Ammonioborite Merlino S, Sartori F Science 171 (1971) 377-379 Ammonioborite: New borate polyion and its structure _database_code_amcsd 0015421 CELL PARAMETERS: 25.2700 9.6500 11.5600 90.000 94.280 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2811.108 Density (g/cm3): 1.731 MAX. ABS. INTENSITY / VOLUME**2: 2.683072812 RIR: 0.505 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.02 17.35 12.5998 2 0 0 2 9.81 37.47 9.0118 1 1 0 4 12.63 2.04 7.0096 1 1 1 4 13.98 5.41 6.3358 3 1 0 4 14.06 9.26 6.2999 4 0 0 2 15.37 11.92 5.7639 0 0 2 2 15.58 100.00 5.6893 -3 1 1 4 16.34 41.50 5.4250 3 1 1 4 16.43 2.15 5.3960 -2 0 2 2 17.39 5.46 5.0995 2 0 2 2 18.39 24.55 4.8250 0 2 0 2 18.49 5.72 4.7979 1 1 2 4 19.87 1.59 4.4673 5 1 0 4 20.09 1.64 4.4200 -4 0 2 2 20.24 17.98 4.3883 -3 1 2 4 20.98 3.47 4.2352 -2 2 1 4 21.15 16.44 4.1999 6 0 0 2 21.36 9.13 4.1592 2 2 1 4 21.42 2.92 4.1489 3 1 2 4 21.66 3.11 4.1028 4 0 2 2 21.81 4.64 4.0756 5 1 1 4 24.15 6.60 3.6855 -4 2 1 4 24.75 3.92 3.5968 -2 2 2 4 24.82 13.13 3.5868 4 2 1 4 25.41 1.98 3.5048 2 2 2 4 25.44 2.28 3.5011 1 1 3 4 26.03 1.79 3.4230 5 1 2 4 26.43 11.06 3.3729 7 1 0 4 26.44 3.34 3.3708 -3 1 3 4 27.02 4.55 3.2999 -7 1 1 4 27.36 7.51 3.2592 -4 2 2 4 27.82 2.01 3.2065 3 1 3 4 27.96 1.36 3.1908 1 3 0 4 28.17 86.03 3.1679 6 2 0 4 28.56 4.51 3.1256 4 2 2 4 28.80 88.43 3.0996 -6 2 1 4 28.96 5.44 3.0826 -1 3 1 4 29.11 1.27 3.0677 1 3 1 4 29.66 33.91 3.0116 6 2 1 4 29.72 3.80 3.0058 0 2 3 4 29.74 1.29 3.0041 -7 1 2 4 30.96 4.75 2.8881 3 3 1 4 31.03 43.10 2.8819 0 0 4 2 31.32 1.49 2.8561 -2 0 4 2 31.45 4.55 2.8446 -6 2 2 4 31.66 13.59 2.8262 7 1 2 4 32.19 4.55 2.7805 1 3 2 4 32.24 2.23 2.7766 -4 2 3 4 32.36 1.86 2.7665 -1 1 4 4 32.38 1.65 2.7649 2 0 4 2 33.26 1.72 2.6935 -3 3 2 4 33.32 3.63 2.6890 9 1 0 4 33.65 7.65 2.6634 -5 3 1 4 33.99 7.39 2.6376 8 2 0 4 34.02 1.63 2.6352 3 3 2 4 34.12 1.63 2.6276 -7 1 3 4 34.40 1.11 2.6068 -8 2 1 4 35.63 2.80 2.5200 10 0 0 2 35.70 1.34 2.5148 -6 2 3 4 36.04 1.86 2.4924 -5 3 2 4 36.43 3.61 2.4663 -1 3 3 4 36.78 2.58 2.4435 1 3 3 4 37.27 1.64 2.4125 0 4 0 2 37.50 2.12 2.3986 7 3 0 4 37.81 1.12 2.3795 6 2 3 4 37.92 1.87 2.3726 9 1 2 4 37.97 4.33 2.3695 2 4 0 4 38.11 2.70 2.3613 0 4 1 4 38.22 1.25 2.3549 -4 2 4 4 38.72 13.93 2.3254 7 3 1 4 38.91 1.21 2.3145 2 4 1 4 39.69 6.42 2.2709 -7 1 4 4 39.99 4.51 2.2546 -7 3 2 4 40.67 1.52 2.2186 -11 1 1 4 41.02 2.37 2.2001 4 4 1 4 41.14 6.51 2.1941 -6 2 4 4 41.49 6.29 2.1765 7 3 2 4 41.69 4.15 2.1663 10 2 1 4 42.05 1.11 2.1488 -1 3 4 4 42.42 1.32 2.1308 -10 2 2 4 42.46 1.13 2.1287 1 3 4 4 42.47 4.24 2.1284 3 1 5 4 42.67 2.44 2.1191 7 1 4 4 42.70 1.71 2.1176 -4 4 2 4 42.90 1.06 2.1079 -3 3 4 4 43.08 1.72 2.1000 12 0 0 2 43.52 6.48 2.0796 4 4 2 4 43.63 5.16 2.0744 6 2 4 4 44.12 1.32 2.0524 3 3 4 4 44.29 1.12 2.0450 6 4 1 4 44.46 3.82 2.0378 10 2 2 4 44.64 1.26 2.0299 11 1 2 4 44.65 2.04 2.0296 -2 4 3 4 44.87 2.14 2.0201 -9 3 2 4 45.61 9.22 1.9891 -10 2 3 4 46.16 4.84 1.9666 -4 4 3 4 46.91 1.66 1.9369 4 2 5 4 47.31 1.90 1.9213 0 0 6 2 47.31 3.55 1.9213 4 4 3 4 47.33 1.12 1.9208 -2 0 6 2 47.45 10.64 1.9162 -6 2 5 4 47.88 2.48 1.8999 -1 5 1 4 47.89 2.24 1.8994 9 1 4 4 47.97 2.32 1.8963 1 5 1 4 48.20 4.78 1.8879 8 2 4 4 48.46 1.53 1.8786 2 0 6 2 48.48 1.21 1.8779 10 2 3 4 49.15 2.53 1.8535 13 1 1 4 49.98 4.01 1.8249 -10 2 4 4 50.24 1.75 1.8161 6 2 5 4 50.54 1.48 1.8058 3 3 5 4 50.71 1.49 1.8001 7 3 4 4 50.77 3.15 1.7984 -4 4 4 4 50.95 2.77 1.7923 -5 3 5 4 53.59 2.97 1.7101 10 4 1 4 58.25 2.70 1.5839 12 4 0 4 58.36 1.54 1.5813 -12 4 1 4 59.34 1.06 1.5574 12 4 1 4 62.88 1.05 1.4779 14 0 4 2 63.33 1.09 1.4685 2 6 3 4 65.37 1.87 1.4276 -16 0 4 2 68.68 1.76 1.3666 -13 5 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.