Wulfingite Jacobs H, Niemann A, Kockelmann W Zeitschrift fur Anorganische und Allgemeine Chemie 631 (2005) 1247-1254 Low temperature investigations of hydrogen bridge bonds in the hydroxides beta-Be(OH)2 and epsilon-Zn(OH)2 by Raman-spectroscopy as well as X-ray and neutron diffraction Locality: synthetic Sample: T = 120 K _database_code_amcsd 0015825 CELL PARAMETERS: 4.8888 5.1285 8.5029 90.000 90.000 90.000 SPACE GROUP: P2_12_12_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 213.187 Density (g/cm3): 3.097 MAX. ABS. INTENSITY / VOLUME**2: 30.57853945 RIR: 3.215 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 20.22 100.00 4.3916 0 1 1 4 20.89 1.15 4.2515 0 0 2 2 20.96 80.58 4.2382 1 0 1 4 25.17 6.23 3.5386 1 1 0 4 27.25 21.65 3.2731 0 1 2 4 27.30 54.43 3.2670 1 1 1 4 27.81 42.80 3.2081 1 0 2 4 32.93 41.58 2.7198 1 1 2 4 34.99 5.56 2.5643 0 2 0 2 36.21 8.88 2.4807 0 1 3 4 36.60 6.99 2.4551 0 2 1 4 36.65 6.52 2.4520 1 0 3 4 36.77 6.18 2.4444 2 0 0 2 38.31 6.40 2.3492 2 0 1 4 39.69 33.40 2.2708 1 2 0 4 40.79 27.08 2.2122 1 1 3 4 40.90 3.14 2.2066 2 1 0 4 41.14 5.62 2.1940 1 2 1 4 42.32 22.95 2.1358 2 1 1 4 42.53 13.18 2.1257 0 0 4 2 45.27 2.84 2.0030 1 2 2 4 46.36 5.35 1.9585 2 1 2 4 47.83 7.70 1.9015 0 2 3 4 49.22 8.03 1.8511 2 0 3 4 51.57 2.46 1.7722 1 2 3 4 52.56 10.31 1.7411 2 1 3 4 52.85 7.44 1.7322 2 2 1 4 54.77 1.84 1.6760 0 3 1 4 56.32 17.96 1.6335 2 2 2 4 57.06 7.84 1.6142 0 1 5 4 57.08 2.56 1.6137 1 3 0 4 57.37 4.58 1.6062 1 0 5 4 57.45 5.52 1.6040 2 0 4 4 58.16 8.27 1.5861 0 3 2 4 58.19 11.66 1.5854 1 3 1 4 59.52 2.25 1.5531 3 1 0 4 59.57 18.90 1.5519 1 2 4 4 60.39 4.97 1.5328 1 1 5 4 60.47 8.90 1.5309 2 1 4 4 60.61 7.07 1.5278 3 1 1 4 60.88 10.86 1.5216 3 0 2 4 61.46 1.51 1.5087 1 3 2 4 61.81 2.81 1.5009 2 2 3 4 63.80 1.35 1.4588 3 1 2 4 65.91 5.02 1.4172 0 2 5 4 66.14 1.16 1.4127 3 0 3 4 66.70 5.66 1.4023 1 3 3 4 67.80 6.86 1.3823 2 3 1 4 68.72 1.82 1.3660 0 1 6 4 68.95 5.28 1.3620 3 1 3 4 68.99 1.34 1.3612 1 2 5 4 69.07 1.35 1.3599 2 2 4 4 69.19 3.51 1.3577 3 2 1 4 69.83 1.57 1.3470 2 1 5 4 70.82 3.35 1.3305 2 3 2 4 71.75 6.81 1.3156 1 1 6 4 72.19 1.11 1.3086 3 2 2 4 73.92 2.50 1.2821 0 4 0 2 75.74 2.63 1.2559 2 3 3 4 75.87 2.63 1.2540 3 1 4 4 77.08 3.81 1.2374 3 2 3 4 77.83 1.97 1.2272 1 4 1 4 77.92 1.16 1.2261 2 2 5 4 79.17 1.53 1.2098 4 0 1 4 80.56 1.35 1.1924 2 1 6 4 80.71 1.56 1.1906 1 4 2 4 80.85 2.87 1.1889 4 1 0 4 81.42 1.18 1.1820 0 1 7 4 81.62 2.38 1.1795 3 3 0 4 81.68 1.46 1.1789 1 0 7 4 81.80 1.23 1.1774 4 1 1 4 82.38 2.65 1.1706 1 3 5 4 84.48 1.52 1.1468 3 1 5 4 85.46 1.09 1.1362 1 4 3 4 86.47 1.25 1.1254 2 4 1 4 86.77 1.08 1.1223 4 0 3 4 88.37 3.74 1.1061 2 2 6 4 89.20 2.14 1.0979 0 4 4 4 89.22 1.04 1.0978 0 2 7 4 89.36 1.37 1.0964 4 1 3 4 89.92 1.82 1.0910 0 3 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.