data_global _chemical_name_mineral 'Sulfur' loop_ _publ_author_name 'Steudel R' 'Steidel J' 'Reinhardt R' _journal_name_full 'Zeitschrift fur Naturforschung' _journal_volume B38 _journal_year 1983 _journal_page_first 1548 _journal_page_last 1556 _publ_section_title ; X-ray structural analyses of cyclodecasulfur (S10) and of a cyclohexasulfur-cyclodecasulfur molecular addition compound (S6*S10) Sample: at T = 163 K ; _database_code_amcsd 0015839 _chemical_compound_source 'Synthetic' _chemical_formula_sum 'S5' _cell_length_a 12.533 _cell_length_b 10.275 _cell_length_c 12.776 _cell_angle_alpha 90 _cell_angle_beta 37.98 _cell_angle_gamma 90 _cell_volume 1012.464 _exptl_crystal_density_diffrn 2.104 _symmetry_space_group_name_H-M 'C 1 2/c 1' loop_ _space_group_symop_operation_xyz 'x,y,z' '1/2+x,1/2+y,z' 'x,-y,1/2+z' '1/2+x,1/2-y,1/2+z' '-x,y,1/2-z' '1/2-x,1/2+y,1/2-z' '-x,-y,-z' '1/2-x,1/2-y,-z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z S1 0.59590 0.28780 0.73080 S2 0.76090 0.44010 0.56400 S3 0.76570 0.55170 0.69310 S4 0.54570 0.66270 0.87260 S5 0.59470 0.81440 0.73210 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1 0.02540 0.01940 0.03260 -0.00070 -0.02360 0.00360 S2 0.02180 0.02010 0.02890 -0.00010 -0.01820 -0.00060 S3 0.02640 0.02530 0.04370 0.00340 -0.02970 -0.00440 S4 0.02630 0.03140 0.02670 0.00460 -0.02160 -0.00310 S5 0.02630 0.02090 0.03550 -0.00300 -0.02510 0.00030