data_global _chemical_name_mineral 'Olshanskyite' loop_ _publ_author_name 'Callegari A' 'Mazzi F' 'Tadini C' _journal_name_full 'The Canadian Mineralogist' _journal_volume 39 _journal_year 2001 _journal_page_first 137 _journal_page_last 144 _publ_section_title ; The crystal structure of olshanskyite ; _database_code_amcsd 0005707 _chemical_compound_source 'Fuka mine, Okayama Prefecture, Japan' _chemical_formula_sum 'Ca2 B3 O13 H13' _cell_length_a 7.953 _cell_length_b 9.873 _cell_length_c 7.362 _cell_angle_alpha 111.00 _cell_angle_beta 94.65 _cell_angle_gamma 107.53 _cell_volume 502.874 _exptl_crystal_density_diffrn 2.204 _symmetry_space_group_name_H-M 'P -1' loop_ _space_group_symop_operation_xyz 'x,y,z' '-x,-y,-z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv Ca1 0.08117 0.03398 0.25741 0.00950 Ca2 0.11601 0.67181 0.41741 0.01039 B1 0.28400 0.02910 0.63440 0.00836 B2 0.23580 0.28640 0.69110 0.00861 B3 0.52830 0.28740 0.85300 0.00925 O1 0.25900 -0.06830 0.41970 0.01051 O2 0.20030 -0.09010 0.71340 0.01102 O3 0.16840 0.12090 0.64530 0.00988 O4 0.17900 0.30220 0.50270 0.01203 O5 0.12960 0.35930 0.82910 0.01102 O6 0.42970 0.35890 0.75940 0.01001 O7 0.72260 0.35390 0.85680 0.01305 O8 0.49760 0.31710 0.05970 0.01545 O9 0.46930 0.11900 0.73780 0.01013 O10 0.06910 0.17910 0.05410 0.01431 O11 0.35870 0.05240 0.12490 0.02090 O12 -0.05000 0.39180 0.26960 0.01621 O13 0.37050 0.60720 0.51140 0.01912 H1 0.35500 -0.07700 0.37600 0.04306 H2 0.24800 -0.06300 -0.16700 0.03926 H4 0.24600 0.38200 0.49100 0.03926 H5 0.10000 0.30800 -0.09400 0.03673 H7 0.76700 0.44600 -0.04900 0.03293 H8 0.50200 0.41000 0.11500 0.03673 H10 0.18200 0.21900 0.06600 0.04306 H11a 0.42400 0.12800 0.10300 0.05193 H11b 0.43100 0.01000 0.16600 0.05953 H12a -0.00100 0.32000 0.19900 0.05066 H12b -0.14000 0.37900 0.18000 0.04939 H13a 0.42700 0.64800 0.64300 0.04559 H13b 0.45200 0.62400 0.43100 0.04179 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Ca1 0.00930 0.01010 0.00930 0.00350 0.00240 0.00420 Ca2 0.00950 0.00840 0.01290 0.00310 0.00220 0.00390 B1 0.00780 0.00690 0.00980 0.00230 0.00210 0.00280 B2 0.00840 0.00770 0.00910 0.00280 0.00140 0.00290 B3 0.00810 0.00830 0.01000 0.00250 0.00150 0.00260 O1 0.00990 0.01140 0.00910 0.00410 0.00290 0.00260 O2 0.01230 0.01000 0.01080 0.00200 0.00240 0.00570 O3 0.00720 0.00700 0.01450 0.00250 0.00230 0.00350 O4 0.01250 0.01210 0.01060 0.00240 0.00040 0.00570 O5 0.01200 0.00990 0.01150 0.00500 0.00420 0.00340 O6 0.00740 0.00840 0.01310 0.00150 0.00070 0.00430 O7 0.00750 0.01020 0.01620 0.00110 0.00110 0.00130 O8 0.02370 0.01170 0.01110 0.00640 0.00540 0.00460 O9 0.00720 0.00730 0.01330 0.00220 0.00080 0.00200 O10 0.01580 0.01450 0.01250 0.00460 0.00350 0.00600 O11 0.01530 0.03140 0.02350 0.00940 0.00760 0.01860 O12 0.01910 0.01150 0.01710 0.00570 0.00200 0.00490 O13 0.01440 0.02570 0.02070 0.00770 0.00370 0.01240