data_global _chemical_name_mineral 'Jamesonite' loop_ _publ_author_name 'Leone P' 'Le Leuch L M' 'Palvadeau P' 'Molinie P' 'Moelo Y' _journal_name_full 'Solid State Sciences' _journal_volume 5 _journal_year 2003 _journal_page_first 771 _journal_page_last 776 _publ_section_title ; Single crystal structures and magnetic properties of two iron or manganese-lead-antimony sulfides: MPb4Sb6S14 (M: Fe, Mn) ; _database_code_amcsd 0015519 _chemical_compound_source 'Siberia' _chemical_formula_sum 'Pb4 Sb6 Fe S14' _cell_length_a 4.0235 _cell_length_b 19.074 _cell_length_c 15.737 _cell_angle_alpha 90 _cell_angle_beta 91.89 _cell_angle_gamma 90 _cell_volume 1207.067 _exptl_crystal_density_diffrn 5.679 _symmetry_space_group_name_H-M 'P 1 21/c 1' loop_ _space_group_symop_operation_xyz 'x,y,z' 'x,1/2-y,1/2+z' '-x,1/2+y,1/2-z' '-x,-y,-z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv Pb1 0.44150 0.23983 0.57470 0.03490 Pb2 0.46380 0.14056 0.81770 0.03760 Sb1 0.88190 0.04877 0.60418 0.03250 Sb2 0.91090 0.93675 0.81978 0.03150 Sb3 0.88140 0.15908 0.36996 0.03730 Fe 0.50000 0.00000 0.00000 0.03590 S1 0.45480 0.10210 0.49700 0.03150 S2 0.94920 0.15910 0.68260 0.02930 S3 0.97670 0.04370 0.90420 0.02590 S4 0.93010 0.26910 0.44790 0.02930 S5 0.46900 0.00380 0.71410 0.02950 S6 0.42300 0.29640 0.77570 0.03420 S7 0.51260 0.39370 0.58120 0.03230 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pb1 0.03540 0.03280 0.03640 0.00050 -0.00010 0.00050 Pb2 0.03520 0.04370 0.03400 -0.00060 -0.00030 0.00330 Sb1 0.04200 0.02800 0.02770 -0.00260 0.00300 0.00120 Sb2 0.03740 0.02880 0.02880 -0.00200 0.00720 -0.00350 Sb3 0.04800 0.03040 0.03290 -0.01020 -0.00920 0.00550 Fe 0.05300 0.02500 0.03000 -0.00500 0.00900 -0.00400