Sigismundite
Demartin F, Gramaccioli C M, Pilati T, Sciesa E
The Canadian Mineralogist 34 (1996) 827-834
Sigismundite, (Ba,K,Pb)Na3(Ca,Sr)(Fe,Mg,Mn)14Al(OH)2(PO4)12, a new
Ba-rich member of the arrojadite group from Spluga Valley, Italy
Locality: Spluga Valley, Italy
_database_code_amcsd 0005505
CELL PARAMETERS: 16.4060 9.9450 24.4700 90.000 105.730 90.000
SPACE GROUP: C2/c
X-RAY WAVELENGTH: 1.541838
Cell Volume: 3842.950
Density (g/cm3): 3.125
MAX. ABS. INTENSITY / VOLUME**2: 5.681686356
RIR: 0.592
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
7.51 5.00 11.7768 0 0 2 2
10.51 7.23 8.4153 1 1 0 4
11.21 6.71 7.8958 2 0 0 2
11.67 5.56 7.5851 1 1 1 4
11.68 7.29 7.5768 -2 0 2 2
13.79 1.49 6.4221 1 1 2 4
15.05 1.25 5.8884 0 0 4 2
15.11 11.23 5.8640 2 0 2 2
16.15 16.54 5.4867 -2 0 4 2
16.52 1.36 5.3670 1 1 3 4
17.84 31.98 4.9725 0 2 0 2
18.53 1.70 4.7875 -3 1 1 4
18.75 1.94 4.7317 -3 1 2 4
19.08 1.35 4.6524 3 1 0 4
19.38 16.86 4.5809 0 2 2 4
19.61 22.58 4.5271 1 1 4 4
21.11 3.16 4.2076 2 2 0 4
21.37 20.93 4.1572 -2 2 2 4
21.72 2.71 4.0924 -4 0 2 2
22.16 4.93 4.0110 3 1 2 4
22.39 2.88 3.9703 -2 0 6 2
22.52 11.38 3.9479 4 0 0 2
23.44 4.14 3.7960 -3 1 5 4
23.46 1.97 3.7925 2 2 2 4
25.95 5.45 3.4329 -3 1 6 4
26.06 4.04 3.4198 0 2 5 4
26.28 1.72 3.3909 -2 2 5 4
26.40 19.87 3.3756 1 1 6 4
27.13 19.44 3.2874 3 1 4 4
27.35 3.40 3.2605 -4 0 6 2
27.49 2.85 3.2443 1 3 0 4
27.54 2.46 3.2384 -1 3 1 4
27.78 7.60 3.2110 2 2 4 4
27.97 3.11 3.1900 1 3 1 4
27.99 51.51 3.1875 2 0 6 2
28.12 17.29 3.1734 -1 3 2 4
28.24 5.79 3.1599 -4 2 2 4
28.70 1.72 3.1108 -4 2 3 4
28.77 12.10 3.1026 -2 2 6 4
28.78 8.35 3.1022 -3 1 7 4
28.91 3.46 3.0879 -5 1 1 4
28.95 5.43 3.0841 1 3 2 4
28.98 1.76 3.0812 0 2 6 4
29.63 2.41 3.0145 -5 1 4 4
29.64 100.00 3.0135 -4 2 4 4
30.39 2.25 2.9411 1 3 3 4
30.46 1.45 2.9345 2 2 5 4
30.71 1.00 2.9109 -1 3 4 4
30.84 6.19 2.8991 -5 1 5 4
31.44 3.31 2.8458 4 2 2 4
31.71 17.73 2.8222 -3 3 2 4
31.84 15.47 2.8107 -3 1 8 4
31.90 8.14 2.8051 3 3 0 4
32.12 1.42 2.7867 0 2 7 4
32.24 7.60 2.7769 1 3 4 4
32.30 1.38 2.7715 -3 3 3 4
32.47 15.07 2.7574 -5 1 6 4
32.64 19.10 2.7433 -4 0 8 2
32.69 4.07 2.7393 3 3 1 4
32.79 20.49 2.7310 -6 0 2 2
32.85 1.07 2.7266 -4 2 6 4
33.20 3.94 2.6984 3 1 6 4
33.34 3.03 2.6877 -3 3 4 4
33.39 62.62 2.6835 2 2 6 4
33.90 12.17 2.6440 3 3 2 4
34.43 1.43 2.6050 1 3 5 4
34.56 1.86 2.5954 5 1 3 4
34.57 1.91 2.5948 -2 2 8 4
34.88 14.41 2.5721 -1 3 6 4
