Cl5 H2 In K2 O Wignacourt J, Lorriaux-Rubbens A, Barbier P, Mairesse G, Wallart F Spectrochimica Acta A, Molecular Spectroscopy 36 (1980) 403-411 Structural stdudy of K2 In Cl5, H2 O by X-Ray, Raman and IR spectroscopies _cod_database_code 1004070 _database_code_amcsd 0015623 CELL PARAMETERS: 13.9050 9.9520 7.1850 90.000 90.000 90.000 SPACE GROUP: Pnma X-RAY WAVELENGTH: 1.541838 Cell Volume: 994.279 Density (g/cm3): 2.594 MAX. ABS. INTENSITY / VOLUME**2: 16.60848763 RIR: 2.085 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.87 2.99 6.3832 1 0 1 4 15.21 97.12 5.8254 0 1 1 4 15.55 100.00 5.6994 2 1 0 4 16.50 8.68 5.3730 1 1 1 8 17.75 49.72 4.9963 2 0 1 4 17.83 19.67 4.9760 0 2 0 2 19.88 2.98 4.4652 2 1 1 8 22.66 5.47 3.9245 1 2 1 8 22.83 1.64 3.8949 3 0 1 4 24.54 4.90 3.6270 3 1 1 8 24.78 5.47 3.5925 0 0 2 2 25.26 34.71 3.5257 2 2 1 8 25.61 13.31 3.4783 1 0 2 4 25.63 15.97 3.4762 4 0 0 2 27.16 4.37 3.2835 1 1 2 8 28.52 19.64 3.1292 4 0 1 4 29.12 25.87 3.0671 3 2 1 8 29.39 16.73 3.0391 2 1 2 8 29.66 18.24 3.0118 0 3 1 4 29.84 20.08 2.9940 2 3 0 4 29.93 18.58 2.9851 4 1 1 8 30.37 1.93 2.9436 1 3 1 8 30.70 4.17 2.9127 0 2 2 4 31.38 26.67 2.8508 1 2 2 8 31.39 20.29 2.8497 4 2 0 4 31.51 48.49 2.8395 3 0 2 4 32.80 4.46 2.7305 3 1 2 8 34.58 2.42 2.5935 5 0 1 4 35.55 1.95 2.5255 3 3 1 8 35.78 2.57 2.5097 5 1 1 8 35.95 30.71 2.4982 4 0 2 4 36.10 56.52 2.4880 0 4 0 2 36.43 4.38 2.4662 3 2 2 8 37.10 2.16 2.4230 4 1 2 8 37.46 2.00 2.4006 1 3 2 8 38.13 6.34 2.3602 1 0 3 4 39.17 7.10 2.3000 2 3 2 8 39.23 4.65 2.2965 1 1 3 8 39.59 8.22 2.2763 4 3 1 8 39.81 7.00 2.2644 2 0 3 4 39.94 4.04 2.2571 6 1 0 4 40.40 8.18 2.2326 4 2 2 8 40.50 10.86 2.2271 2 4 1 8 40.92 7.77 2.2056 6 0 1 4 41.04 13.89 2.1991 5 0 2 4 41.88 2.12 2.1572 3 3 2 8 41.96 2.68 2.1534 6 1 1 8 42.08 12.50 2.1473 5 1 2 8 42.39 6.04 2.1325 1 2 3 8 43.06 1.49 2.1008 6 2 0 4 43.49 9.81 2.0807 3 1 3 8 44.28 2.41 2.0454 0 4 2 4 44.33 1.13 2.0432 5 3 1 8 44.79 5.03 2.0236 1 4 2 8 44.80 6.56 2.0232 4 4 0 4 44.96 9.42 2.0164 6 2 1 8 45.45 1.01 1.9956 4 3 2 8 46.41 5.61 1.9564 3 2 3 8 46.64 7.99 1.9475 4 4 1 8 46.64 2.39 1.9474 6 0 2 4 46.97 3.49 1.9346 4 1 3 8 47.26 2.49 1.9232 1 3 3 8 47.39 4.69 1.9182 0 5 1 4 47.49 2.61 1.9146 7 0 1 4 47.52 5.12 1.9135 2 5 0 4 47.58 4.11 1.9112 6 1 2 8 47.88 2.19 1.8998 6 3 0 4 48.66 23.05 1.8713 3 4 2 8 49.64 1.53 1.8367 6 3 1 8 49.74 7.04 1.8329 5 3 2 8 50.28 5.18 1.8148 5 0 3 4 50.31 1.15 1.8135 6 2 