Jamesonite Leone P, Le Leuch L M, Palvadeau P, Molinie P, Moelo Y Solid State Sciences 5 (2003) 771-776 Single crystal structures and magnetic properties of two iron or manganese-lead-antimony sulfides: MPb4Sb6S14 (M: Fe, Mn) Locality: Siberia _database_code_amcsd 0015519 CELL PARAMETERS: 4.0235 19.0740 15.7370 90.000 91.890 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1207.067 Density (g/cm3): 5.678 MAX. ABS. INTENSITY / VOLUME**2: 55.69454310 RIR: 3.194 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.27 7.79 9.5370 0 2 0 2 10.85 17.54 8.1550 0 2 1 4 11.25 1.22 7.8642 0 0 2 2 14.60 9.76 6.0674 0 2 2 4 15.03 3.96 5.8946 0 3 1 4 17.54 8.22 5.0553 0 1 3 4 19.45 1.85 4.5634 0 4 1 4 21.80 31.35 4.0775 0 4 2 4 21.97 2.83 4.0450 0 3 3 4 22.10 7.28 4.0213 1 0 0 2 22.61 16.38 3.9321 0 0 4 2 23.09 41.82 3.8511 0 1 4 4 23.12 1.05 3.8465 -1 1 1 4 23.48 9.06 3.7885 1 1 1 4 24.00 3.18 3.7073 0 5 1 4 24.02 29.20 3.7054 1 2 0 4 24.51 4.31 3.6314 -1 2 1 4 24.85 37.47 3.5824 1 2 1 4 24.98 1.24 3.5653 -1 1 2 4 25.20 2.42 3.5335 1 0 2 2 25.25 7.68 3.5276 0 4 3 4 25.64 2.62 3.4743 1 1 2 4 25.96 100.00 3.4323 0 5 2 4 26.22 1.27 3.3986 1 3 0 4 26.27 2.80 3.3919 -1 2 2 4 26.66 5.96 3.3442 0 3 4 4 26.68 12.28 3.3412 -1 3 1 4 26.91 5.23 3.3134 1 2 2 4 27.91 3.89 3.1970 -1 1 3 4 28.32 43.06 3.1519 -1 3 2 4 28.65 2.39 3.1160 0 6 1 4 28.76 16.84 3.1038 0 1 5 4 28.91 13.73 3.0885 1 3 2 4 28.95 14.71 3.0846 0 5 3 4 29.08 2.34 3.0702 -1 2 3 4 29.46 3.22 3.0315 -1 4 1 4 29.95 16.03 2.9835 1 2 3 4 30.33 11.91 2.9473 0 6 2 4 30.96 11.68 2.8888 -1 3 3 4 30.96 1.85 2.8879 -1 4 2 4 31.29 3.46 2.8590 -1 0 4 2 31.51 4.29 2.8390 1 4 2 4 31.65 53.11 2.8274 -1 1 4 4 31.74 1.62 2.8195 0 3 5 4 31.77 41.17 2.8162 1 3 3 4 32.35 1.09 2.7676 1 5 0 4 32.36 5.39 2.7662 1 0 4 2 32.70 21.40 2.7386 -1 2 4 4 32.71 1.60 2.7380 0 5 4 4 32.71 24.31 2.7376 1 1 4 4 32.95 25.39 2.7183 0 6 3 4 33.37 1.45 2.6849 0 7 1 4 33.42 7.72 2.6815 -1 4 3 4 34.10 1.39 2.6294 -1 5 2 4 34.18 10.79 2.6232 1 4 3 4 34.60 2.27 2.5923 1 5 2 4 34.85 