35.43 11.96 2.5334 0 2 8 4
35.54 23.07 2.5256 4 2 4 4
35.55 11.78 2.5256 -6 0 6 2
36.13 17.27 2.4862 0 4 0 2
36.58 2.02 2.4563 -3 3 6 4
36.95 1.13 2.4326 0 4 2 4
37.44 11.54 2.4020 -4 2 8 4
37.57 12.18 2.3937 -6 2 2 4
38.03 6.22 2.3658 -6 2 4 4
38.61 1.12 2.3320 -5 3 2 4
38.85 3.97 2.3178 -6 2 5 4
39.37 1.26 2.2885 -5 3 4 4
39.41 4.86 2.2867 5 3 0 4
39.51 1.45 2.2809 -7 1 3 4
39.65 1.86 2.2731 1 3 7 4
39.97 5.70 2.2556 3 1 8 4
40.14 1.37 2.2466 -4 2 9 4
40.20 1.00 2.2433 -1 3 8 4
40.32 8.12 2.2368 -5 3 5 4
40.63 1.40 2.2207 2 4 3 4
40.80 2.34 2.2114 4 2 6 4
41.02 2.94 2.2000 7 1 0 4
41.05 4.73 2.1988 0 4 5 4
41.27 1.03 2.1876 1 1 10 4
41.40 10.46 2.1808 -7 1 6 4
41.57 3.91 2.1724 -6 2 7 4
42.47 4.63 2.1286 0 2 10 4
42.55 5.07 2.1249 -4 4 2 4
42.60 1.72 2.1222 1 3 8 4
42.99 2.32 2.1038 4 4 0 4
43.02 1.10 2.1027 4 0 8 2
43.07 3.02 2.1004 0 4 6 4
43.13 2.23 2.0976 6 2 3 4
43.25 3.27 2.0917 -5 3 7 4
43.54 1.50 2.0786 -4 4 4 4
43.77 1.04 2.0684 -3 3 9 4
43.81 1.41 2.0663 7 1 2 4
44.10 1.42 2.0535 -6 0 10 2
44.41 1.20 2.0398 -7 1 8 4
45.21 1.90 2.0055 6 2 4 4
45.70 1.47 1.9851 -4 0 12 2
45.93 1.38 1.9757 -1 1 12 4
45.98 5.36 1.9739 8 0 0 2
46.02 1.52 1.9721 -1 5 1 4
46.36 1.14 1.9586 -1 3 10 4
46.37 1.09 1.9583 -7 1 9 4
46.40 5.97 1.9571 -1 5 2 4
46.85 6.08 1.9393 2 2 10 4
46.91 6.70 1.9367 4 2 8 4
46.94 1.12 1.9356 1 5 2 4
47.22 1.71 1.9250 -2 4 8 4
47.25 1.97 1.9238 3 1 10 4
47.63 2.33 1.9094 -7 3 2 4
47.89 2.21 1.8996 0 4 8 4
47.91 1.27 1.8987 1 5 3 4
47.92 3.33 1.8985 3 3 8 4
47.93 1.15 1.8980 -6 2 10 4
47.98 2.48 1.8963 4 4 4 4
48.03 8.72 1.8942 -8 0 8 2
48.07 1.39 1.8929 -7 3 1 4
48.25 1.77 1.8862 -2 2 12 4
48.82 2.39 1.8656 -3 5 2 4
48.83 2.76 1.8650 7 3 0 4
49.48 5.70 1.8422 -4 4 8 4
49.58 4.81 1.8385 -6 4 2 4
49.69 3.51 1.8347 -3 3 11 4
49.74 1.11 1.8331 -2 4 9 4
49.91 1.50 1.8273 7 3 1 4
51.28 2.48 1.7814 7 3 2 4
51.58 1.80 1.7718 -6 4 6 4
51.73 3.45 1.7670 -8 0 10 2
51.81 2.47 1.7647 -9 1 6 4
52.21 1.88 1.7519 4 4 6 4
52.36 2.14 1.7474 -3 5 6 4
52.45 8.52 1.7447 -2 0 14 2
52.48 7.98 1.7436 -2 4 10 4
52.61 2.90 1.7397 1 5 6 4
52.64 6.85 1.7386 6 4 2 4
52.76 3.50 1.7352 8 0 4 2
52.81 2.35 1.7336 7 1 6 4
52.93 2.03 1.7299 -3 3 12 4
53.02 2.66 1.7272 3 5 4 4
53.18 1.01 1.7224 -1 3 12 4
53.38 2.18 1.7165 -6 2 12 4
54.02 1.29 1.6976 -1 1 14 4
54.09 2.23 1.6955 -4 4 10 4
54.52 3.04 1.6831 5 5 0 4
55.14 4.45 1.6655 -1 5 8 4
55.38 1.06 1.6590 -5 3 12 4
