Ba7 F32 Fe6 H4 O2 Crosnier-Lopez M, Calage Y, Duroy H, Fourquet J Zeitschrift fur Anorganische und Allgemeine Chemie 621 (1995) 1025-1032 Ba7 Fe6 F32 . 2(H2 O): original isolated trimers (Fe3 F16)(7-) in a new defective jarlite-type compound _cod_database_code 1000375 _database_code_amcsd 0015812 CELL PARAMETERS: 17.0230 11.4820 7.6240 90.000 101.130 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 1462.144 Density (g/cm3): 4.397 MAX. ABS. INTENSITY / VOLUME**2: 26.95105168 RIR: 1.996 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.35 13.55 9.4620 1 1 0 4 10.59 45.58 8.3514 2 0 0 2 11.83 4.30 7.4806 0 0 1 2 14.27 8.60 6.2077 -1 1 1 4 14.29 12.13 6.1984 -2 0 1 2 15.43 11.98 5.7410 0 2 0 2 17.70 6.41 5.0097 3 1 0 4 18.76 8.15 4.7310 2 2 0 4 19.49 9.20 4.5544 0 2 1 4 19.54 1.24 4.5433 -3 1 1 4 21.09 5.42 4.2119 -2 2 1 4 21.28 18.95 4.1757 4 0 0 2 22.29 3.47 3.9885 -4 0 1 2 23.02 44.02 3.8638 3 1 1 4 23.32 3.72 3.8145 2 2 1 4 23.79 11.44 3.7403 0 0 2 2 23.85 19.69 3.7306 1 3 0 4 24.12 8.32 3.6896 -2 0 2 2 24.62 53.19 3.6162 -1 1 2 4 26.23 14.89 3.3975 -1 3 1 4 26.38 16.48 3.3791 4 0 1 2 26.39 100.00 3.3769 4 2 0 4 26.57 1.74 3.3552 1 1 2 4 27.16 8.65 3.2829 -3 1 2 4 27.17 24.72 3.2825 1 3 1 4 27.22 38.47 3.2756 -4 2 1 4 27.81 1.97 3.2076 5 1 0 4 27.96 10.97 3.1915 2 0 2 2 28.16 6.57 3.1684 -5 1 1 4 28.30 10.30 3.1540 3 3 0 4 28.48 60.99 3.1339 0 2 2 4 28.76 19.50 3.1039 -2 2 2 4 28.81 19.44 3.0992 -4 0 2 2 29.51 20.78 3.0272 -3 3 1 4 31.16 27.47 2.8705 0 4 0 2 31.98 8.42 2.7987 3 3 1 4 32.07 5.90 2.7910 -6 0 1 2 32.09 8.38 2.7894 2 2 2 4 32.34 6.61 2.7680 5 1 1 4 32.84 11.12 2.7272 -4 2 2 4 33.00 2.94 2.7146 2 4 0 4 33.18 2.64 2.7002 -1 3 2 4 33.26 6.53 2.6941 -5 1 2 4 33.44 4.13 2.6800 0 4 1 4 35.17 1.25 2.5520 4 0 2 2 35.67 1.12 2.5168 5 3 0 4 35.85 1.68 2.5049 6 2 0 4 35.96 3.35 2.4977 -5 3 1 4 36.24 4.32 2.4789 -1 1 3 4 36.32 1.09 2.4735 -6 0 2 2 38.04 2.17 2.3655 4 4 0 4 38.30 5.11 2.3498 -4 0 3 2 38.32 1.91 2.3488 1 1 3 4 38.54 2.66 2.3362 7 1 0 4 38.61 2.61 2.3320 4 2 2 4 38.65 14.48 2.3298 -4 4 1 4 38.94 8.82 2.3127 -2 2 3 4 39.33 24.82 2.2909 3 3 2 4 39.40 1.53 2.2871 0 2 3 4 39.40 3.77 2.2870 5 3 1 4 39.58 11.93 2.2772 0 4 2 4 39.67 11.84 2.2721 2 0 3 2 39.79 2.19 2.2656 -2 4 2 4 40.17 24.50 2.2447 -5 3 2 4 40.29 1.36 2.2384 5 1 2 4 41.27 7.07 