data_global _chemical_name_mineral 'Althausite' loop_ _publ_author_name 'Romming C' 'Raade G' _journal_name_full 'American Mineralogist' _journal_volume 65 _journal_year 1980 _journal_page_first 488 _journal_page_last 498 _publ_section_title ; The crystal structure of althausite, Mg4(PO4)2(OH,O)(F, ) ; _database_code_amcsd 0000784 _chemical_formula_sum 'Mg4 P2 O8.56 F.25 H.37' _cell_length_a 8.258 _cell_length_b 6.054 _cell_length_c 14.383 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 719.063 _exptl_crystal_density_diffrn 2.783 _symmetry_space_group_name_H-M 'P n m a' loop_ _space_group_symop_operation_xyz 'x,y,z' 'x,1/2-y,z' '-x,1/2+y,-z' '1/2-x,1/2+y,1/2+z' '1/2+x,1/2-y,1/2-z' '1/2+x,y,1/2-z' '1/2-x,-y,1/2+z' '-x,-y,-z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_U_iso_or_equiv Mg1 0.13402 0.00414 0.16858 1.00000 ? Mg2 0.34763 0.25000 0.42143 1.00000 ? Mg3 0.07712 0.25000 0.57505 1.00000 ? P1 0.48845 0.25000 0.14583 1.00000 ? P2 0.22456 0.25000 0.84820 1.00000 ? O11 0.38234 0.04123 0.14137 1.00000 ? O12 0.60739 0.25000 0.06273 1.00000 ? O13 0.59147 0.25000 0.23554 1.00000 ? O21 0.11583 0.04268 0.85336 1.00000 ? O22 0.32077 0.25000 0.75588 1.00000 ? O23 0.34092 0.25000 0.93021 1.00000 ? F 0.33500 0.25000 0.56627 0.25000 ? O 0.09124 0.25000 0.07585 0.19000 ? O-h 0.09124 0.25000 0.07585 0.37000 ? H 0.15400 0.25000 0.03500 0.37000 0.02026 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Mg1 0.00670 0.00490 0.00850 0.00090 0.00040 0.00090 Mg2 0.00540 0.00660 0.01110 0.00000 0.00210 0.00000 Mg3 0.00680 0.00630 0.00750 0.00000 -0.00070 0.00000 P1 0.00370 0.00410 0.00480 0.00000 -0.00010 0.00000 P2 0.00430 0.00450 0.00550 0.00000 0.00040 0.00000 O11 0.00610 0.00690 0.01120 -0.00130 0.00060 -0.00060 O12 0.00640 0.01120 0.00720 0.00000 0.00120 0.00000 O13 0.01020 0.00800 0.00650 0.00000 -0.00290 0.00160 O21 0.00680 0.00710 0.01200 -0.00160 -0.00040 0.00000 O22 0.01080 0.00760 0.00760 0.00000 0.00350 0.00000 O23 0.00680 0.01870 0.00850 0.00000 -0.00280 0.00000 F 0.00640 0.00660 0.00570 0.00000 -0.00160 0.00000 O 0.00600 0.00820 0.00710 0.00000 0.00080 0.00000 O-h 0.00600 0.00820 0.00710 0.00000 0.00080 0.00000