1.74 2.5747 0 7 2 4 35.39 1.65 2.5365 1 3 4 4 35.52 3.96 2.5277 0 2 6 4 36.36 3.67 2.4709 -1 6 1 4 36.36 1.11 2.4708 -1 5 3 4 36.60 2.30 2.4553 1 6 1 4 36.92 4.96 2.4348 -1 2 5 4 37.61 4.25 2.3913 -1 6 2 4 37.73 1.41 2.3842 0 8 0 2 38.08 6.21 2.3633 1 6 2 4 38.08 5.42 2.3629 1 2 5 4 38.18 1.83 2.3573 0 8 1 4 39.22 17.42 2.2972 0 4 6 4 39.49 1.44 2.2817 0 8 2 4 39.58 7.70 2.2771 1 3 5 4 39.97 2.76 2.2558 1 7 0 4 40.27 4.52 2.2397 0 7 4 4 40.28 18.24 2.2387 -1 7 1 4 40.34 2.87 2.2360 0 6 5 4 40.74 1.41 2.2148 -1 1 6 4 41.28 1.46 2.1870 0 2 7 4 41.44 5.86 2.1790 -1 7 2 4 41.59 1.13 2.1714 -1 2 6 4 41.61 1.84 2.1704 0 8 3 4 41.87 1.25 2.1578 1 7 2 4 42.53 1.28 2.1258 -1 6 4 4 42.68 1.70 2.1185 0 3 7 4 42.86 6.42 2.1100 1 2 6 4 43.36 1.40 2.0868 1 6 4 4 43.37 4.64 2.0862 -1 7 3 4 43.99 5.59 2.0583 1 7 3 4 44.16 22.02 2.0509 1 8 0 4 44.22 7.75 2.0483 1 3 6 4 44.58 11.57 2.0326 0 4 7 4 44.65 4.97 2.0293 1 8 1 4 44.81 5.53 2.0225 0 6 6 4 44.87 8.75 2.0200 -1 4 6 4 45.09 12.09 2.0107 2 0 0 2 45.35 8.68 1.9996 2 1 0 4 45.54 4.88 1.9918 -2 1 1 4 45.98 1.23 1.9740 -1 6 5 4 46.17 2.89 1.9661 0 0 8 2 46.32 5.32 1.9600 -2 2 1 4 46.43 2.04 1.9557 0 1 8 4 46.63 2.48 1.9477 -1 2 7 4 46.80 5.85 1.9412 1 7 4 4 46.93 1.85 1.9360 0 5 7 4 47.20 1.91 1.9256 0 2 8 4 47.21 5.55 1.9251 -1 5 6 4 47.68 7.92 1.9074 0 10 0 2 47.90 2.56 1.8991 1 8 3 4 47.99 5.32 1.8959 1 2 7 4 48.05 4.16 1.8935 0 10 1 4 48.36 3.11 1.8820 1 5 6 4 48.82 6.69 1.8656 0 9 4 4 49.02 2.76 1.8584 1 9 1 4 49.30 1.12 1.8482 2 1 3 4 49.65 4.03 1.8362 -1 4 7 4 49.69 7.47 1.8349 0 6 7 4 49.73 1.36 1.8335 2 4 1 4 49.80 4.63 1.8311 -1 8 4 4 49.96 8.21 1.8256 -1 6 6 4 50.15 2.79 1.8190 -2 3 3 4 50.20 4.96 1.8173 1 7 5 4 50.28 3.41 1.8146 -2 0 4 2 50.98 8.44 1.7912 2 4 2 4 51.03 2.56 1.7897 -1 0 8 2 51.27 3.17 1.7819 -1 1 8 4 51.74 1.81 1.7667 2 0 4 2 51.83 2.19 1.7641 -1 5 7 4 51.98 5.57 1.7592 2 1 4 4 52.03 1.74 1.7576 0 9 5 4 52.41 9.33 1.7459 -2 5 2 4 52.59 3.28 1.7403 0 1 9 4 53.08 1.95 1.7253 1 5 7 4 53.29 2.11 1.7190 0 2 9 4 53.39 5.42 1.7161 