Wulfingite Jacobs H, Niemann A, Kockelmann W Zeitschrift fur Anorganische und Allgemeine Chemie 631 (2005) 1247-1254 Low temperature investigations of hydrogen bridge bonds in the hydroxides beta-Be(OH)2 and epsilon-Zn(OH)2 by Raman-spectroscopy as well as X-ray and neutron diffraction Locality: synthetic Sample: T = 50 K _database_code_amcsd 0015826 CELL PARAMETERS: 4.8863 5.1261 8.5066 90.000 90.000 90.000 SPACE GROUP: P2_12_12_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 213.068 Density (g/cm3): 3.099 MAX. ABS. INTENSITY / VOLUME**2: 30.66702759 RIR: 3.222 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 20.23 100.00 4.3905 0 1 1 4 20.89 1.12 4.2533 0 0 2 2 20.97 80.29 4.2370 1 0 1 4 25.18 6.28 3.5369 1 1 0 4 27.24 21.84 3.2733 0 1 2 4 27.31 55.15 3.2658 1 1 1 4 27.81 43.03 3.2081 1 0 2 4 32.94 41.96 2.7195 1 1 2 4 35.01 5.47 2.5630 0 2 0 2 36.20 8.92 2.4812 0 1 3 4 36.62 7.03 2.4541 0 2 1 4 36.64 6.70 2.4525 1 0 3 4 36.79 6.25 2.4431 2 0 0 2 38.33 6.48 2.3482 2 0 1 4 39.71 34.01 2.2697 1 2 0 4 40.79 27.57 2.2123 1 1 3 4 40.92 3.19 2.2054 2 1 0 4 41.16 5.64 2.1930 1 2 1 4 42.34 23.43 2.1349 2 1 1 4 42.51 13.44 2.1267 0 0 4 2 45.29 2.87 2.0025 1 2 2 4 46.38 5.50 1.9579 2 1 2 4 47.84 7.98 1.9014 0 2 3 4 49.23 8.13 1.8509 2 0 3 4 51.58 2.50 1.7720 1 2 3 4 52.57 10.65 1.7409 2 1 3 4 52.88 7.68 1.7314 2 2 1 4 54.80 1.95 1.6752 0 3 1 4 56.34 18.55 1.6329 2 2 2 4 57.04 8.17 1.6147 0 1 5 4 57.11 2.66 1.6129 1 3 0 4 57.35 4.68 1.6067 1 0 5 4 57.45 5.76 1.6041 2 0 4 4 58.18 8.54 1.5855 0 3 2 4 58.22 12.02 1.5847 1 3 1 4 59.56 2.31 1.5523 3 1 0 4 59.57 19.67 1.5519 1 2 4 4 60.37 5.23 1.5332 1 1 5 4 60.47 9.18 1.5309 2 1 4 4 60.64 7.34 1.5271 3 1 1 4 60.91 11.25 1.5210 3 0 2 4 61.48 1.58 1.5081 1 3 2 4 61.83 2.90 1.5005 2 2 3 4 63.83 1.41 1.4582 3 1 2 4 65.90 5.21 1.4175 0 2 5 4 66.17 1.22 1.4123 3 0 3 4 66.72 5.87 1.4020 1 3 3 4 67.83 7.13 1.3816 2 3 1 4 68.69 1.91 1.3665 0 1 6 4 68.97 5.51 1.3616 3 1 3 4 68.98 1.40 1.3613 1 2 5 4 69.08 1.44 1.3597 2 2 4 4 69.23 3.68 1.3571 3 2 1 4 69.82 1.65 1.3471 2 1 5 4 70.85 3.50 1.3300 2 3 2 4 71.72 7.13 1.3160 1 1 6 4 72.22 1.13 1.3080 3 2 2 4 73.96 2.66 1.2815 0 4 0 2 75.76 2.77 1.2555 2 3 3 4 75.88 2.79 1.2538 3 1 4 4 77.11 4.01 1.2370 3 2 3 4 77.88 2.10 1.2266 1 4 1 4 77.92 1.22 1.2261 2 2 5 4 79.22 1.62 1.2092 4 0 1 4 80.54 1.44 1.1926 2 1 6 4 80.75 1.67 1.1901 1 4 2 4 80.90 3.06 1.1883 4 1 0 4 81.38 1.24 1.1825 0 1 7 4 81.64 1.58 1.1793 1 0 7 4 81.67 2.51 1.1790 3 3 0 4 81.85 1.30 1.1769 4 1 1 4 82.39 2.84 1.1705 1 3 5 4 82.62 1.07 1.1678 0 4 3 4 84.49 1.59 1.1467 3 1 5 4 85.49 1.18 1.1358 1 4 3 4 86.52 1.35 1.1249 2 4 1 4 86.81 1.15 1.1219 4 0 3 4 88.36 4.03 1.1062 2 2 6 4 89.19 1.14 1.0981 0 2 7 4 89.23 2.33 1.0976 0 4 4 4 89.41 1.50 1.0959 4 1 3 4 89.91 1.94 1.0911 0 3 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.