Solongoite Yamnova N A, Simonov M A, Belov N V Soviet Physics Crystallography 22 (1977) 356-357 Refined crystal structure of solongoite Ca2[B3O4(OH)4]Cl _database_code_amcsd 0015575 CELL PARAMETERS: 7.9750 12.5710 7.2370 90.000 90.000 86.140 SPACE GROUP: P2_1/b X-RAY WAVELENGTH: 1.541838 Cell Volume: 723.890 Density (g/cm3): 2.569 MAX. ABS. INTENSITY / VOLUME**2: 3.291930060 RIR: 0.417 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.12 18.01 7.9569 1 0 0 2 14.12 89.79 6.2712 0 2 0 2 14.13 4.42 6.2684 0 1 1 4 16.56 100.00 5.3538 1 0 1 4 17.41 26.20 5.0949 1 2 0 2 18.60 2.15 4.7717 -1 2 0 2 18.72 2.29 4.7394 0 2 1 4 22.35 14.06 3.9785 2 0 0 2 24.59 11.81 3.6202 0 3 1 4 24.60 3.01 3.6185 0 0 2 2 25.55 3.00 3.4864 2 0 1 4 25.70 19.48 3.4667 2 2 0 2 26.12 53.90 3.4113 2 1 1 4 26.45 19.83 3.3700 1 3 1 4 26.94 1.41 3.3090 2 -1 1 4 27.07 41.02 3.2939 1 0 2 4 27.34 31.70 3.2616 -2 2 0 2 27.66 1.18 3.2250 -1 3 1 4 27.81 23.52 3.2079 1 1 2 4 28.20 11.31 3.1643 1 -1 2 4 28.47 11.48 3.1356 0 4 0 2 28.48 15.14 3.1342 0 2 2 4 28.55 27.13 3.1265 2 2 1 4 29.92 1.19 2.9867 1 4 0 2 30.05 30.83 2.9736 2 -2 1 4 30.30 22.19 2.9502 1 2 2 4 31.02 2.31 2.8832 -1 2 2 4 31.08 5.63 2.8772 0 4 1 4 31.36 4.64 2.8525 -1 4 0 2 32.43 6.56 2.7608 1 4 1 4 32.45 8.23 2.7588 2 3 1 4 32.73 2.43 2.7360 0 3 2 4 33.48 19.90 2.6769 2 0 2 4 33.78 18.00 2.6538 -1 4 1 4 33.79 1.94 2.6523 3 0 0 2 34.18 65.52 2.6231 1 3 2 4 34.45 53.51 2.6031 -2 3 1 4 34.58 66.81 2.5941 2 -1 2 4 35.15 87.57 2.5530 -1 3 2 4 35.23 8.30 2.5475 2 4 0 2 35.86 23.03 2.5040 3 2 0 2 36.07 25.85 2.4903 3 0 1 4 36.33 4.99 2.4727 3 1 1 4 37.11 11.10 2.4227 2 -2 2 4 37.25 1.92 2.4137 3 -1 1 4 37.43 2.90 2.4029 2 4 1 4 37.70 3.24 2.3859 -3 2 0 2 37.96 5.11 2.3702 0 5 1 4 37.97 13.30 2.3697 0 4 2 4 37.98 1.16 2.3689 0 1 3 4 38.03 5.09 2.3664 3 2 1 4 38.95 27.62 2.3121 1 5 1 4 39.02 19.39 2.3086 1 0 3 4 39.11 17.40 2.3034 1 4 2 4 39.13 17.92 2.3022 2 3 2 4 39.55 1.58 2.2784 1 1 3 4 39.78 13.18 2.2659 3 -2 1 4 40.05 1.19 2.2515 0 2 3 4 40.39 3.34 2.2330 -1 5 1 4 40.84 10.82 2.2094 -2 3 2 4 40.99 78.53 2.2016 3 3 1 4 41.97 3.13 2.1529 -1 2 3 4 42.25 4.29 2.1392 3 0 2 4 43.17 1.75 2.0957 2 5 1 4 43.29 5.86 2.0900 3 -1 2 4 43.30 1.60 2.0895 0 3 3 4 43.44 1.71 2.0830 2 4 2 4 43.89 2.93 2.0628 2 0 3 4 43.92 10.63 2.0616 0 5 2 4 44.04 4.25 2.0561 