Deloryite Tali R, Tabachenko V V, Kovba L M Russian Journal of Inorganic Chemistry 38 (1993) 1350-1352 Crystal structure of Cu4UO2(MoO4)2(OH)6 Locality: synthetic _database_code_amcsd 0018337 CELL PARAMETERS: 19.8392 5.5108 6.1009 90.000 90.000 104.477 SPACE GROUP: B2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 645.832 Density (g/cm3): 4.834 MAX. ABS. INTENSITY / VOLUME**2: 45.27732581 RIR: 3.050 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.21 3.42 9.6046 2 0 0 2 15.24 2.32 5.8147 1 0 1 4 16.61 17.97 5.3358 0 1 0 2 18.48 89.77 4.8023 4 0 0 2 20.10 32.16 4.4170 3 0 1 4 20.97 46.52 4.2364 2 1 0 2 21.58 1.43 4.1179 -4 1 0 2 21.74 98.46 4.0885 1 -1 1 4 23.47 20.50 3.7911 1 1 1 4 23.83 100.00 3.7334 3 -1 1 4 27.44 52.15 3.2510 5 0 1 4 27.87 13.87 3.2015 6 0 0 2 27.93 27.75 3.1944 4 1 0 2 28.71 12.94 3.1096 -6 1 0 2 28.98 23.51 3.0809 5 -1 1 4 29.28 26.28 3.0505 0 0 2 2 30.75 30.77 2.9073 2 0 2 4 32.51 1.14 2.7543 -2 2 0 2 33.59 3.50 2.6679 0 2 0 2 33.85 4.33 2.6482 0 1 2 4 33.98 10.68 2.6382 2 -1 2 4 34.12 36.34 2.6277 -4 2 0 2 34.84 2.75 2.5749 4 0 2 4 35.23 2.38 2.5471 5 1 1 4 35.88 21.22 2.5027 7 0 1 4 35.96 13.39 2.4975 -1 2 1 4 36.00 1.33 2.4950 7 -1 1 4 36.15 5.18 2.4849 6 1 0 2 36.21 2.36 2.4808 3 -2 1 4 36.29 51.74 2.4755 2 1 2 4 37.02 9.82 2.4286 -8 1 0 2 37.45 2.26 2.4012 8 0 0 2 38.16 25.03 2.3582 1 2 1 4 41.47 35.60 2.1776 6 -1 2 4 42.50 9.39 2.1271 3 2 1 4 42.69 13.48 2.1182 4 2 0 2 43.29 5.23 2.0900 7 1 1 4 43.58 2.81 2.0768 7 -2 1 4 43.98 19.99 2.0590 -8 2 0 2 44.31 4.87 2.0443 2 -2 2 4 45.00 8.01 2.0146 9 0 1 4 45.56 16.53 1.9909 4 -2 2 4 46.04 8.08 1.9712 -10 1 0 2 46.87 3.71 1.9382 3 0 3 4 47.18 31.55 1.9266 6 1 2 4 47.67 10.83 1.9078 1 -1 3 4 47.88 3.10 1.9000 8 -1 2 4 48.50 1.58 1.8768 5 2 1 4 48.56 3.08 1.8748 1 1 3 4 48.76 13.42 1.8677 3 -1 3 4 48.79 10.11 1.8667 6 -2 2 4 49.65 1.46 1.8362 6 2 0 2 49.75 4.49 1.8328 -2 3 0 2 49.87 7.97 1.8286 9 -2 1 4 50.04 2.41 1.8229 -4 3 0 2 50.80 8.72 1.7974 5 0 3 4 51.18 1.02 1.7847 -10 2 0 2 51.37 4.05 1.7786 0 3 0 2 51.73 4.50 1.7670 5 -1 3 4 52.18 8.92 1.7530 9 1 1 4 52.60 2.54 1.7399 4 2 2 4 53.22 2.54 1.7212 5 -3 1 4 53.71 2.41 1.7066 8 -2 2 4 54.79 1.05 1.6755 2 3 0 2 55.13 1.79 1.6659 1 3 1 4 55.50 20.09 1.6556 10 -1 2 4 55.67 1.21 1.6511 -12 1 0 2 56.20 6.96 1.6366 7 -3 1 4 56.31 5.84 1.6339 7 0 3 4 56.36 3.74 1.6325 -1 2 3 4 56.62 2.86 1.6255 10 0 2 4 57.39 6.73 1.6055 11 -2 1 4 57.58 8.17 1.6008 12 0 0 2 57.72 11.03 1.5972 8 2 0 2 57.94 6.87 1.5916 1 2 3 4 58.69 4.94 1.5732 6 2 2 4 58.77 25.91 1.5711 -2 3 2 4 59.26 