H38 N8 O27 P8 Schuelke U, Averbuch-Pouchot M, Durif A Zeitschrift fur Anorganische und Allgemeine Chemie 619 (1993) 374-380 Preparation and crystal structure of ammonium cyclooctaphosphate trihydrate: (NH4)8P8O24 . 3H2O _cod_database_code 1007215 _database_code_amcsd 0015900 CELL PARAMETERS: 24.2680 6.7000 20.5860 90.000 112.060 90.000 SPACE GROUP: Cc X-RAY WAVELENGTH: 1.541838 Cell Volume: 3102.148 Density (g/cm3): 1.777 MAX. ABS. INTENSITY / VOLUME**2: 5.393059353 RIR: 0.988 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.86 17.64 11.2457 2 0 0 1 9.27 28.40 9.5395 0 0 2 1 9.65 1.55 9.1692 -2 0 2 1 13.79 4.91 6.4211 1 1 0 2 14.07 100.00 6.2931 -1 1 1 2 14.25 16.67 6.2139 2 0 2 1 14.99 12.77 5.9117 -4 0 2 1 15.02 48.48 5.8976 1 1 1 2 15.76 14.62 5.6228 4 0 0 1 17.19 7.20 5.1596 -3 1 1 2 17.25 19.29 5.1394 -2 0 4 1 17.46 1.30 5.0804 1 1 2 2 17.75 8.96 4.9957 3 1 0 2 17.86 2.78 4.9657 -3 1 2 2 18.55 2.30 4.7822 -1 1 3 2 18.60 24.80 4.7697 0 0 4 1 19.36 10.01 4.5846 -4 0 4 1 19.46 14.75 4.5612 3 1 1 2 19.66 13.39 4.5158 -3 1 3 2 20.68 20.48 4.2942 1 1 3 2 21.99 9.03 4.0420 -1 1 4 2 22.05 1.18 4.0304 3 1 2 2 22.70 15.69 3.9169 -5 1 2 2 22.82 7.98 3.8964 2 0 4 1 23.74 1.85 3.7486 6 0 0 1 23.83 23.52 3.7346 5 1 0 2 24.06 2.83 3.6984 -6 0 4 1 25.28 2.01 3.5235 3 1 3 2 25.29 17.34 3.5214 -5 1 4 2 25.58 17.12 3.4817 -3 1 5 2 25.70 9.44 3.4669 5 1 1 2 25.85 11.35 3.4466 -1 1 5 2 26.52 7.51 3.3611 -4 0 6 1 26.61 23.89 3.3500 0 2 0 2 27.02 6.19 3.2995 0 2 1 2 27.73 1.05 3.2172 -5 1 5 2 28.06 3.60 3.1798 0 0 6 1 28.25 1.75 3.1593 5 1 2 2 28.46 8.54 3.1359 1 1 5 2 28.67 4.05 3.1135 6 0 2 1 28.73 6.65 3.1070 4 0 4 1 28.94 19.18 3.0856 3 1 4 2 29.22 8.69 3.0564 -6 0 6 1 29.23 2.85 3.0556 -7 1 3 2 29.28 1.34 3.0506 -3 1 6 2 29.56 3.47 3.0220 -8 0 2 1 29.58 5.43 3.0201 -7 1 1 2 29.80 2.20 2.9983 -2 2 3 2 29.99 6.58 2.9794 -1 1 6 2 30.15 1.47 2.9639 0 2 3 2 30.19 4.15 2.9607 -7 1 4 2 30.24 15.07 2.9558 -8 0 4 1 30.31 2.47 2.9488 2 2 2 2 30.51 5.58 2.9300 -4 2 1 2 30.72 8.20 2.9101 -5 1 6 2 31.33 1.89 2.8551 5 1 3 2 31.56 8.44 2.8346 -4 2 3 2 31.83 2.34 2.8114 8 0 0 1 31.89 2.24 2.8064 -2 2 4 2 32.34 3.40 2.7683 4 2 1 2 