2.1877 4 4 1 4 41.52 1.70 2.1747 -4 2 3 4 41.55 5.74 2.1735 -5 1 3 4 41.80 7.84 2.1608 1 5 1 4 42.35 10.57 2.1342 2 4 2 4 42.59 11.90 2.1229 3 5 0 4 42.65 18.99 2.1197 -8 0 1 2 42.67 8.36 2.1189 7 1 1 4 42.74 2.72 2.1157 -1 3 3 4 42.80 8.55 2.1127 2 2 3 4 42.95 5.37 2.1060 -4 4 2 4 43.25 4.01 2.0920 3 1 3 4 43.34 20.72 2.0879 8 0 0 2 43.45 1.66 2.0829 -3 5 1 4 43.75 5.23 2.0692 -3 3 3 4 43.82 6.49 2.0661 -6 0 3 2 44.57 7.16 2.0330 1 3 3 4 44.76 9.72 2.0248 7 3 0 4 45.25 7.72 2.0039 3 5 1 4 45.32 8.14 2.0011 -6 4 1 4 45.48 1.04 1.9942 -8 0 2 2 45.85 8.35 1.9793 4 0 3 2 46.15 19.69 1.9668 -1 5 2 4 46.27 1.98 1.9621 8 2 0 4 46.73 2.22 1.9441 -6 2 3 4 47.04 15.02 1.9319 6 2 2 4 47.41 1.58 1.9174 8 0 1 2 47.43 1.69 1.9170 -7 3 2 4 47.45 5.64 1.9161 -5 3 3 4 47.51 2.02 1.9137 0 6 0 2 47.68 7.09 1.9075 -3 5 2 4 47.68 4.32 1.9072 4 4 2 4 47.74 14.28 1.9051 -2 0 4 2 47.97 2.18 1.8966 -2 4 3 4 48.07 2.68 1.8926 -7 1 3 4 48.30 5.44 1.8842 -5 5 1 4 48.31 11.51 1.8838 -8 2 2 4 48.35 2.69 1.8825 0 4 3 4 48.46 1.83 1.8784 7 3 1 4 48.59 5.22 1.8738 -6 4 2 4 48.98 1.03 1.8596 3 3 3 4 49.40 2.05 1.8448 -4 0 4 2 49.77 2.46 1.8320 7 1 2 4 49.87 1.21 1.8285 -2 6 1 4 50.16 11.21 1.8187 8 2 1 4 50.17 2.59 1.8183 -4 4 3 4 50.96 1.10 1.7919 2 6 1 4 51.06 8.15 1.7887 5 5 1 4 51.17 1.07 1.7852 -9 1 2 4 51.28 1.37 1.7815 2 4 3 4 51.82 1.14 1.7641 -5 1 4 4 52.14 2.33 1.7542 2 0 4 2 52.61 2.64 1.7397 4 6 0 4 53.08 4.55 1.7254 -4 6 1 4 53.76 8.14 1.7052 -8 4 1 4 53.81 1.79 1.7036 0 6 2 4 53.88 4.78 1.7015 -1 3 4 4 53.89 1.25 1.7013 6 0 3 2 53.97 1.58 1.6990 -8 2 3 4 54.16 5.73 1.6935 -9 3 1 4 54.30 1.09 1.6895 8 0 2 2 54.33 2.93 1.6885 8 4 0 4 54.68 3.87 1.6786 -3 5 3 4 54.71 10.85 1.6776 2 2 4 4 55.16 1.16 1.6652 4 6 1 4 55.38 4.09 1.6590 1 5 3 4 55.52 2.26 1.6551 5 3 3 4 56.02 8.96 1.6415 -6 2 4 4 56.36 1.37 1.6324 1 7 0 4 56.37 5.31 1.6323 -9 1 3 4 57.56 2.79 1.6012 -1 7 1 4 57.84 1.40 1.5942 -7 5 2 4 58.06 4.03 1.5887 1 7 1 4 58.11 12.07 1.5873 -2 4 4 4 58.48 1.49 1.5783 -6 6 1 4 58.68 1.99 1.5734 3 7 0 4 58.70 1.35 1.5727 9 3 1 4 58.74 2.88 1.5718 7 5 1 4 59.20 2.39 1.5607 3 5 3 4 59.36 3.75 1.5569 -3 7 1 4 59.57 1.36 1.5519 -4 4 4 4 61.20 1.79 1.5144 -9 3 3 4 61.61 2.95 1.5053 11 1 0 4 61.89 1.03 1.4992 5 1 4 4 62.81 4.36 1.4794 -10 2 3 4 63.14 5.14 1.4725 -7 5 3 4 63.57 3.94 1.4637 2 