55.42 1.04 1.6578 -2 4 11 4
55.51 1.66 1.6554 5 3 8 4
55.58 1.05 1.6534 0 6 1 4
55.84 4.53 1.6463 -2 2 14 4
55.87 3.11 1.6457 -3 5 8 4
56.03 4.85 1.6413 0 6 2 4
56.10 4.60 1.6394 1 3 12 4
56.14 8.17 1.6383 8 2 4 4
56.27 1.50 1.6348 -5 5 6 4
56.32 1.68 1.6334 5 5 2 4
56.44 1.74 1.6302 -8 0 12 2
56.62 1.56 1.6256 -10 0 6 2
56.74 1.43 1.6224 -4 4 11 4
57.06 2.88 1.6141 1 5 8 4
57.25 1.63 1.6092 -3 1 15 4
57.38 1.14 1.6058 1 1 14 4
57.59 1.13 1.6006 -5 5 7 4
57.60 1.55 1.6002 9 1 3 4
57.73 1.14 1.5968 -9 3 4 4
57.86 7.46 1.5937 4 0 12 2
58.34 1.48 1.5816 -10 0 8 2
58.41 1.02 1.5799 -8 4 4 4
58.65 1.81 1.5741 7 1 8 4
59.24 1.29 1.5598 5 5 4 4
59.32 4.58 1.5578 6 0 10 2
59.69 3.50 1.5491 -8 2 12 4
59.82 2.26 1.5459 8 4 0 4
59.86 4.50 1.5451 -10 2 6 4
59.99 1.94 1.5421 2 6 4 4
60.14 1.19 1.5385 -1 5 10 4
60.35 1.12 1.5337 -8 4 7 4
61.02 3.51 1.5185 -4 6 4 4
61.06 3.73 1.5177 4 2 12 4
61.16 1.44 1.5154 -10 0 10 2
61.30 2.41 1.5122 -7 5 4 4
61.31 1.52 1.5121 10 0 2 2
61.48 1.02 1.5081 2 6 5 4
61.52 1.25 1.5072 -10 2 8 4
62.05 1.40 1.4957 4 6 2 4
62.23 1.46 1.4919 9 3 2 4
62.23 1.13 1.4919 7 5 0 4
63.08 3.39 1.4738 -5 5 10 4
63.23 2.34 1.4706 2 6 6 4
63.73 2.05 1.4602 -9 1 13 4
63.92 2.63 1.4565 -11 1 7 4
64.40 1.99 1.4467 10 2 2 4
64.52 1.26 1.4443 0 6 8 4
65.34 3.84 1.4281 -2 4 14 4
65.61 1.68 1.4229 8 4 4 4
65.83 1.68 1.4187 -4 6 8 4
66.00 1.76 1.4155 4 0 14 2
66.05 1.19 1.4145 -1 7 1 4
66.21 3.31 1.4115 0 2 16 4
66.23 2.93 1.4111 -6 6 4 4
66.49 4.16 1.4062 8 2 8 4
66.54 1.91 1.4054 -6 2 16 4
67.40 1.68 1.3895 -9 3 12 4
68.28 1.05 1.3736 -3 7 2 4
68.37 1.79 1.3721 -2 6 10 4
68.39 1.15 1.3716 3 7 0 4
68.51 1.03 1.3697 6 6 2 4
69.73 1.29 1.3485 -9 3 13 4
69.75 1.16 1.3483 -4 6 10 4
69.76 1.22 1.3481 -10 0 14 2
69.91 1.70 1.3456 -11 3 7 4
70.14 2.73 1.3417 4 4 12 4
70.67 1.17 1.3330 10 4 0 4
71.17 1.66 1.3248 7 3 10 4
71.26 2.06 1.3234 -6 0 18 2
71.46 1.40 1.3201 6 4 10 4
71.72 2.89 1.3160 12 0 0 2
71.89 2.12 1.3133 1 3 16 4
72.29 1.05 1.3070 -9 3 14 4
72.31 1.25 1.3067 -7 3 16 4
73.64 1.20 1.2864 -5 7 5 4
73.66 1.27 1.2861 -2 6 12 4
74.14 2.52 1.2789 -6 2 18 4
75.29 1.21 1.2622 -6 4 16 4
77.03 1.44 1.2379 2 0 18 2
77.79 2.68 1.2277 -7 1 19 4
78.30 1.37 1.2211 -13 1 1 4
84.55 1.03 1.1460 0 2 20 4
86.26 1.10 1.1277 -9 5 15 4
86.95 1.82 1.1204 -9 7 4 4
87.95 1.07 1.1103 4 8 6 4
89.45 1.14 1.0955 -4 8 10 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.