Rosickyite Steudel R, Steidel J, Reinhardt R Zeitschrift fur Naturforschung B38 (1983) 1548-1556 X-ray structural analyses of cyclodecasulfur (S10) and of a cyclohexasulfur-cyclodecasulfur molecular addition compound (S6*S10) Locality: synthetic Sample: at T = 163 K _database_code_amcsd 0015841 CELL PARAMETERS: 12.5330 10.2750 12.7760 90.000 37.980 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 1012.464 Density (g/cm3): 2.103 MAX. ABS. INTENSITY / VOLUME**2: 8.323938867 RIR: 1.289 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.35 2.15 7.7938 1 1 1 4 14.36 3.53 6.1683 1 1 0 4 14.81 4.35 5.9800 2 0 2 2 17.26 6.59 5.1375 0 2 0 2 17.51 46.64 5.0638 1 1 2 4 20.65 1.78 4.3007 0 2 1 4 22.62 50.63 3.9311 0 0 2 2 22.82 20.37 3.8969 2 2 2 4 23.06 1.85 3.8563 2 0 0 2 23.27 19.49 3.8220 -1 1 1 4 23.42 8.00 3.7983 2 2 1 4 23.45 53.61 3.7933 3 1 2 4 23.94 27.04 3.7167 3 1 3 4 27.33 2.44 3.2636 1 1 3 4 27.45 100.00 3.2488 2 2 3 4 28.52 7.92 3.1302 1 3 0 4 28.59 25.94 3.1220 0 2 2 4 28.95 70.62 3.0841 2 2 0 4 29.30 1.36 3.0480 3 1 4 4 29.88 4.92 2.9900 4 0 4 2 30.28 13.71 2.9518 1 3 2 4 30.73 1.05 2.9098 2 0 4 2 31.72 10.39 2.8205 4 0 2 2 33.59 5.16 2.6679 4 2 3 4 33.90 11.06 2.6445 -1 1 2 4 34.05 5.14 2.6331 -1 3 1 4 34.52 3.61 2.5979 3 3 3 4 34.71 5.76 2.5842 4 2 4 4 35.45 5.06 2.5319 2 2 4 4 36.01 3.93 2.4940 3 1 0 4 36.34 15.88 2.4724 4 2 2 4 36.81 15.72 2.4417 0 4 1 4 37.03 8.46 2.4278 1 3 3 4 37.60 1.98 2.3923 3 3 1 4 37.66 1.60 2.3888 3 1 5 4 38.31 2.09 2.3496 1 1 4 4 38.56 1.96 2.3350 3 3 4 4 38.56 2.76 2.3345 0 2 3 4 38.65 5.07 2.3297 5 1 5 4 42.02 1.43 2.1504 0 4 2 4 42.27 2.06 2.1380 -1 3 2 4 42.27 1.24 2.1379 2 4 0 4 42.30 1.29 2.1366 4 2 1 4 43.14 2.69 2.0969 4 0 6 2 43.62 10.33 2.0752 5 1 6 4 43.84 1.32 2.0651 5 1 2 4 43.98 1.47 2.0587 -2 0 2 2 44.39 6.17 2.0408 6 0 4 2 44.75 8.17 2.0253 1 5 1 4 45.33 1.70 2.0005 -1 1 3 4 45.44 3.58 1.9959 3 3 5 4 45.50 4.52 1.9933 6 0 6 2 45.74 6.74 1.9836 4 4 3 4 45.82 1.26 1.9805 -3 1 1 4 46.00 4.31 1.9729 1 3 4 4 46.30 3.08 1.9611 5 3 5 4 47.01 9.39 1.9331 6 2 5 4 47.20 1.49 1.9257 2 4 4 4 47.71 2.33 1.9062 3 1 6 4 47.97 3.59 1.8967 6 2 4 4 48.78 1.44 1.8667 -2 4 1 4 49.58 1.63 1.8387 -1 5 1 4 49.66 1.36 1.8358 0 2 4 4 49.70 23.30 1.8345 0 4 3 4 50.40 2.62 1.8107 4 4 5 4 50.56 9.54 1.8052 4 2 0 4 50.86 2.48 1.7953 5 3 2 4 51.82 1.77 1.7644 1 5 3 4 52.20 1.27 1.7524 -1 3 3 4 52.25 1.09 1.7507 3 5 1 4 53.23 2.08 1.7209 2 0 6 2 53.75 4.99 1.7053 6 2 7 4 54.35 2.20 1.6879 3 3 6 4 54.87 1.72 1.6733 0 6 1 4 54.93 7.63 1.6715 6 0 2 2 55.37 7.64 1.6592 2 4 5 4 56.13 1.89 1.6387 2 6 1 4 56.39 4.00 1.6318 2 2 6 4 56.46 2.83 1.6297 1 3 5 4 56.85 4.62 1.6195 6 4 5 4 56.87 3.28 1.6191 -3 1 2 4 57.70 1.48 1.5978 5 3 1 4 58.03 2.11 1.5895 6 2 2 4 58.19 5.00 1.5854 2 6 3 4 58.32 1.60 1.5822 7 -3 6 4 58.57 3.13 1.5761 3 5 5 4 58.62 1.27 1.5748 6 4 6 4 58.64 1.41 1.5743 7 -3 5 4 59.02 3.74 1.5651 2 6 0 4 59.19 1.06 1.5610 0 4 4 4 59.28 2.63 1.5588 5 5 5 4 59.37 3.61 1.5566 5 5 3 4 60.50 3.68 1.5303 -4 2 1 4 61.07 7.77 1.5173 6 4 3 4 61.69 4.40 1.5036 0 2 5 4 61.79 4.26 1.5014 4 6 3 4 62.49 1.30 1.4863 1 1 6 4 62.86 2.40 1.4784 6 4 7 4 63.56 1.07 1.4638 4 6 2 4 64.36 1.21 1.4476 -1 5 3 4 65.59 2.06 1.4233 1 7 2 4 67.71 1.27 1.3839 4 6 1 4 67.78 1.11 1.3826 -1 7 1 4 69.06 1.35 1.3600 -4 4 1 4 73.70 2.58 1.2854 6 0 0 2 73.77 2.27 1.2844 0 8 0 2 74.92 1.36 1.2676 0 8 1 4 83.46 1.14 1.1582 0 6 5 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.