Linekite Hughes Kubatko K A, Burns P C The Canadian Mineralogist 42 (2004) 997-1003 The crystal structure of a novel uranyl tricarbonate, K2Ca3[(UO2)(CO3)3]2(H2O)6 Locality: synthetic _database_code_amcsd 0019771 CELL PARAMETERS: 17.0150 18.0480 18.3940 90.000 90.000 90.000 SPACE GROUP: Pnnm X-RAY WAVELENGTH: 1.541838 Cell Volume: 5648.553 Density (g/cm3): 2.847 MAX. ABS. INTENSITY / VOLUME**2: 40.66927559 RIR: 4.651 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.62 2.39 9.1970 0 0 2 2 10.40 100.00 8.5075 2 0 0 2 13.75 65.38 6.4412 0 2 2 4 14.18 3.70 6.2453 2 0 2 4 14.31 1.32 6.1903 2 2 0 4 14.71 1.62 6.0240 1 2 2 8 15.01 16.05 5.9019 2 1 2 8 15.50 1.13 5.7179 0 3 1 4 16.13 9.98 5.4945 1 1 3 8 16.35 6.15 5.4201 1 3 1 8 16.35 1.87 5.4199 3 0 1 4 17.27 99.62 5.1354 2 2 2 8 18.06 8.96 4.9120 2 3 0 4 19.30 22.21 4.5985 0 0 4 2 19.68 17.73 4.5120 0 4 0 2 20.50 1.72 4.3327 2 3 2 8 20.88 3.63 4.2537 4 0 0 2 21.46 2.21 4.1403 4 1 0 4 21.91 1.56 4.0570 3 1 3 8 21.97 21.54 4.0454 2 0 4 4 22.07 2.51 4.0267 3 3 1 8 22.30 21.31 3.9861 2 4 0 4 22.52 5.92 3.9474 2 1 4 8 23.04 3.01 3.8608 4 0 2 4 23.53 5.33 3.7805 3 2 3 8 23.56 3.46 3.7754 4 1 2 8 25.09 20.93 3.5496 4 2 2 8 25.26 3.28 3.5264 1 1 5 8 25.65 10.22 3.4732 4 3 0 4 25.69 1.19 3.4677 1 5 1 8 25.69 3.03 3.4676 3 4 1 8 26.64 1.74 3.3462 5 0 1 4 27.45 2.05 3.2492 4 3 2 8 27.70 7.54 3.2206 0 4 4 4 28.59 4.55 3.1226 4 0 4 4 28.85 8.78 3.0951 4 4 0 4 28.93 2.79 3.0864 1 3 5 8 29.02 5.41 3.0769 4 1 4 8 29.13 1.98 3.0657 0 0 6 2 29.19 5.19 3.0599 1 5 3 8 29.66 8.18 3.0120 2 4 4 8 29.70 3.28 3.0080 0 6 0 2 29.74 1.06 3.0043 3 5 1 8 30.61 1.20 2.9203 3 2 5 8 30.80 7.88 2.9027 0 2 6 4 31.29 7.88 2.8590 0 6 2 4 31.41 3.43 2.8480 2 1 6 8 31.66 5.65 2.8258 5 2 3 8 31.74 1.94 2.8194 1 6 2 8 31.82 1.32 2.8120 1 4 5 8 31.95 1.65 2.8015 6 1 0 4 32.30 1.44 2.7715 4 3 4 8 32.59 10.63 2.7472 2 2 6 8 32.84 2.03 2.7273 3 5 3 8 33.05 11.06 2.7100 2 6 2 8 33.06 1.54 2.7099 6 0 2 4 33.27 1.11 2.6933 2 5 4 8 33.34 2.09 2.6877 5 4 1 8 33.44 2.25 2.6799 6 1 2 8 33.60 2.59 2.6671 5 3 3 8 34.00 2.62 2.6367 4 5 2 8 34.56 2.25 2.5954 6 2 2 8 34.91 1.07 2.5705 1 1 7 8 34.94 10.10 2.5677 4 4 4 8 34.98 2.14 2.5651 6 3 0 4 35.23 1.62 2.5474 3 4 5 8 35.55 1.95 2.5251 1 7 1 8 35.95 2.16 2.4981 5 0 5 4 35.99 1.28 2.4956 1 2 7 8 36.11 1.38 2.4871 4 0 6 4 36.36 2.68 2.4708 6 3 2 8 36.62 1.62 2.4540 5 5 1 8 36.86 1.45 2.4382 3 6 3 8 37.25 1.47 2.4138 6 0 4 4 37.46 1.74 2.4010 6 4 0 4 37.51 3.67 2.3977 4 2 6 8 37.60 1.24 2.3925 6 1 4 8 37.66 1.14 2.3886 7 