Sulfur Schmidt V M, Wilhelm E, Debaerdemaeker T, Hellner E, Kutoglu A Zeitschrift fur Anorganische und Allgemeine Chemie 405 (1974) 153-162 Darstellung und kristallstruktur von cyclooktadekaschwefel, S18, und cycloikosaschwefel, S20 Locality: synthetic Note: structure for S18 _database_code_amcsd 0015780 CELL PARAMETERS: 21.1520 11.4410 7.5810 90.000 90.000 90.000 SPACE GROUP: P2_12_12_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1834.602 Density (g/cm3): 2.089 MAX. ABS. INTENSITY / VOLUME**2: 4.834329227 RIR: 0.753 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.36 7.29 10.5760 2 0 0 2 11.39 2.14 7.7662 2 1 0 4 14.01 11.47 6.3196 0 1 1 4 14.63 4.37 6.0551 1 1 1 4 14.76 3.30 6.0024 3 1 0 4 16.34 9.40 5.4249 2 1 1 4 16.77 15.98 5.2880 4 0 0 2 18.48 1.75 4.8001 4 1 0 4 18.86 18.41 4.7059 3 1 1 4 19.89 100.00 4.4635 1 2 1 4 19.99 15.73 4.4423 3 2 0 4 21.92 13.87 4.0555 4 1 1 4 23.21 2.34 3.8327 3 2 1 4 23.47 15.99 3.7905 0 0 2 2 23.71 42.39 3.7532 1 3 0 4 23.85 49.12 3.7311 1 0 2 4 24.74 13.04 3.5982 0 1 2 4 24.82 38.38 3.5875 2 3 0 4 25.10 10.79 3.5472 1 1 2 4 25.26 61.12 3.5253 6 0 0 2 25.34 24.07 3.5154 5 1 1 4 25.78 26.38 3.4561 4 2 1 4 26.16 13.24 3.4069 0 3 1 4 26.16 3.70 3.4064 2 1 2 4 26.20 14.69 3.4014 5 2 0 4 26.50 5.92 3.3635 1 3 1 4 26.57 27.94 3.3544 3 3 0 4 26.70 60.66 3.3386 3 0 2 4 28.56 26.35 3.1251 1 2 2 4 28.77 56.50 3.1033 5 2 1 4 28.86 1.05 3.0932 4 3 0 4 29.00 13.65 3.0787 6 1 1 4 29.11 1.64 3.0675 3 3 1 4 29.50 2.01 3.0275 2 2 2 4 30.04 2.67 2.9748 4 1 2 4 30.60 1.57 2.9215 7 1 0 4 31.01 12.10 2.8835 3 2 2 4 31.23 9.53 2.8640 4 3 1 4 31.27 2.06 2.8602 0 4 0 2 31.59 1.76 2.8326 5 3 0 4 31.70 3.14 2.8230 5 0 2 4 32.08 2.57 2.7905 6 2 1 4 32.67 10.61 2.7408 5 1 2 4 32.85 2.52 2.7261 7 1 1 4 33.02 3.48 2.7124 4 2 2 4 33.33 26.11 2.6884 0 3 2 4 33.49 9.08 2.6761 0 4 1 4 33.54 5.84 2.6719 7 2 0 4 33.60 15.42 2.6670 1 3 2 4 33.76 2.87 2.6549 1 4 1 4 33.78 21.90 2.6534 5 3 1 4 33.90 1.73 2.6440 8 0 0 2 34.42 2.31 2.6056 2 3 2 4 34.75 2.72 2.5814 6 0 2 4 34.83 1.19 2.5761 8 1 0 4 35.46 38.52 2.5316 5 2 2 4 35.65 5.68 2.5181 6 1 2 4 35.74 6.37 2.5120 3 3 2 4 36.67 2.49 2.4509 1 1 3 4 36.68 24.52 2.4498 6 3 1 4 37.53 14.00 2.3965 4 3 2 4 37.67 3.01 2.3878 4 4 1 4 38.66 1.11 2.3290 3 1 3 4 39.21 4.39 2.2978 1 2 3 4 39.47 6.32 2.2832 0 4 2 4 39.71 1.93 2.2700 1 4 2 4 39.72 4.18 2.2690 5 3 2 4 39.86 5.32 2.2616 5 4 1 4 39.88 6.63 2.2606 7 3 1 4 40.34 1.26 2.2361 4 1 3 4 41.34 12.80 2.1839 7 2 2 4 41.44 1.94 2.1789 1 5 1 4 41.58 1.95 2.1721 3 4 2 4 42.13 1.78 2.1451 2 5 1 4 42.41 