B2 Na3 O6 Y Zhang Y, Chen X, Liang J, Xu T Journal of Alloys and Compounds 333 (2002) 72-75 Synthesis and structural study of new rarte earth sodium borates of Na3Ln(BO2)3(Ln=Y,Gd) _cod_database_code 1100065 _database_code_amcsd 0018244 CELL PARAMETERS: 6.5050 8.5172 12.0213 90.000 118.720 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 584.096 Density (g/cm3): 3.132 MAX. ABS. INTENSITY / VOLUME**2: 8.022733008 RIR: 0.834 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.36 39.95 6.6252 0 1 1 4 15.53 100.00 5.7047 1 0 0 2 16.53 80.72 5.3638 -1 0 2 2 16.82 19.80 5.2712 0 0 2 2 17.18 2.82 5.1619 -1 1 1 4 18.72 14.34 4.7398 1 1 0 4 19.56 19.85 4.5388 -1 1 2 4 19.81 38.82 4.4822 0 1 2 4 22.52 81.98 3.9486 0 2 1 4 23.45 21.81 3.7935 1 1 1 4 24.79 2.44 3.5910 -1 1 3 4 25.01 44.41 3.5604 -1 2 1 4 26.11 2.60 3.4126 1 2 0 4 27.46 33.50 3.2485 0 1 3 4 27.49 77.85 3.2448 -2 0 2 2 29.46 19.86 3.0322 -2 1 2 4 29.73 8.57 3.0047 -1 0 4 2 29.74 5.19 3.0036 1 2 1 4 29.97 6.84 2.9819 1 1 2 4 30.14 1.61 2.9652 -2 1 1 4 30.83 8.12 2.9000 -1 2 3 4 31.58 8.26 2.8335 -1 1 4 4 32.67 10.46 2.7414 0 3 1 4 33.05 3.08 2.7105 0 2 3 4 33.12 59.37 2.7047 2 1 0 4 33.41 8.24 2.6819 -2 0 4 2 34.02 15.55 2.6356 0 0 4 2 34.48 1.04 2.6010 -1 3 1 4 34.76 35.77 2.5810 -2 2 2 4 35.08 33.20 2.5581 -2 1 4 4 35.20 1.07 2.5498 1 2 2 4 35.31 3.54 2.5417 1 3 0 4 35.35 19.85 2.5393 -2 2 1 4 35.66 48.34 2.5178 0 1 4 4 35.78 5.06 2.5093 -1 3 2 4 35.93 51.07 2.4996 0 3 2 4 36.29 20.41 2.4758 -2 2 3 4 36.60 1.01 2.4551 -1 2 4 4 37.45 6.81 2.4013 1 1 3 4 37.92 1.99 2.3725 2 1 1 4 37.97 2.85 2.3699 2 2 0 4 38.16 5.46 2.3585 1 3 1 4 39.04 2.68 2.3074 -1 3 3 4 39.22 16.20 2.2969 -1 1 5 4 39.72 1.50 2.2694 -2 2 4 4 40.53 2.02 2.2259 -2 1 5 4 40.86 46.33 2.2084 0 3 3 4 41.87 18.82 2.1577 1 2 3 4 42.06 11.80 2.1484 -3 0 2 2 42.30 7.69 2.1368 2 2 1 4 42.45 10.80 2.1293 0 4 0 2 42.67 8.61 2.1188 1 3 2 4 42.68 1.34 2.1185 2 0 2 2 43.27 22.86 2.0908 -3 0 4 2 43.44 9.21 2.0831 -3 1 2 4 43.49 16.33 2.0811 -1 2 5 4 43.60 3.64 2.0758 -2 3 3 4 44.24 2.97 2.0472 1 0 4 2 44.25 17.40 2.0467 0 1 5 4 44.80 