5.23 1.5593 3 3 1 4 59.45 2.70 1.5548 -12 2 0 2 60.72 13.11 1.5252 0 0 4 2 60.79 4.50 1.5236 9 -3 1 4 60.99 4.11 1.5191 6 -3 2 4 61.20 3.16 1.5145 3 2 3 4 61.79 5.99 1.5015 11 1 1 4 61.81 1.80 1.5010 7 1 3 4 62.79 3.53 1.4799 13 -1 1 4 63.15 2.57 1.4723 9 0 3 4 63.23 4.74 1.4706 10 1 2 4 63.33 7.88 1.4685 2 3 2 4 64.05 5.14 1.4537 4 0 4 4 64.56 1.52 1.4435 8 -3 2 4 64.86 4.65 1.4375 5 3 1 4 64.99 3.63 1.4351 2 1 4 4 65.90 5.12 1.4175 12 0 2 4 65.96 3.35 1.4163 13 -2 1 4 66.03 4.98 1.4150 8 2 2 4 66.80 1.58 1.4004 11 -3 1 4 67.11 3.01 1.3948 9 -2 3 4 68.09 1.26 1.3770 6 0 4 4 68.13 3.97 1.3764 4 1 4 4 68.34 1.40 1.3726 -12 3 0 2 68.52 1.88 1.3694 6 -1 4 4 69.04 3.52 1.3604 9 1 3 4 69.61 2.26 1.3506 10 -3 2 4 69.92 1.13 1.3454 5 -3 3 4 70.08 4.14 1.3427 -3 4 1 4 70.40 3.19 1.3375 5 -4 1 4 70.61 3.13 1.3340 0 4 0 2 71.21 1.03 1.3241 0 2 4 4 71.33 2.07 1.3222 -1 4 1 4 71.52 7.42 1.3191 4 -2 4 4 71.78 2.59 1.3151 7 3 1 4 71.86 2.97 1.3138 -8 4 0 2 72.50 3.22 1.3038 7 -3 3 4 72.75 1.38 1.2999 6 1 4 4 73.23 3.65 1.2925 15 -1 1 4 73.29 2.57 1.2916 8 -1 4 4 73.52 1.85 1.2882 11 2 1 4 73.54 3.10 1.2879 11 -2 3 4 73.72 1.74 1.2852 14 -1 2 4 74.50 1.94 1.2736 10 2 2 4 75.19 2.45 1.2637 3 3 3 4 75.78 1.20 1.2553 14 1 0 2 75.92 1.02 1.2533 15 0 1 4 76.06 1.48 1.2513 14 0 2 4 76.32 1.59 1.2477 -14 3 0 2 76.56 2.12 1.2445 9 -3 3 4 77.05 3.66 1.2377 4 2 4 4 77.45 2.94 1.2323 11 1 3 4 77.96 5.40 1.2256 8 -2 4 4 78.21 1.50 1.2222 0 4 2 4 78.36 1.82 1.2203 13 -1 3 4 78.82 2.36 1.2143 -16 2 0 2 79.18 2.82 1.2097 4 4 0 2 79.42 1.55 1.2067 8 -4 2 4 79.45 2.67 1.2063 10 -1 4 4 79.90 1.76 1.2006 16 0 0 2 80.25 2.41 1.1962 5 3 3 4 80.65 2.10 1.1913 1 -1 5 4 81.26 1.75 1.1839 13 -2 3 4 81.47 2.55 1.1813 3 -1 5 4 81.58 2.31 1.1801 -12 4 0 2 81.66 2.93 1.1791 2 4 2 4 82.23 1.96 1.1724 -2 3 4 4 82.45 1.04 1.1698 4 -3 4 4 82.64 1.07 1.1676 10 3 0 2 83.04 2.03 1.1629 5 0 5 4 83.22 3.94 1.1609 14 1 2 4 83.45 1.81 1.1583 10 -4 2 4 83.49 1.82 1.1578 0 3 4 4 83.76 5.33 1.1548 14 -3 2 4 83.78 1.04 1.1546 5 -1 5 4 83.92 2.14 1.1530 13 2 1 4 84.61 1.25 1.1454 17 -1 1 4 85.11 2.37 1.1399 -3 4 3 4 85.41 1.83 1.1367 5 -4 3 4 86.21 1.83 1.1282 16 -2 2 4 86.30 1.14 1.1272 -1 4 3 4 86.56 1.22 1.1245 4 4 2 4 86.72 1.51 1.1229 7 3 3 4 87.49 1.57 1.1149 7 0 5 4 87.53 1.02 1.1145 -1 2 5 4 87.87 1.29 1.1111 17 0 1 4 88.11 2.20 1.1087 15 -1 3 4 88.38 1.10 1.1060 11 2 3 4 88.56 4.32 1.1042 12 0 4 4 88.68 5.47 1.1031 8 2 4 4 88.86 1.95 1.1012 1 2 5 4 88.93 1.91 1.1006 12 -4 2 4 89.97 3.42 1.0905 10 3 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.