1 6 0 2 44.25 5.68 2.0469 2 1 3 4 44.46 16.81 2.0379 1 3 3 4 44.77 16.20 2.0241 2 -1 3 4 44.80 4.75 2.0230 1 5 2 4 45.15 8.15 2.0083 0 6 1 4 45.24 1.20 2.0044 -1 3 3 4 45.54 5.82 1.9919 3 -2 2 4 45.54 5.88 1.9918 -2 4 2 4 45.61 5.81 1.9892 -1 6 0 2 45.79 20.22 1.9815 -2 5 1 4 45.88 7.61 1.9778 1 6 1 4 46.09 14.50 1.9694 -1 5 2 4 46.30 8.39 1.9610 -3 4 0 2 46.84 2.00 1.9395 2 -2 3 4 47.40 20.30 1.9181 4 0 1 4 47.40 36.92 1.9180 -1 6 1 4 47.49 3.43 1.9147 4 1 1 4 47.77 6.43 1.9040 2 6 0 2 48.07 12.15 1.8927 -3 4 1 4 48.51 21.07 1.8766 1 4 3 4 48.53 10.92 1.8760 2 3 3 4 48.60 3.81 1.8732 2 5 2 4 48.74 14.67 1.8684 4 2 1 4 48.87 1.17 1.8638 3 -3 2 4 49.50 17.08 1.8414 2 6 1 4 49.95 9.20 1.8260 3 5 1 4 49.98 20.36 1.8248 -2 3 3 4 50.44 4.97 1.8092 0 0 4 2 50.66 5.70 1.8018 4 -2 1 4 51.00 5.19 1.7907 0 1 4 4 51.09 1.06 1.7877 1 6 2 4 51.39 18.36 1.7781 3 1 3 4 52.09 3.53 1.7557 3 -1 3 4 52.25 5.41 1.7506 1 1 4 4 52.49 17.74 1.7434 1 -1 4 4 52.58 3.90 1.7406 4 1 2 4 52.62 8.16 1.7393 0 7 1 4 52.64 6.58 1.7388 0 5 3 4 52.65 19.18 1.7384 0 2 4 4 53.41 4.99 1.7155 1 5 3 4 53.50 6.36 1.7129 4 -1 2 4 53.74 2.09 1.7057 4 2 2 4 53.99 4.63 1.6983 3 6 0 2 54.06 2.94 1.6963 3 -2 3 4 54.55 2.36 1.6824 -1 5 3 4 55.03 7.44 1.6688 3 3 3 4 55.82 5.18 1.6469 2 0 4 4 55.94 6.30 1.6437 4 3 2 4 56.30 2.46 1.6342 1 3 4 4 56.56 1.84 1.6271 2 -1 4 4 57.39 1.12 1.6057 0 7 2 4 57.45 1.58 1.6039 2 2 4 4 57.95 5.16 1.5914 5 0 0 2 57.97 5.51 1.5909 4 -4 1 4 57.98 3.00 1.5906 -3 6 0 2 58.18 2.72 1.5857 -3 5 2 4 58.32 1.90 1.5821 2 -2 4 4 58.32 1.55 1.5821 3 4 3 4 58.56 5.74 1.5762 4 -3 2 4 58.90 2.21 1.5679 5 2 0 2 58.91 2.09 1.5678 0 8 0 2 58.95 1.78 1.5667 -2 5 3 4 59.10 1.42 1.5632 4 4 2 4 59.30 7.56 1.5583 1 8 0 2 59.44 3.80 1.5550 5 1 1 4 59.50 1.92 1.5535 -3 6 1 4 59.76 2.29 1.5475 1 4 4 4 59.77 2.02 1.5471 2 3 4 4 60.31 10.87 1.5347 4 0 3 4 60.31 1.77 1.5347 -1 6 3 4 60.41 1.67 1.5323 5 2 1 4 60.50 3.65 1.5302 5 -1 1 4 60.90 1.09 1.5212 2 7 2 4 61.00 3.53 1.5190 -1 8 0 2 61.03 6.96 1.5183 -5 2 0 2 61.04 1.20 1.5180 -2 3 4 4 61.22 2.31 1.5139 4 -1 3 4 61.45 2.64 1.5089 4 2 3 4 62.22 2.28 1.4921 4 6 0 2 62.28 1.57 1.4908 3 1 4 4 62.35 2.94 1.4892 5 3 1 4 62.48 1.70 1.4866 -1 8 1 4 62.49 5.95 1.4863 3 5 3 4 62.87 3.55 1.4781 -4 5 1 4 63.11 1.63 1.4732 4 -2 3 4 63.13 1.57 1.4728 4 5 2 4 63.62 4.85 1.4625 