1.05 2.0232 -1 4 1 4 45.05 3.33 2.0122 2 3 0 4 45.47 16.00 1.9949 1 4 0 4 45.48 7.93 1.9945 -3 1 1 4 45.57 18.30 1.9905 1 1 4 4 45.85 27.17 1.9791 -1 4 2 4 45.97 12.98 1.9743 0 4 2 4 46.59 3.09 1.9496 -2 3 4 4 47.05 5.23 1.9316 0 3 4 4 47.12 2.06 1.9286 -2 1 6 4 47.12 18.17 1.9286 -3 2 3 4 47.74 4.13 1.9050 -3 1 5 4 47.81 4.00 1.9026 1 4 1 4 47.96 1.31 1.8967 2 2 2 4 48.16 18.31 1.8896 0 2 5 4 48.49 2.49 1.8774 1 3 3 4 48.50 2.43 1.8768 -3 2 4 4 48.87 11.92 1.8636 2 3 1 4 49.09 8.84 1.8559 3 1 0 4 49.30 1.21 1.8482 -3 2 1 4 49.39 1.21 1.8451 1 2 4 4 49.94 8.62 1.8263 -1 3 5 4 50.09 1.16 1.8211 0 4 3 4 50.85 6.19 1.7955 -2 2 6 4 51.02 9.06 1.7900 -2 3 5 4 51.15 5.37 1.7859 2 1 3 4 51.32 20.29 1.7802 -2 4 2 4 51.44 9.58 1.7763 -3 2 5 4 52.05 3.98 1.7571 0 0 6 2 52.28 1.89 1.7498 -3 1 6 4 52.45 3.23 1.7446 -2 4 3 4 53.23 1.83 1.7208 0 1 6 4 53.49 1.05 1.7132 -3 3 2 4 53.72 1.88 1.7063 2 4 0 4 54.01 5.31 1.6979 2 3 2 4 54.04 3.57 1.6969 3 1 1 4 54.59 9.07 1.6811 -2 1 7 4 54.68 8.19 1.6786 2 2 3 4 55.07 5.77 1.6676 -2 4 4 4 55.24 3.86 1.6628 -3 3 1 4 55.33 1.22 1.6605 1 3 4 4 55.76 1.62 1.6485 -3 2 6 4 56.37 4.08 1.6322 1 5 0 4 56.68 6.17 1.6241 -2 3 6 4 56.70 3.68 1.6235 -1 5 2 4 56.74 15.02 1.6224 -4 0 4 2 56.76 2.15 1.6218 1 4 3 4 56.80 1.06 1.6209 0 5 2 4 56.98 8.40 1.6162 -1 3 6 4 57.11 5.55 1.6128 2 4 1 4 57.22 2.73 1.6099 -3 3 5 4 57.45 9.96 1.6041 3 2 1 4 57.62 6.79 1.5998 1 2 5 4 57.86 1.10 1.5937 -4 1 4 4 57.94 3.71 1.5917 2 0 4 2 57.98 5.23 1.5907 -2 2 7 4 58.01 9.72 1.5898 -3 1 7 4 58.35 2.68 1.5816 -4 0 2 2 58.39 1.33 1.5805 1 5 1 4 58.41 3.83 1.5799 3 3 0 4 59.03 1.47 1.5648 -1 5 3 4 59.03 5.53 1.5648 3 0 2 2 59.55 1.77 1.5525 -1 2 7 4 60.12 1.69 1.5390 3 1 2 4 60.39 1.98 1.5328 0 5 3 4 60.89 2.01 1.5214 -4 0 6 2 61.20 1.93 1.5145 -4 2 3 4 61.27 1.38 1.5129 -3 3 6 4 61.29 3.87 1.5123 -3 4 2 4 61.75 2.88 1.5023 -2 0 8 2 61.77 2.87 1.5019 1 5 2 4 61.77 2.87 1.5018 2 4 2 4 61.86 1.25 1.4998 -2 5 1 4 62.23 8.35 1.4919 -3 4 4 4 62.27 1.48 1.4910 2 2 4 4 62.45 1.06 1.4872 -4 2 5 4 62.48 1.94 1.4864 -2 5 3 4 62.70 3.02 1.4819 -1 5 4 4 62.86 2.58 