Arrojadite Yakubovich O V, Matviyenko Y N, Simonov M A, Melnikov O K Vestnik Moskovskogo Universiteta Geologiya 41 (1986) 36-47 The crystalline structure of synthetic Fe3+-arrojadites with the idealized formula K2Na5Fe2+14Fe3+(PO4)12(OH)2 Locality: synthetic Note: the number of errors and/or typos in this paper is large _database_code_amcsd 0015708 CELL PARAMETERS: 16.5300 10.0840 24.6400 90.000 105.750 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 3953.001 Density (g/cm3): 3.676 MAX. ABS. INTENSITY / VOLUME**2: 10.33910925 RIR: 0.916 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.46 4.78 11.8574 0 0 2 2 10.51 2.48 8.4143 -1 1 1 4 11.12 4.14 7.9547 2 0 0 2 11.59 20.65 7.6337 -2 0 2 2 13.65 23.58 6.4854 1 1 2 4 14.94 4.11 5.9287 0 0 4 2 15.00 15.66 5.9057 2 0 2 2 16.04 18.44 5.5265 -2 0 4 2 16.93 4.32 5.2357 -1 1 4 4 17.59 18.73 5.0420 0 2 0 2 18.58 3.65 4.7743 -3 1 2 4 18.91 4.14 4.6936 3 1 0 4 19.13 4.38 4.6399 0 2 2 4 19.45 8.27 4.5648 1 1 4 4 19.54 1.30 4.5434 -3 1 3 4 21.13 2.16 4.2042 -3 1 4 4 21.55 7.42 4.1234 -4 0 2 2 21.98 1.10 4.0443 3 1 2 4 23.16 4.46 3.8409 0 2 4 4 23.24 1.80 3.8275 -3 1 5 4 23.39 1.67 3.8024 -1 1 6 4 25.15 1.46 3.5405 2 2 3 4 25.79 1.51 3.4547 0 2 5 4 26.20 14.70 3.4015 1 1 6 4 26.91 7.24 3.3130 3 1 4 4 27.11 2.73 3.2887 1 3 0 4 27.51 7.48 3.2427 2 2 4 4 27.74 15.81 3.2159 -1 3 2 4 27.80 35.08 3.2094 2 0 6 2 28.40 2.76 3.1421 -4 2 3 4 28.55 4.18 3.1265 -3 1 7 4 28.57 4.49 3.1243 1 3 2 4 28.68 2.74 3.1130 -5 1 1 4 29.15 1.55 3.0631 -2 0 8 2 29.35 100.00 3.0432 -4 2 4 4 29.39 5.33 3.0390 -5 1 4 4 29.44 1.21 3.0344 5 1 0 4 30.01 1.69 2.9778 1 3 3 4 30.15 3.58 2.9644 0 0 8 2 30.27 3.40 2.9529 4 0 4 2 30.33 3.56 2.9469 -1 3 4 4 30.45 2.38 2.9352 -1 1 8 4 30.59 1.64 2.9225 -5 1 5 4 31.13 1.66 2.8727 4 2 2 4 31.18 1.74 2.8686 -3 3 1 4 31.26 1.15 2.8616 -2 2 7 4 31.31 22.69 2.8566 -3 3 2 4 31.51 12.07 2.8391 3 3 0 4 31.59 6.36 2.8323 -3 1 8 4 31.82 1.27 2.8120 0 2 7 4 31.85 9.04 2.8098 1 3 4 4 32.21 18.03 2.7794 -5 1 6 4 32.30 3.34 2.7718 3 3 1 4 32.40 25.15 2.7632 -4 0 8 2 32.53 1.87 2.7521 -4 2 6 4 32.54 19.93 2.7516 -6 0 2 2 32.94 4.25 2.7192 -3 3 4 4 32.95 4.54 2.7186 3 1 6 4 33.09 79.37 2.7075 2 2 6 4 33.51 2.11 2.6744 3 3 2 4 34.03 1.94 2.6343 1 3 5 4 34.25 2.68 2.6179 -2 2 8 4 34.48 6.22 2.6008 -1 3 6 4 35.12 11.04 2.5554 0 2 8 4 35.22 27.41 2.5481 4 2 4 4 35.27 5.14 2.5446 -6 0 6 2 35.61 21.36 2.5210 0 4 0 2 36.48 2.19 2.4631 -2 0 10 2 36.59 1.82 2.4556 5 1 4 4 36.68 1.07 2.4499 6 0 2 2 37.04 1.95 2.4269 3 3 4 4 37.10 9.57 2.4232 -4 2 8 4 37.23 16.13 2.4153 -6 2 2 4 37.57 2.71 2.3938 -2 4 2 4 37.68 6.44 2.3872 -6 2 4 4 37.87 3.56 2.3755 -1 1 10 4 38.29 1.53 2.3507 -3 3 7 4 38.50 4.22 2.3386 -6 2 5 4 38.82 2.70 2.3200 0 4 4 4 38.98 2.14 2.3108 5 3 0 4 39.19 2.74 2.2989 -7 1 3 4 39.23 1.07 2.2962 1 3 7 4 39.31 2.28 2.2918 -7 1 2 4 39.44 1.06 2.2846 -7 1 4 4 39.48 1.88 2.2824 2 2 8 4 39.48 1.09 2.2823 6 2 1 4 39.78 1.58 2.2660 -1 3 8 4 39.89 5.94 2.2602 -5 3 5 4 40.10 1.45 2.2486 2 4 3 4 40.52 2.66 2.2261 0 4 5 4 40.69 2.04 2.2172 7 1 0 4 40.77 1.39 2.2131 -2 2 10 4 41.07 7.81 2.1979 -7 1 6 4 41.20 2.28 2.1913 -6 2 7 4 41.97 1.46 2.1527 5 1 6 4 42.11 1.91 2.1460 0 2 10 4 42.17 1.60 2.1429 1 3 8 4 42.45 2.61 2.1293 4 4 0 4 42.53 1.31 2.1255 0 4 6 4 42.64 3.94 2.1205 2 0 10 2 42.70 1.26 2.1173 4 0 8 2 42.75 1.81 2.1154 6 2 3 4 42.80 2.56 2.1127 -5 3 7 4 43.00 3.00 2.1036 -4 4 4 4 44.05 1.41 2.0556 -7 1 8 4 44.82 1.31 2.0222 6 2 4 4 45.13 1.45 2.0089 -8 0 6 2 45.36 1.24 1.9994 -1 5 1 4 45.59 2.03 1.9898 -1 1 12 4 45.62 4.69 1.9887 8 0 0 2 45.63 1.09 1.9880 1 5 1 4 45.73 3.54 1.9840 -1 5 2 4 45.90 2.38 1.9769 -1 3 10 4 46.46 4.29 1.9547 2 2 10 4 46.52 5.45 1.9522 4 2 8 4 46.66 4.71 1.9465 -2 4 8 4 47.24 1.15 1.9241 1 5 3 4 47.34 2.35 1.9204 0 4 8 4 47.42 3.75 1.9173 4 4 4 4 47.43 2.14 1.9168 7 1 4 4 47.45 3.46 1.9160 3 3 8 4 47.58 1.09 1.9111 -7 3 1 4 47.65 7.79 1.9084 -8 0 8 2 48.14 2.25 1.8902 -3 5 2 4 48.34 2.80 1.8828 7 3 0 4 48.80 1.93 1.8662 -8 2 6 4 48.91 5.20 1.8624 -4 4 8 4 49.01 1.88 1.8588 -6 4 2 4 49.21 1.34 1.8514 -3 3 11 4 49.72 1.46 1.8338 6 2 6 4 50.41 1.68 1.8102 -1 5 6 4 50.78 2.98 1.7979 7 3 2 4 51.18 1.90 1.7849 -8 2 8 4 51.32 2.67 1.7802 -8 0 10 2 51.63 1.90 1.7702 4 4 6 4 51.67 1.10 1.7691 -3 5 6 4 51.90 10.20 1.7618 -2 4 10 4 51.92 1.29 1.7610 1 5 6 4 52.05 12.91 1.7569 6 4 2 4 52.06 4.79 1.7568 -2 0 14 2 52.33 1.22 1.7484 3 5 4 4 52.35 2.76 1.7478 8 0 4 2 52.43 3.62 1.7452 -3 3 12 4 52.56 1.11 1.7412 9 1 0 4 52.92 3.78 1.7303 -6 2 12 4 53.49 2.09 1.7129 -4 