2 8 50.83 1.06 1.7962 0 0 4 2 50.86 1.48 1.7954 5 4 1 8 50.99 5.57 1.7910 3 3 3 8 51.16 1.07 1.7853 5 1 3 8 51.28 8.20 1.7814 1 0 4 4 51.86 17.45 1.7629 4 4 2 8 52.16 7.23 1.7536 1 1 4 8 52.63 2.12 1.7391 2 0 4 4 52.65 1.46 1.7384 7 0 2 4 52.66 6.37 1.7381 8 0 0 2 53.52 4.51 1.7123 1 4 3 8 53.52 2.01 1.7122 8 1 0 4 54.10 2.16 1.6953 4 3 3 8 54.30 3.89 1.6894 8 0 1 4 54.32 2.48 1.6889 2 5 2 8 54.65 3.10 1.6795 4 5 1 8 54.65 2.63 1.6794 6 3 2 8 54.73 1.05 1.6772 1 2 4 8 54.81 3.53 1.6749 3 0 4 4 54.82 4.66 1.6747 2 4 3 8 55.14 5.43 1.6656 8 1 1 8 55.69 5.68 1.6504 6 4 1 8 55.79 9.31 1.6477 5 4 2 8 56.01 1.44 1.6418 2 2 4 8 56.04 1.89 1.6409 8 2 0 4 57.62 1.31 1.5997 8 2 1 8 58.64 2.74 1.5742 2 6 1 8 58.84 4.61 1.5695 1 3 4 8 60.10 1.26 1.5396 8 3 0 4 60.36 1.90 1.5335 6 4 2 8 60.69 2.32 1.5261 3 6 1 8 60.88 1.11 1.5216 1 5 3 8 60.97 1.42 1.5196 4 2 4 8 61.07 2.01 1.5173 7 4 1 8 61.34 1.82 1.5112 7 1 3 8 61.38 1.35 1.5105 9 0 1 4 61.61 3.62 1.5054 8 3 1 8 61.98 2.12 1.4972 1 6 2 8 61.99 1.39 1.4970 4 6 0 4 62.99 3.13 1.4757 5 5 2 8 63.44 4.49 1.4662 5 4 3 8 63.67 2.29 1.4615 7 2 3 8 64.06 2.56 1.4536 3 5 3 8 64.31 7.26 1.4484 1 4 4 8 65.28 1.90 1.4294 1 0 5 4 65.48 1.81 1.4254 2 4 4 8 65.50 1.41 1.4250 7 4 2 8 65.51 5.79 1.4249 8 4 0 4 66.03 1.03 1.4149 1 1 5 8 66.77 1.03 1.4010 4 5 3 8 66.95 3.59 1.3976 8 4 1 8 67.11 1.31 1.3947 0 7 1 4 67.21 1.51 1.3929 2 7 0 4 67.26 1.34 1.3920 6 5 2 8 67.40 3.43 1.3894 3 4 4 8 67.45 1.30 1.3886 7 3 3 8 67.82 1.34 1.3818 4 6 2 8 68.76 1.94 1.3652 6 2 4 8 69.08 1.16 1.3597 3 1 5 8 69.23 1.19 1.3571 1 6 3 8 69.40 1.09 1.3541 2 2 5 8 69.43 1.03 1.3537 8 2 3 8 70.71 2.88 1.3323 7 0 4 4 71.01 2.39 1.3274 1 5 4 8 71.12 1.86 1.3256 6 6 1 8 72.85 3.37 1.2983 9 0 3 4 73.11 1.04 1.2944 4 7 1 8 73.32 1.44 1.2912 9 4 1 8 73.53 1.99 1.2880 8 5 1 8 74.29 2.33 1.2766 5 0 5 4 76.59 3.94 1.2440 0 8 0 2 76.93 2.10 1.2394 1 4 5 8 79.33 1.03 1.2077 11 2 1 8 79.38 1.25 1.2071 2 8 1 8 80.44 1.32 1.1939 5 7 2 8 81.41 1.06 1.1821 3 7 3 8 82.05 3.53 1.1745 7 4 4 8 83.01 2.59 1.1633 9 1 4 8 83.28 1.01 1.1602 1 2 6 8 83.62 1.80 1.1564 7 1 5 8 83.65 1.00 1.1560 4 8 1 8 84.10 4.26 1.1510 9 4 3 8 84.74 2.09 1.1440 12 0 1 4 85.15 3.31 1.1394 3 8 2 8 85.49 3.07 1.1358 5 4 5 8 85.83 1.61 1.1322 4 0 6 4 87.62 2.86 1.1136 4 8 2 8 87.86 1.19 1.1112 1 7 4 8 87.88 1.49 1.1109 11 1 3 8 88.53 2.16 1.1045 9 3 4 8 89.13 1.49 1.0986 7 3 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.