2 50.87 1.42 1.7949 -8 0 7 2 51.43 6.56 1.7768 -10 0 5 2 51.56 3.59 1.7725 -9 1 4 4 51.82 1.85 1.7641 1 1 6 4 52.37 4.65 1.7472 6 0 4 2 52.55 5.72 1.7414 -10 0 1 2 52.56 1.30 1.7413 7 1 2 4 52.82 2.87 1.7332 -3 0 8 2 52.91 1.34 1.7304 -6 0 8 2 52.96 1.78 1.7289 -9 1 1 4 53.00 3.33 1.7276 -6 1 7 4 53.53 1.88 1.7119 5 1 4 4 53.76 1.48 1.7051 -9 0 7 2 54.37 7.95 1.6874 1 2 3 4 54.61 1.54 1.6807 -7 1 7 4 54.68 6.52 1.6786 -5 2 2 4 54.82 5.79 1.6747 2 1 6 4 55.57 4.13 1.6537 -5 2 3 4 55.63 4.83 1.6523 -1 2 4 4 56.26 5.40 1.6350 0 1 7 4 56.28 1.13 1.6346 2 2 3 4 56.66 2.38 1.6246 0 2 4 4 56.77 1.43 1.6216 -8 1 7 4 57.29 7.38 1.6082 -10 1 5 4 57.30 1.20 1.6078 -6 2 2 4 57.47 1.17 1.6036 -5 2 4 4 57.65 1.99 1.5990 7 0 4 2 57.85 2.13 1.5940 -6 2 3 4 57.96 2.44 1.5911 4 2 2 4 58.12 5.10 1.5871 5 2 1 4 58.16 5.25 1.5861 6 1 4 4 58.33 6.44 1.5818 -10 1 1 4 58.41 1.38 1.5799 -9 0 8 2 58.58 3.01 1.5757 -3 1 8 4 58.67 1.47 1.5736 -6 1 8 4 58.90 1.36 1.5680 -3 2 5 4 59.21 3.14 1.5606 6 2 0 4 59.29 1.21 1.5587 -5 0 9 2 59.32 4.91 1.5580 -4 2 5 4 59.46 1.61 1.5545 -9 1 7 4 60.44 1.38 1.5316 -3 0 9 2 63.06 1.21 1.4742 9 0 3 2 63.13 2.38 1.4728 7 1 4 4 63.85 1.72 1.4579 -9 1 8 4 64.68 1.48 1.4411 -5 1 9 4 65.41 1.33 1.4267 11 0 1 2 65.78 1.79 1.4197 -3 1 9 4 68.13 1.87 1.3763 -9 2 4 4 68.28 1.52 1.3736 9 1 3 4 69.36 1.79 1.3550 -6 2 7 4 69.81 1.09 1.3473 5 2 4 4 70.55 1.59 1.3349 11 1 1 4 70.91 3.27 1.3290 2 2 6 4 72.17 3.03 1.3089 0 2 7 4 72.30 1.07 1.3068 -7 1 10 4 73.07 4.26 1.2950 -10 2 5 4 73.84 3.17 1.2834 6 2 4 4 73.99 3.91 1.2811 -10 2 1 4 74.21 1.95 1.2778 -3 2 8 4 74.99 1.02 1.2665 -9 2 7 4 75.30 1.08 1.2621 -8 0 11 2 75.38 3.67 1.2609 0 3 0 2 78.30 1.55 1.2211 7 2 4 4 78.63 1.61 1.2167 -15 0 4 2 78.96 1.13 1.2126 -9 2 8 4 80.17 1.51 1.1972 -8 1 11 4 80.37 1.99 1.1947 1 3 3 4 80.63 1.63 1.1916 -5 3 2 4 80.73 1.16 1.1903 -3 2 9 4 80.99 1.07 1.1871 -13 0 10 2 81.36 1.27 1.1827 3 1 9 4 81.37 1.08 1.1826 -5 3 3 4 81.42 1.26 1.1820 -1 3 4 4 81.45 1.18 1.1817 12 1 2 4 81.72 1.16 1.1783 5 1 8 4 82.73 1.01 1.1666 1 1 10 4 83.06 1.07 1.1627 9 2 3 4 83.45 1.11 1.1583 -15 -1 4 4 83.52 1.43 1.1575 5 3 1 4 83.53 1.03 1.1574 -2 1 11 4 84.55 1.47 1.1460 -4 3 5 4 85.19 1.23 1.1390 11 2 1 4 85.78 1.49 1.1327 -13 1 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.