1 1 8 37.92 4.35 2.3728 4 6 2 8 38.07 4.26 2.3637 3 1 7 8 38.61 1.00 2.3318 6 2 4 8 38.76 1.16 2.3231 6 4 2 8 39.08 3.93 2.3052 3 2 7 8 39.18 1.20 2.2992 0 0 8 2 39.96 1.03 2.2560 0 8 0 2 40.26 1.62 2.2402 6 3 4 8 40.65 1.23 2.2196 2 0 8 4 40.93 3.50 2.2049 4 7 0 4 41.18 2.06 2.1919 7 2 3 8 41.31 3.32 2.1855 5 4 5 8 41.41 1.18 2.1806 2 8 0 4 41.46 1.15 2.1781 4 4 6 8 41.68 2.28 2.1672 6 5 2 8 41.91 1.82 2.1554 2 2 8 8 42.08 1.29 2.1471 0 6 6 4 42.14 1.35 2.1441 4 7 2 8 42.53 1.42 2.1256 7 4 1 8 42.75 1.31 2.1154 5 6 3 8 42.81 1.28 2.1123 8 1 0 4 42.90 3.33 2.1080 1 5 7 8 43.18 2.54 2.0953 1 7 5 8 43.47 2.88 2.0818 2 6 6 8 43.68 1.03 2.0722 8 0 2 4 43.73 1.18 2.0702 8 2 0 4 43.77 1.70 2.0680 6 1 6 8 43.88 1.13 2.0634 6 6 0 4 43.98 1.81 2.0587 8 1 2 8 44.21 1.45 2.0486 0 4 8 4 44.22 1.02 2.0480 4 5 6 8 44.35 2.73 2.0424 5 7 1 8 44.68 2.76 2.0280 7 0 5 4 44.71 5.47 2.0267 5 2 7 8 44.75 1.11 2.0254 0 8 4 4 44.81 1.92 2.0227 4 0 8 4 45.10 1.42 2.0101 4 1 8 8 45.24 1.23 2.0042 7 5 1 8 45.51 1.78 1.9930 4 8 0 4 45.54 2.08 1.9917 2 4 8 8 45.60 3.67 1.9894 3 5 7 8 45.63 1.61 1.9882 4 7 4 8 45.98 1.57 1.9737 4 2 8 8 46.07 2.96 1.9703 2 8 4 8 47.27 2.93 1.9228 1 3 9 8 47.27 1.09 1.9228 3 0 9 4 47.36 1.03 1.9194 8 1 4 8 47.43 1.07 1.9167 4 6 6 8 47.67 2.25 1.9077 6 7 0 4 48.03 1.28 1.8941 1 9 3 8 48.21 1.68 1.8877 8 2 4 8 48.33 1.58 1.8831 8 4 2 8 48.40 1.02 1.8807 3 9 1 8 48.40 1.18 1.8806 9 0 1 4 49.26 2.41 1.8498 7 4 5 8 49.38 1.27 1.8457 4 4 8 8 49.60 1.50 1.8381 8 3 4 8 49.79 1.07 1.8315 3 3 9 8 49.87 1.34 1.8287 4 8 4 8 50.08 1.45 1.8213 3 8 5 8 50.52 1.01 1.8067 3 9 3 8 50.62 1.37 1.8033 6 5 6 8 50.81 1.56 1.7971 8 5 2 8 50.90 1.12 1.7941 5 7 5 8 51.34 1.56 1.7796 4 9 2 8 51.59 1.16 1.7715 9 2 3 8 51.68 2.00 1.7688 3 4 9 8 51.70 1.39 1.7681 7 5 5 8 51.85 1.47 1.7632 2 2 10 8 51.89 1.64 1.7621 6 7 4 8 52.21 2.78 1.7521 5 0 9 4 52.21 1.29 1.7520 6 2 8 8 52.26 2.59 1.7505 7 2 7 8 52.73 1.15 1.7359 9 4 1 8 52.80 1.37 1.7339 2 10 2 8 53.57 1.32 1.7107 5 6 7 8 54.58 1.13 1.6815 9 0 5 4 54.83 1.02 1.6743 5 8 5 8 54.87 1.30 1.6731 10 0 2 4 56.33 1.40 1.6333 5 4 9 8 56.58 1.02 1.6268 1 11 1 8 57.14 1.45 1.6120 6 9 2 8 57.82 2.73 1.5946 1 7 9 8 58.12 1.52 1.5872 1 9 7 8 58.59 1.02 1.5756 9 4 5 8 58.87 1.13 1.5687 10 4 2 8 59.05 1.36 1.5643 7 0 9 4 59.85 1.05 1.5453 8 7 4 8 60.31 1.34 1.5347 3 9 7 8 60.31 1.34 1.5347 7 6 7 8 61.27 1.47 1.5129 9 2 7 8 62.19 1.11 1.4927 1 11 5 8 62.76 1.23 1.4804 5 2 11 8 62.88 1.22 1.4780 7 4 9 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.