H192 N36 O132 P12 Te12 Averbuch-Pouchot M, Schuelke U Zeitschrift fur Anorganische und Allgemeine Chemie 622 (1996) 1997-2002 Preparation and crystal structure of guanidinium cyclododecaphosphate telluric acid hydrate: (C (N H2)2)12 P12 O36. 12Te (O H)6 . 24H2 O _cod_database_code 1008859 _database_code_amcsd 0016725 CELL PARAMETERS: 15.8540 15.8540 51.2600 90.000 90.000 120.000 SPACE GROUP: R-3 X-RAY WAVELENGTH: 1.541838 Cell Volume: 11158.011 Density (g/cm3): 2.152 MAX. ABS. INTENSITY / VOLUME**2: 13.95517037 RIR: 2.112 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.66 1.80 13.2625 1 0 1 6 10.35 45.72 8.5433 0 0 6 2 11.16 91.84 7.9270 1 1 0 6 12.31 2.58 7.1908 1 1 3 6 13.01 3.01 6.8042 0 2 1 6 13.35 2.52 6.6312 2 0 2 6 14.64 1.78 6.0514 0 2 4 6 15.25 6.39 5.8109 1 1 6 6 15.25 14.12 5.8109 2 -1 6 6 15.53 1.27 5.7042 2 0 5 6 15.56 44.38 5.6956 0 0 9 2 19.17 1.46 4.6301 1 2 5 6 19.19 55.03 4.6254 2 -1 9 6 19.39 100.00 4.5767 3 0 0 6 20.09 1.84 4.4208 0 3 3 6 20.09 3.61 4.4208 3 0 3 6 20.79 1.52 4.2717 0 0 12 2 22.03 39.55 4.0343 0 3 6 6 22.03 50.47 4.0343 3 0 6 6 22.04 1.50 4.0327 1 2 8 6 22.43 2.19 3.9635 2 2 0 6 23.04 8.66 3.8610 4 -2 3 6 23.04 8.22 3.8610 2 2 3 6 23.66 8.76 3.7604 2 -1 12 6 24.76 2.37 3.5954 4 -2 6 6 24.76 13.95 3.5954 2 2 6 6 24.96 38.96 3.5676 0 3 9 6 24.96 23.90 3.5676 3 0 9 6 26.08 18.93 3.4173 0 0 15 2 27.42 1.50 3.2533 4 -2 9 6 27.42 8.62 3.2533 2 2 9 6 28.44 2.13 3.1381 1 1 15 6 28.44 1.70 3.1381 2 -1 15 6 28.58 1.11 3.1228 0 3 12 6 29.82 2.76 2.9961 1 4 0 6 30.29 2.61 2.9511 -1 5 3 6 30.29 3.50 2.9511 1 4 3 6 30.29 4.51 2.9511 4 1 3 6 30.77 7.11 2.9055 2 2 12 6 30.77 1.89 2.9055 4 -2 12 6 31.65 2.14 2.8273 -1 5 6 6 31.65 1.22 2.8273 1 4 6 6 31.65 6.60 2.8273 5 -1 6 6 32.70 15.90 2.7382 0 3 15 6 32.70 11.78 2.7382 3 0 15 6 33.80 6.62 2.6516 -1 5 9 6 33.80 1.17 2.6516 1 4 9 6 33.80 2.32 2.6516 4 1 9 6 33.80 1.63 2.6516 5 -1 9 6 33.93 3.20 2.6423 3 3 0 6 34.34 2.17 2.6113 3 3 3 6 34.66 11.60 2.5882 2 2 15 6 35.56 5.44 2.5244 6 -3 6 6 35.56 11.58 2.5244 3 3 6 6 36.64 2.88 2.4529 4 1 12 6 36.64 1.01 2.4529 1 4 12 6 37.52 1.12 2.3969 6 -3 9 6 37.52 7.80 2.3969 3 3 9 6 38.94 1.58 2.3127 2 2 18 6 39.38 5.49 2.2883 6 0 0 6 39.74 2.99 2.2681 0 6 3 6 39.74 1.00 2.2681 6 0 3 6 40.02 10.04 2.2529 -1 5 15 6 40.02 5.28 2.2529 5 -1 15 6 40.82 2.90 2.2104 0 6 6 6 40.82 1.48 2.2104 6 0 6 6 41.05 1.89 2.1986 5 2 0 6 41.95 1.91 2.1538 0 3 21 6 41.95 2.03 2.1538 3 0 21 6 42.46 6.35 2.1292 2 5 6 6 42.46 1.77 2.1292 -2 7 6 6 42.46 