Froodite Zhuravlev N N Soviet Journal of Experimental and Theoretical Physics 5 (1957) 1064-1072 Structure of superconductors. X. Thermal, microscopic and x-ray investigation of the bismuth-palladium system Locality: synthetic Note: low temperature modification Note: unable to reproduce reported bond lengths _database_code_amcsd 0015531 CELL PARAMETERS: 12.7400 4.2500 5.6650 90.000 102.580 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 299.368 Density (g/cm3): 11.633 MAX. ABS. INTENSITY / VOLUME**2: 273.6334916 RIR: 7.659 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.25 11.37 6.2171 2 0 0 2 22.10 4.64 4.0216 1 1 0 4 23.75 1.27 3.7462 2 0 1 2 26.47 2.76 3.3670 -1 1 1 4 28.35 53.67 3.1485 1 1 1 4 28.72 6.81 3.1085 4 0 0 2 29.75 12.81 3.0035 -4 0 1 2 30.12 62.67 2.9673 3 1 0 4 31.93 100.00 2.8030 -3 1 1 4 32.38 45.89 2.7645 0 0 2 2 32.45 20.15 2.7589 -2 0 2 2 36.10 28.39 2.4880 4 0 1 2 36.53 32.94 2.4596 3 1 1 4 38.18 3.77 2.3570 -1 1 2 4 38.41 16.18 2.3436 2 0 2 2 38.58 4.26 2.3335 -4 0 2 2 40.89 18.75 2.2067 1 1 2 4 41.00 37.89 2.2011 -3 1 2 4 42.10 21.46 2.1464 5 1 0 4 42.20 1.17 2.1413 -5 1 1 4 42.54 40.56 2.1250 0 2 0 2 43.15 19.73 2.0964 -6 0 1 2 45.09 1.03 2.0108 2 2 0 4 48.28 6.29 1.8849 5 1 1 4 52.14 2.43 1.7543 4 2 0 4 52.77 4.75 1.7347 -4 2 1 4 53.19 3.76 1.7220 -1 1 3 4 54.35 11.65 1.6880 -3 1 3 4 54.46 18.38 1.6848 0 2 2 4 54.51 8.28 1.6835 -2 2 2 4 54.96 1.25 1.6706 2 0 3 2 56.12 9.43 1.6389 7 1 0 4 56.36 11.35 1.6325 1 1 3 4 56.99 13.41 1.6159 4 2 1 4 58.04 7.38 1.5892 -8 0 1 2 58.64 8.13 1.5742 2 2 2 4 58.77 2.20 1.5712 -4 2 2 4 59.26 13.72 1.5593 5 1 2 4 59.41 11.22 1.5557 -6 0 3 2 59.51 8.05 1.5534 -7 1 2 4 59.67 2.94 1.5496 -5 1 3 4 62.20 11.54 1.4924 -6 2 1 4 62.23 2.35 1.4918 7 1 1 4 64.11 3.88 1.4526 4 0 3 2 65.87 6.40 1.4180 8 0 1 2 65.96 7.10 1.4162 -2 0 4 2 69.29 3.40 1.3561 1 3 1 4 70.21 4.23 1.3405 3 3 0 4 70.53 2.20 1.3352 -3 1 4 4 71.20 7.53 1.3243 -3 3 1 4 72.75 1.07 1.2999 7 1 2 4 73.05 2.80 1.2952 -9 1 2 4 73.33 1.96 1.2910 2 0 4 2 73.91 3.15 1.2823 3 3 1 4 74.08 3.75 1.2798 1 1 4 4 74.31 2.01 1.2765 -5 1 4 4 74.57 6.13 1.2726 -8 2 1 4 75.78 9.58 1.2553 -6 2 3 4 76.25 2.17 1.2487 6 0 3 2 76.73 2.23 1.2420 1 3 2 4 76.81 4.53 1.2410 -3 3 2 4 77.55 2.70 1.2309 5 3 0 4 78.18 2.15 1.2226 9 1 1 4 80.01 3.63 1.1992 4 2 3 4 80.51 1.83 1.1930 -9 1 3 4 81.23 2.69 1.1843 3 1 4 4 81.63 6.18 1.1795 8 2 1 4 81.71 6.86 1.1785 -2 2 4 4 82.01 1.02 1.1750 5 3 1 4 83.85 1.18 1.1538 -10 0 3 2 86.77 2.39 1.1223 -3 3 3 4 87.25 4.73 1.1173 -11 1 1 4 88.22 2.06 1.1076 7 3 0 4 88.42 2.50 1.1056 1 3 3 4 88.64 2.16 1.1034 2 2 4 4 89.19 1.45 1.0980 -11 1 2 4 89.77 1.68 1.0924 11 1 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.