1.4784 3 3 1 4 62.99 2.21 1.4758 1 4 4 4 63.36 1.93 1.4678 -2 3 7 4 63.38 1.29 1.4676 1 1 6 4 64.47 2.95 1.4453 -1 0 8 2 64.77 7.66 1.4394 -3 1 8 4 65.21 1.51 1.4306 0 5 4 4 65.44 2.74 1.4262 4 0 0 2 65.77 8.08 1.4199 0 2 7 4 66.36 4.16 1.4086 -4 3 4 4 66.38 1.96 1.4082 1 5 3 4 66.43 1.81 1.4073 -4 3 3 4 66.46 5.61 1.4068 0 6 1 4 66.47 3.30 1.4066 4 1 0 4 66.51 3.15 1.4059 -3 3 7 4 66.70 1.80 1.4024 2 5 1 4 67.55 2.77 1.3867 -1 6 1 4 67.65 1.31 1.3848 2 1 5 4 67.83 6.19 1.3816 -4 3 2 4 68.46 3.18 1.3704 3 3 2 4 68.48 4.57 1.3702 -2 5 5 4 68.57 1.11 1.3686 -1 2 8 4 69.03 1.29 1.3606 -4 2 7 4 69.34 3.15 1.3552 0 4 6 4 70.21 1.84 1.3405 3 2 3 4 70.47 1.33 1.3363 -1 6 3 4 70.52 1.75 1.3354 -4 3 1 4 70.56 3.16 1.3348 -3 5 2 4 70.67 1.45 1.3330 2 2 5 4 71.00 2.89 1.3275 2 5 2 4 71.16 2.18 1.3250 0 5 5 4 71.18 1.17 1.3246 -4 1 8 4 71.71 2.23 1.3162 0 6 3 4 72.59 2.31 1.3023 0 1 8 4 73.06 1.54 1.2951 -2 6 1 4 73.31 1.04 1.2913 -2 5 6 4 73.37 1.57 1.2905 -4 4 4 4 73.64 2.25 1.2864 -2 6 3 4 73.78 1.50 1.2842 -5 1 4 4 73.98 4.10 1.2813 -4 3 7 4 74.20 2.31 1.2780 3 0 4 2 74.41 1.30 1.2749 2 4 4 4 74.69 2.49 1.2708 -2 2 9 4 74.73 3.77 1.2703 4 2 1 4 75.38 1.71 1.2609 3 4 2 4 75.39 3.27 1.2609 -3 2 9 4 76.06 1.34 1.2514 1 2 7 4 76.77 2.14 1.2415 -5 2 5 4 77.04 2.54 1.2379 -4 4 6 4 77.27 1.71 1.2348 1 6 3 4 77.38 1.29 1.2333 -3 5 6 4 77.48 1.93 1.2319 -4 1 9 4 77.81 1.09 1.2275 -2 4 8 4 78.33 2.36 1.2207 1 4 6 4 78.96 1.26 1.2125 -4 3 8 4 80.67 1.45 1.1911 -5 2 7 4 81.02 1.25 1.1868 -3 6 3 4 81.17 1.71 1.1849 4 4 0 4 81.79 2.29 1.1775 0 6 5 4 82.15 1.07 1.1733 -3 5 7 4 83.03 1.36 1.1631 -1 7 3 4 83.07 1.85 1.1627 -1 3 9 4 83.26 2.50 1.1605 0 1 9 4 83.65 1.75 1.1561 1 1 8 4 83.94 1.72 1.1528 -5 2 1 4 85.42 1.07 1.1366 1 7 2 4 85.51 2.66 1.1356 -2 7 1 4 85.70 1.19 1.1336 4 1 3 4 86.35 1.05 1.1267 -2 5 8 4 86.62 1.80 1.1239 -5 1 9 4 86.91 2.55 1.1208 2 6 3 4 87.27 1.95 1.1171 2 1 7 4 89.35 1.44 1.0964 1 6 5 4 89.58 1.54 1.0943 1 7 3 4 89.66 1.10 1.0935 4 5 0 4 89.66 1.92 1.0935 -2 6 7 4 89.87 1.16 1.0915 2 7 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.