1.83 2.1314 5 1 3 4 42.42 6.56 2.1306 8 1 2 4 42.75 3.49 2.1152 10 0 0 2 43.32 4.79 2.0888 8 3 1 4 43.51 1.42 2.0800 10 1 0 4 46.13 6.45 1.9677 9 1 2 4 46.97 3.71 1.9346 9 3 1 4 47.01 1.89 1.9330 6 2 3 4 47.97 1.30 1.8963 11 1 0 4 48.04 21.55 1.8938 0 4 3 4 48.21 1.59 1.8877 1 0 4 4 48.39 5.71 1.8808 8 4 1 4 48.70 1.01 1.8698 0 1 4 4 49.52 1.68 1.8407 3 6 0 4 49.63 1.13 1.8369 4 5 2 4 50.02 1.36 1.8235 10 1 2 4 50.07 3.58 1.8216 7 4 2 4 50.60 5.65 1.8040 8 1 3 4 50.94 3.24 1.7926 1 2 4 4 51.20 2.00 1.7841 4 0 4 4 51.40 6.99 1.7776 5 5 2 4 51.57 12.48 1.7722 11 2 1 4 51.66 2.15 1.7694 9 3 2 4 51.77 3.24 1.7659 9 4 1 4 51.87 5.88 1.7627 12 0 0 2 52.03 2.07 1.7577 10 2 2 4 52.42 7.20 1.7456 4 6 1 4 52.92 5.35 1.7302 8 5 0 4 52.98 1.98 1.7285 5 4 3 4 53.43 1.54 1.7149 11 0 2 4 53.51 2.95 1.7123 6 5 2 4 53.59 7.80 1.7102 5 1 4 4 53.82 3.31 1.7032 4 2 4 4 53.87 5.25 1.7018 9 1 3 4 53.91 3.12 1.7007 10 4 0 4 54.01 4.23 1.6979 1 6 2 4 54.03 1.65 1.6972 0 3 4 4 54.13 8.76 1.6944 5 6 1 4 54.22 2.70 1.6918 1 3 4 4 54.25 2.14 1.6907 1 5 3 4 54.57 1.72 1.6818 2 6 2 4 54.78 1.64 1.6758 2 3 4 4 54.82 4.08 1.6748 2 5 3 4 55.01 1.79 1.6693 6 0 4 4 55.05 17.75 1.6683 6 4 3 4 55.36 2.38 1.6594 10 4 1 4 55.50 2.81 1.6556 5 2 4 4 55.64 5.24 1.6518 6 1 4 4 55.78 1.31 1.6480 9 2 3 4 55.94 3.43 1.6437 7 5 2 4 55.98 1.87 1.6426 11 2 2 4 56.10 2.72 1.6395 9 5 0 4 56.17 1.86 1.6376 6 6 1 4 57.02 1.42 1.6151 4 5 3 4 57.38 1.12 1.6059 10 1 3 4 57.88 2.36 1.5932 1 7 1 4 58.01 3.62 1.5900 7 1 4 4 58.29 1.09 1.5829 12 1 2 4 58.40 2.29 1.5801 5 6 2 4 58.52 4.83 1.5773 7 6 1 4 58.58 1.79 1.5757 13 1 1 4 58.65 1.19 1.5740 8 5 2 4 58.87 1.19 1.5686 9 3 3 4 59.52 1.89 1.5532 10 5 0 4 59.58 1.06 1.5517 10 4 2 4 60.01 2.08 1.5417 3 4 4 4 60.54 3.02 1.5294 4 7 1 4 61.03 1.73 1.5182 1 6 3 4 61.10 1.79 1.5167 11 1 3 4 61.16 2.10 1.5154 8 6 1 4 61.99 1.16 1.4971 1 7 2 4 62.08 1.19 1.4952 13 0 2 4 62.10 3.26 1.4947 5 7 1 4 62.44 4.28 1.4874 8 2 4 4 63.07 1.93 1.4741 12 3 2 4 63.16 1.39 1.4720 12 4 1 4 63.29 1.94 1.4694 14 1 1 4 63.64 3.18 1.4621 1 2 5 4 64.99 1.60 1.4349 3 2 5 4 65.02 3.93 1.4344 14 2 1 4 65.96 1.15 1.4163 5 1 5 4 66.54 1.10 1.4053 0 8 1 4 66.74 1.37 1.4016 12 2 3 4 67.65 2.28 1.3848 5 2 5 4 67.78 1.88 1.3826 6 1 5 4 71.14 2.97 1.3252 6 8 0 4 71.27 1.09 1.3233 10 5 3 4 71.31 1.44 1.3226 15 3 0 4 71.37 2.10 1.3216 15 0 2 4 71.86 1.52 1.3137 11 2 4 4 73.38 2.23 1.2903 12 4 3 4 73.50 1.14 1.2885 14 1 3 4 80.47 1.09 1.1935 11 6 3 4 80.80 1.42 1.1894 6 0 6 4 85.62 1.01 1.1344 8 1 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.