2.03 2.1292 5 2 6 6 42.58 2.72 2.1234 0 6 9 6 42.58 1.61 2.1234 6 0 9 6 43.28 4.69 2.0903 6 -3 15 6 43.28 6.92 2.0903 3 3 15 6 43.54 4.55 2.0784 2 2 21 6 43.86 1.05 2.0641 1 4 18 6 43.90 1.23 2.0623 2 -1 24 6 44.16 3.34 2.0510 2 5 9 6 44.16 1.26 2.0510 5 2 9 6 44.94 2.47 2.0171 0 6 12 6 45.79 1.63 1.9818 4 4 0 6 46.11 1.04 1.9686 8 -4 3 6 46.45 1.30 1.9548 -2 7 12 6 46.45 1.50 1.9548 5 2 12 6 46.91 1.80 1.9370 3 3 18 6 46.95 1.95 1.9354 0 3 24 6 46.95 1.72 1.9354 3 0 24 6 47.84 5.37 1.9014 0 6 15 6 47.84 4.63 1.9014 6 0 15 6 48.08 3.85 1.8924 -1 5 21 6 48.08 4.30 1.8924 5 -1 21 6 48.41 1.35 1.8802 4 -2 24 6 48.41 3.30 1.8802 2 2 24 6 49.28 6.96 1.8490 2 5 15 6 49.28 6.85 1.8490 5 2 15 6 50.16 1.41 1.8186 7 1 0 6 50.93 1.76 1.7930 6 -3 21 6 50.93 2.82 1.7930 3 3 21 6 51.37 2.02 1.7787 8 -1 6 6 52.63 4.00 1.7392 -1 5 24 6 52.63 4.46 1.7392 5 -1 24 6 52.85 1.53 1.7324 -1 8 9 6 52.93 3.47 1.7298 3 6 0 6 52.93 4.78 1.7298 6 3 0 6 53.45 2.74 1.7143 8 -4 15 6 54.09 1.33 1.6954 -3 9 6 6 54.09 4.33 1.6954 3 6 6 6 54.09 2.02 1.6954 6 3 6 6 54.09 2.94 1.6954 9 -3 6 6 54.97 1.36 1.6703 1 1 30 6 55.00 1.33 1.6694 0 6 21 6 55.31 1.05 1.6610 6 -3 24 6 55.52 1.85 1.6552 -3 9 9 6 55.52 2.61 1.6552 3 6 9 6 55.52 2.03 1.6552 6 3 9 6 55.52 2.01 1.6552 9 -3 9 6 56.32 3.64 1.6336 2 5 21 6 56.32 2.68 1.6336 5 2 21 6 57.40 2.41 1.6054 -1 8 15 6 57.40 1.79 1.6054 8 -1 15 6 58.85 2.00 1.5691 2 2 30 6 58.85 1.04 1.5691 4 -2 30 6 59.94 1.06 1.5434 3 6 15 6 59.94 1.75 1.5434 -3 9 15 6 59.94 1.72 1.5434 6 3 15 6 60.14 1.45 1.5385 8 -4 21 6 60.43 1.80 1.5320 2 5 24 6 60.43 1.59 1.5320 5 2 24 6 60.63 1.45 1.5273 5 5 9 6 60.71 2.82 1.5256 9 0 0 6 61.77 1.20 1.5018 0 9 6 6 61.77 1.37 1.5018 9 0 6 6 61.94 1.04 1.4981 2 8 0 6 62.58 1.15 1.4843 4 1 30 6 62.58 2.62 1.4843 -1 5 30 6 62.58 2.31 1.4843 5 -1 30 6 63.00 1.26 1.4755 2 8 6 6 63.09 1.66 1.4736 0 9 9 6 63.09 1.67 1.4736 9 0 9 6 63.83 1.62 1.4583 -1 8 21 6 64.10 1.06 1.4527 8 -4 24 6 66.59 1.19 1.4044 11 -4 6 6 66.75 1.10 1.4015 2 -1 36 6 67.20 1.03 1.3930 9 0 15 6 67.66 1.08 1.3846 8 -1 24 6 67.85 1.25 1.3812 -4 11 9 6 68.37 1.19 1.3720 2 8 15 6 69.70 1.23 1.3491 2 5 30 6 69.70 2.17 1.3491 5 2 30 6 69.70 1.01 1.3491 -2 7 30 6 70.24 1.09 1.3400 4 -2 36 6 71.40 2.19 1.3212 6 6 0 6 72.38 1.30 1.3056 12 -6 6 6 73.13 1.63 1.2941 8 -4 30 6 74.79 1.59 1.2693 3 9 0 6 74.79 1.44 1.2693 9 3 0 6 76.50 1.11 1.2453 -1 8 30 6 76.50 1.12 1.2453 8 -1 30 6 86.27 1.27 1.1275 1 1 45 6 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.