Wulfingite Jacobs H, Niemann A, Kockelmann W Zeitschrift fur Anorganische und Allgemeine Chemie 631 (2005) 1247-1254 Low temperature investigations of hydrogen bridge bonds in the hydroxides beta-Be(OH)2 and epsilon-Zn(OH)2 by Raman-spectroscopy as well as X-ray and neutron diffraction Locality: synthetic Sample: T = 5 K _database_code_amcsd 0015827 CELL PARAMETERS: 4.8856 5.1256 8.5070 90.000 90.000 90.000 SPACE GROUP: P2_12_12_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 213.033 Density (g/cm3): 3.099 MAX. ABS. INTENSITY / VOLUME**2: 30.64658547 RIR: 3.220 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 20.23 100.00 4.3903 0 1 1 4 20.88 1.13 4.2535 0 0 2 2 20.97 80.47 4.2367 1 0 1 4 25.18 6.24 3.5365 1 1 0 4 27.24 21.92 3.2732 0 1 2 4 27.31 55.47 3.2655 1 1 1 4 27.81 42.89 3.2081 1 0 2 4 32.94 42.20 2.7193 1 1 2 4 35.01 5.41 2.5628 0 2 0 2 36.20 8.98 2.4813 0 1 3 4 36.62 7.09 2.4539 0 2 1 4 36.64 6.76 2.4525 1 0 3 4 36.79 6.33 2.4428 2 0 0 2 38.34 6.44 2.3479 2 0 1 4 39.72 34.30 2.2695 1 2 0 4 40.79 27.69 2.2123 1 1 3 4 40.92 3.17 2.2052 2 1 0 4 41.17 5.61 2.1928 1 2 1 4 42.34 23.57 2.1346 2 1 1 4 42.51 13.51 2.1268 0 0 4 2 45.29 2.84 2.0023 1 2 2 4 46.38 5.61 1.9577 2 1 2 4 47.84 8.04 1.9014 0 2 3 4 49.23 8.11 1.8508 2 0 3 4 51.58 2.51 1.7719 1 2 3 4 52.57 10.77 1.7408 2 1 3 4 52.89 7.80 1.7312 2 2 1 4 54.80 2.00 1.6751 0 3 1 4 56.35 18.67 1.6328 2 2 2 4 57.03 8.22 1.6148 0 1 5 4 57.11 2.66 1.6128 1 3 0 4 57.34 4.72 1.6068 1 0 5 4 57.45 5.87 1.6040 2 0 4 4 58.19 8.59 1.5854 0 3 2 4 58.22 12.10 1.5846 1 3 1 4 59.56 2.33 1.5521 3 1 0 4 59.57 19.91 1.5519 1 2 4 4 60.37 5.31 1.5332 1 1 5 4 60.48 9.19 1.5308 2 1 4 4 60.65 7.39 1.5269 3 1 1 4 60.91 11.32 1.5209 3 0 2 4 61.49 1.62 1.5080 1 3 2 4 61.83 2.94 1.5004 2 2 3 4 63.84 1.46 1.4581 3 1 2 4 65.89 5.27 1.4175 0 2 5 4 66.17 1.26 1.4122 3 0 3 4 66.72 5.93 1.4019 1 3 3 4 67.84 7.15 1.3815 2 3 1 4 68.69 1.94 1.3665 0 1 6 4 68.98 5.54 1.3615 3 1 3 4 68.98 1.40 1.3613 1 2 5 4 69.08 1.45 1.3597 2 2 4 4 69.24 3.72 1.3569 3 2 1 4 69.82 1.67 1.3471 2 1 5 4 70.86 3.58 1.3299 2 3 2 4 71.72 7.20 1.3160 1 1 6 4 72.23 1.12 1.3079 3 2 2 4 73.97 2.71 1.2814 0 4 0 2 75.77 2.79 1.2554 2 3 3 4 75.89 2.83 1.2537 3 1 4 4 77.11 4.06 1.2369 3 2 3 4 77.88 2.14 1.2265 1 4 1 4 77.92 1.24 1.2260 2 2 5 4 79.23 1.66 1.2090 4 0 1 4 80.54 1.47 1.1926 2 1 6 4 80.76 1.69 1.1900 1 4 2 4 80.91 3.11 1.1881 4 1 0 4 81.38 1.25 1.1825 0 1 7 4 81.64 1.61 1.1793 1 0 7 4 81.68 2.54 1.1788 3 3 0 4 81.86 1.32 1.1767 4 1 1 4 82.39 2.89 1.1705 1 3 5 4 82.63 1.08 1.1677 0 4 3 4 84.49 1.61 1.1467 3 1 5 4 85.50 1.21 1.1357 1 4 3 4 86.53 1.37 1.1248 2 4 1 4 86.82 1.17 1.1218 4 0 3 4 88.36 4.08 1.1062 2 2 6 4 89.18 1.16 1.0981 0 2 7 4 89.24 2.39 1.0976 0 4 4 4 89.42 1.53 1.0958 4 1 3 4 89.91 1.97 1.0911 0 3 6 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.