2 8 1 4 63.68 2.68 1.4613 4 6 1 4 64.07 1.21 1.4533 1 5 4 4 64.65 1.84 1.4416 3 -2 4 4 64.81 2.10 1.4386 5 2 2 4 64.82 2.32 1.4384 0 7 3 4 65.09 1.17 1.4330 -1 5 4 4 65.29 2.50 1.4291 1 7 3 4 65.91 1.03 1.4171 4 -3 3 4 67.10 1.10 1.3949 -4 6 0 2 67.18 1.22 1.3935 -4 5 2 4 67.33 1.97 1.3908 3 -3 4 4 67.64 1.44 1.3851 -1 2 5 4 68.50 1.34 1.3697 -4 6 1 4 68.57 3.76 1.3685 0 9 1 4 69.05 1.49 1.3602 2 0 5 4 69.16 2.22 1.3583 1 6 4 4 69.45 1.20 1.3534 5 4 2 4 69.59 1.50 1.3510 4 -4 3 4 70.35 1.17 1.3383 -3 7 2 4 70.51 1.13 1.3357 2 2 5 4 70.85 6.34 1.3299 -2 7 3 4 70.87 1.06 1.3297 -3 4 4 4 71.18 1.26 1.3246 4 -1 4 4 71.81 1.62 1.3146 0 8 3 4 71.89 1.01 1.3133 5 -1 3 4 72.83 4.85 1.2986 3 8 2 4 73.08 2.09 1.2949 5 5 2 4 73.13 1.04 1.2941 3 7 3 4 73.33 1.96 1.2911 5 -4 2 4 73.35 4.55 1.2907 -1 4 5 4 73.36 1.20 1.2905 -3 8 1 4 73.49 1.58 1.2887 6 -1 1 4 73.53 1.76 1.2880 4 7 2 4 73.59 2.09 1.2871 5 3 3 4 74.49 1.54 1.2737 4 8 0 2 74.54 1.96 1.2731 0 7 4 4 74.69 2.50 1.2708 -1 9 2 4 74.77 3.07 1.2697 2 8 3 4 74.82 1.41 1.2690 4 6 3 4 74.82 2.13 1.2689 -4 7 1 4 74.85 2.14 1.2685 -2 9 1 4 74.98 1.39 1.2666 1 7 4 4 75.45 2.32 1.2600 3 -1 5 4 75.47 4.79 1.2597 2 9 2 4 75.55 7.51 1.2585 2 4 5 4 75.84 1.50 1.2544 4 8 1 4 76.38 2.32 1.2468 6 1 2 4 77.07 1.80 1.2375 3 -2 5 4 77.52 2.55 1.2314 6 -1 2 4 77.64 1.31 1.2297 2 7 4 4 77.83 1.31 1.2273 5 -5 2 4 77.85 1.89 1.2270 -5 6 0 2 77.87 1.17 1.2267 3 3 5 4 78.20 1.01 1.2224 6 -3 1 4 78.80 1.16 1.2145 6 3 2 4 79.41 2.14 1.2067 0 9 3 4 79.77 4.28 1.2022 5 5 3 4 80.36 4.36 1.1949 5 0 4 4 80.76 1.16 1.1900 6 5 1 4 81.08 4.98 1.1861 1 -1 6 4 81.21 1.92 1.1845 0 2 6 4 82.16 2.49 1.1732 6 -3 2 4 82.90 5.15 1.1645 -3 4 5 4 83.01 1.77 1.1633 -1 8 4 4 83.37 2.47 1.1593 -4 5 4 4 83.41 5.67 1.1588 4 2 5 4 83.69 3.05 1.1556 6 6 0 2 83.99 1.79 1.1523 2 6 5 4 83.99 1.31 1.1522 -3 8 3 4 84.09 1.10 1.1511 4 6 4 4 84.41 1.18 1.1476 5 -5 3 4 85.13 5.14 1.1397 -3 9 2 4 85.18 1.99 1.1392 2 2 6 4 85.37 1.12 1.1371 6 3 3 4 86.44 1.77 1.1258 0 4 6 4 86.67 1.01 1.1233 3 9 3 4 86.87 2.84 1.1213 4 9 2 4 87.15 2.27 1.1184 1 4 6 4 87.16 1.95 1.1183 7 2 1 4 87.34 2.39 1.1165 -2 10 2 4 87.88 3.05 1.1110 4 4 5 4 88.43 2.01 1.1055 -7 2 0 2 88.58 3.31 1.1041 0 9 4 4 88.67 1.16 1.1031 2 11 1 4 89.20 1.98 1.0980 3 0 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.