6 3 4 63.57 3.78 1.4636 6 4 3 4 63.78 1.68 1.4592 7 3 3 4 63.94 4.51 1.4560 8 4 2 4 64.07 2.22 1.4534 1 1 5 4 64.57 2.63 1.4434 7 5 2 4 64.98 2.28 1.4353 0 8 0 2 65.25 3.94 1.4299 6 0 4 2 65.43 1.14 1.4264 1 5 4 4 65.45 3.19 1.4261 10 0 2 2 65.47 1.16 1.4257 2 0 5 2 65.61 4.41 1.4228 3 7 2 4 65.75 1.11 1.4201 -9 5 2 4 66.14 3.43 1.4129 -3 3 5 4 66.20 4.56 1.4116 -5 7 2 4 66.30 2.63 1.4098 -1 3 5 4 66.31 1.06 1.4095 0 8 1 4 66.32 3.32 1.4095 -5 5 4 4 66.47 1.41 1.4065 -11 3 2 4 66.48 3.01 1.4064 5 3 4 4 66.92 2.43 1.3983 -2 8 1 4 67.06 3.05 1.3956 -6 2 5 4 67.07 3.04 1.3955 -12 0 2 2 67.83 2.54 1.3817 2 8 1 4 67.96 2.05 1.3793 9 5 1 4 68.05 1.14 1.3777 -1 7 3 4 68.08 4.51 1.3771 -12 2 1 4 68.52 2.17 1.3694 -9 3 4 4 68.79 1.73 1.3647 -3 7 3 4 69.40 1.60 1.3541 1 7 3 4 69.49 2.19 1.3527 12 2 0 4 69.55 3.66 1.3517 7 7 0 4 70.28 4.04 1.3395 -9 5 3 4 71.60 1.88 1.3179 -5 7 3 4 72.56 1.08 1.3028 -8 6 3 4 73.44 1.62 1.2894 12 2 1 4 73.83 1.54 1.2835 9 5 2 4 74.08 2.06 1.2799 6 4 4 4 74.26 1.97 1.2771 10 4 2 4 74.32 1.73 1.2763 -6 6 4 4 74.36 1.06 1.2757 6 8 0 4 74.79 1.05 1.2694 -2 0 6 2 74.99 6.01 1.2666 11 5 0 4 75.23 1.55 1.2630 -11 5 2 4 75.28 1.40 1.2623 -3 1 6 4 75.79 1.89 1.2551 -12 4 2 4 76.26 2.40 1.2486 11 3 2 4 76.30 1.77 1.2480 -2 8 3 4 76.31 2.16 1.2479 -10 4 4 4 76.32 3.06 1.2477 10 2 3 4 76.60 1.02 1.2439 0 8 3 4 76.77 1.93 1.2415 -1 7 4 4 76.91 3.43 1.2397 -10 0 5 2 76.92 3.72 1.2395 -2 2 6 4 77.00 1.49 1.2384 -9 7 1 4 77.24 3.59 1.2352 1 5 5 4 77.63 2.27 1.2299 -6 0 6 2 78.14 1.13 1.2231 5 7 3 4 78.52 1.76 1.2182 3 9 1 4 79.17 2.03 1.2098 -1 9 2 4 79.97 1.17 1.1997 2 0 6 2 80.25 1.20 1.1962 6 2 5 4 80.60 2.01 1.1919 -7 5 5 4 80.88 1.40 1.1885 -8 8 1 4 81.32 1.45 1.1832 -13 3 3 4 81.36 1.01 1.1826 3 5 5 4 81.92 1.92 1.1760 6 8 2 4 82.06 1.16 1.1744 2 2 6 4 82.65 1.52 1.1674 1 3 6 4 82.87 1.45 1.1649 -8 8 2 4 82.99 1.39 1.1636 -13 1 4 4 84.28 1.45 1.1490 -7 3 6 4 84.35 1.13 1.1482 0 10 0 2 84.78 1.04 1.1435 10 6 2 4 85.28 2.34 1.1381 -10 4 5 4 85.35 1.78 1.1374 7 7 3 4 86.13 1.72 1.1290 -2 10 1 4 87.07 1.88 1.1192 10 2 4 4 87.10 1.05 1.1189 7 3 5 4 87.48 1.55 1.1150 -3 7 5 4 87.54 1.23 1.1144 4 2 6 4 87.63 1.05 1.1135 -1 7 5 4 87.80 1.82 1.1118 5 7 4 4 87.84 1.59 1.1114 -3 5 6 4 89.69 1.15 1.0932 -9 7 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.