0 10 4 4 53.42 3.52 1.7153 1 2 8 4 53.77 1.40 1.7049 1 8 5 4 53.85 3.47 1.7026 -1 9 4 4 53.95 1.61 1.6996 -2 5 3 4 54.13 1.41 1.6944 1 7 6 4 54.18 1.20 1.6928 -2 2 5 4 54.47 2.23 1.6845 2 6 1 4 54.55 2.30 1.6823 1 9 4 4 54.91 1.54 1.6721 0 6 8 4 55.33 1.09 1.6604 -2 3 5 4 55.65 4.09 1.6515 2 6 2 4 55.84 1.36 1.6463 0 11 3 4 56.05 1.50 1.6409 0 4 9 4 57.41 1.17 1.6051 2 7 1 4 57.47 3.66 1.6034 2 6 3 4 57.67 2.04 1.5985 -2 2 6 4 58.57 1.13 1.5759 -2 6 4 4 58.70 1.13 1.5728 0 0 10 2 58.92 1.56 1.5675 0 1 10 4 59.33 1.77 1.5576 -2 7 3 4 59.57 1.19 1.5519 0 2 10 4 60.21 1.46 1.5371 2 8 0 4 60.29 1.45 1.5351 -2 4 6 4 60.55 1.62 1.5291 -1 11 3 4 61.02 3.36 1.5186 0 11 5 4 61.09 1.08 1.5169 0 8 8 4 61.38 2.35 1.5104 -2 7 4 4 61.65 1.03 1.5044 -2 2 7 4 62.21 1.51 1.4922 -2 5 6 4 62.23 1.99 1.4918 2 4 6 4 62.66 1.81 1.4826 -1 11 4 4 63.10 1.12 1.4734 -1 12 1 4 63.26 2.44 1.4701 1 12 1 4 63.81 1.96 1.4587 2 9 0 4 64.03 1.43 1.4541 0 5 10 4 64.12 5.13 1.4523 2 5 6 4 64.26 2.61 1.4496 1 12 2 4 64.60 1.50 1.4428 -1 3 10 4 64.93 1.06 1.4363 2 3 7 4 65.46 1.17 1.4259 0 1 11 4 66.16 2.12 1.4125 1 3 10 4 66.39 1.96 1.4081 2 6 6 4 66.42 2.60 1.4075 1 8 8 4 67.11 1.48 1.3947 -2 3 8 4 67.75 2.36 1.3831 2 0 8 2 67.87 3.06 1.3810 -1 5 10 4 68.27 1.60 1.3739 -2 6 7 4 68.54 1.08 1.3690 0 10 8 4 69.05 3.53 1.3603 -1 13 2 4 69.23 2.32 1.3570 2 9 4 4 69.39 1.07 1.3543 1 5 10 4 70.10 1.38 1.3424 0 14 2 4 70.22 1.17 1.3404 3 0 0 2 70.38 1.46 1.3378 -2 1 9 4 71.58 1.14 1.3182 1 6 10 4 71.80 2.22 1.3147 -2 10 4 4 72.41 1.47 1.3051 -1 10 8 4 74.00 1.05 1.2810 1 12 6 4 74.28 1.44 1.2769 3 2 3 4 74.73 1.75 1.2703 -3 2 4 4 74.93 1.48 1.2674 2 11 3 4 75.04 1.43 1.2659 -2 7 8 4 75.78 1.22 1.2553 0 15 2 4 75.82 1.36 1.2547 -3 5 2 4 77.50 1.98 1.2317 1 1 12 4 79.18 1.13 1.2096 2 2 10 4 79.24 1.33 1.2089 0 14 6 4 79.79 1.23 1.2020 -3 7 1 4 82.21 1.05 1.1726 -3 4 6 4 83.47 1.49 1.1581 3 3 6 4 86.60 1.03 1.1241 -1 14 7 4 87.02 1.51 1.1197 2 10 8 4 87.62 1.20 1.1136 2 14 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.