32.56 5.65 2.7499 2 2 3 2 32.91 1.13 2.7216 3 1 5 2 33.12 5.66 2.7048 -4 2 4 2 34.08 4.81 2.6305 -7 1 6 2 34.15 1.47 2.6257 -5 1 7 2 34.34 1.48 2.6116 -1 1 7 2 34.53 1.36 2.5977 -2 2 5 2 35.04 4.04 2.5606 -6 2 1 2 35.16 2.56 2.5525 -6 2 3 2 35.29 1.47 2.5430 7 1 2 2 35.59 2.06 2.5227 6 0 4 1 35.91 4.72 2.5011 -9 1 3 2 36.14 3.21 2.4854 -9 1 2 2 36.56 9.59 2.4580 8 0 2 1 36.84 2.47 2.4399 -7 1 7 2 37.00 3.65 2.4297 -9 1 1 2 37.19 2.74 2.4174 1 1 7 2 37.33 2.77 2.4091 -9 1 5 2 37.46 1.74 2.4006 6 2 1 2 37.48 4.16 2.3997 -10 0 2 1 37.62 6.58 2.3911 -2 2 6 2 37.72 4.25 2.3849 0 0 8 1 37.79 3.74 2.3807 -6 2 5 2 37.91 2.17 2.3736 -5 1 8 2 37.92 1.56 2.3727 -4 2 6 2 38.25 4.69 2.3529 7 1 3 2 38.64 5.45 2.3304 5 1 5 2 39.30 1.32 2.2923 -8 0 8 1 39.44 1.43 2.2848 -10 0 6 1 39.51 2.87 2.2806 6 2 2 2 39.56 1.27 2.2780 4 2 4 2 40.09 1.70 2.2491 10 0 0 1 40.43 1.57 2.2310 9 1 1 2 40.71 6.84 2.2164 -8 2 4 2 41.59 1.00 2.1713 7 1 4 2 42.04 1.50 2.1491 6 2 3 2 43.05 3.86 2.1012 8 0 4 1 43.45 1.78 2.0829 -8 2 6 2 43.53 2.49 2.0789 -7 1 9 2 43.64 1.31 2.0742 1 3 3 2 43.74 1.30 2.0696 -10 0 8 1 44.02 1.06 2.0570 -4 0 10 1 44.74 1.12 2.0258 10 0 2 1 45.12 3.45 2.0096 -2 0 10 1 45.76 1.77 1.9827 9 1 3 2 46.10 1.57 1.9691 3 1 8 2 46.19 5.71 1.9655 -5 3 4 2 46.19 1.67 1.9653 -5 1 10 2 46.43 1.81 1.9559 5 3 1 2 46.76 1.06 1.9428 0 2 8 2 47.67 1.47 1.9079 0 0 10 1 47.68 1.24 1.9075 -5 3 5 2 48.14 1.97 1.8902 1 3 5 2 48.45 1.07 1.8790 3 3 4 2 48.90 1.74 1.8625 -6 2 9 2 49.14 1.14 1.8542 -1 3 6 2 49.26 1.38 1.8496 -7 3 4 2 49.28 1.83 1.8492 -12 0 8 1 50.34 1.05 1.8126 4 2 7 2 51.02 1.36 1.7900 -8 2 9 2 54.21 1.09 1.6919 -12 0 10 1 54.75 1.90 1.6767 -5 3 8 2 57.27 1.05 1.6086 -10 2 10 2 57.40 1.05 1.6053 4 4 0 2 57.70 1.18 1.5976 -4 4 3 2 58.49 1.24 1.5780 10 0 6 1 59.13 1.13 1.5625 -7 3 9 2 59.39 2.04 1.5563 13 1 2 2 59.50 1.62 1.5535 8 0 8 1 59.94 1.78 1.5433 -6 4 1 2 60.16 3.25 1.5381 -14 2 5 2 60.72 1.09 1.5253 -6 2 12 2 63.16 1.01 1.4720 12 2 3 2 65.17 1.44 1.4315 -6 2 13 2 65.97 1.00 1.4161 3 1 12 2 70.94 1.15 1.3285 -17 1 1 2 74.67 2.00 1.2712 -1 5 5 2 80.50 1.12 1.1931 -19 1 11 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.