4 10 4 53.82 2.86 1.7034 5 5 0 4 54.44 5.45 1.6853 -1 5 8 4 54.80 2.16 1.6751 -5 1 14 4 54.85 1.39 1.6737 -5 3 12 4 54.99 1.50 1.6698 5 3 8 4 55.16 1.71 1.6651 -3 5 8 4 55.20 2.80 1.6640 0 6 2 4 55.38 6.38 1.6589 -2 2 14 4 55.56 3.70 1.6541 -5 5 6 4 55.58 3.77 1.6535 1 3 12 4 55.61 1.53 1.6527 5 5 2 4 55.66 6.77 1.6514 8 2 4 4 55.92 1.15 1.6443 -6 0 14 2 56.03 1.62 1.6414 -2 6 2 4 56.13 1.51 1.6387 -4 4 11 4 56.16 1.54 1.6379 -10 0 6 2 56.35 3.41 1.6327 1 5 8 4 56.60 1.48 1.6261 -9 1 10 4 56.73 1.37 1.6228 2 4 10 4 56.81 1.85 1.6207 -3 1 15 4 57.13 1.39 1.6123 9 1 3 4 57.17 1.03 1.6113 -9 3 4 4 57.38 1.01 1.6057 0 2 14 4 57.42 7.59 1.6047 4 0 12 2 57.77 1.04 1.5960 -8 4 4 4 57.86 2.33 1.5936 -10 0 8 2 58.51 1.74 1.5775 5 5 4 4 58.87 4.61 1.5687 6 0 10 2 59.14 1.80 1.5621 2 6 4 4 59.17 3.51 1.5615 -8 2 12 4 59.17 2.07 1.5614 8 4 0 4 59.33 2.79 1.5578 -10 2 6 4 59.41 1.80 1.5556 -1 5 10 4 59.79 1.37 1.5466 0 6 6 4 60.16 4.21 1.5382 -4 6 4 4 60.55 2.30 1.5292 -7 5 4 4 60.55 2.29 1.5291 4 2 12 4 60.66 1.28 1.5267 -10 0 10 2 60.81 1.86 1.5233 10 0 2 2 61.19 1.55 1.5147 4 6 2 4 61.54 1.21 1.5070 8 4 2 4 61.63 2.11 1.5049 9 3 2 4 62.32 1.16 1.4899 -5 5 10 4 62.37 3.95 1.4889 2 6 6 4 62.42 1.56 1.4877 5 5 6 4 62.81 1.23 1.4795 -9 3 10 4 63.20 1.47 1.4712 -9 1 13 4 63.37 1.73 1.4677 -11 1 7 4 63.38 1.15 1.4676 -2 2 16 4 63.65 1.27 1.4620 0 6 8 4 63.71 1.58 1.4607 4 6 4 4 64.53 1.56 1.4441 -8 2 14 4 64.67 1.81 1.4413 -2 4 14 4 64.94 1.19 1.4359 -4 6 8 4 65.03 1.14 1.4343 -6 6 2 4 65.23 1.06 1.4304 9 3 4 4 65.33 2.71 1.4283 -6 6 4 4 65.49 1.40 1.4252 4 0 14 2 65.66 3.21 1.4220 0 2 16 4 65.92 6.38 1.4169 8 2 8 4 66.67 1.22 1.4028 7 5 4 4 67.25 1.42 1.3922 -3 7 2 4 67.36 1.28 1.3902 3 7 0 4 67.46 1.13 1.3883 -2 6 10 4 68.18 1.02 1.3754 -3 7 4 4 68.50 1.29 1.3697 3 3 14 4 69.23 1.83 1.3572 -11 3 7 4 69.43 3.35 1.3537 4 4 12 4 69.82 1.84 1.3470 -10 4 8 4 70.68 1.87 1.3328 -6 0 18 2 70.73 1.94 1.3319 6 4 10 4 70.75 1.69 1.3316 -1 1 18 4 71.11 1.96 1.3258 12 0 0 2 71.24 1.38 1.3237 1 3 16 4 72.25 1.03 1.3077 10 2 6 4 73.49 1.38 1.2886 -6 2 18 4 77.13 1.54 1.2366 -7 1 19 4 84.56 1.15 1.1459 -14 2 4 4 85.72 1.16 1.1333 -9 7 4 4 88.06 1.33 1.1092 8 6 8 4 88.06 1.33 1.1092 -4 8 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.