Gladite
Topa D, Makovicky E, Balic-Zunic T
The Canadian Mineralogist 40 (2002) 1147-1159
The structural role of excess Cu and Pb in gladite and krupkaite
based on new refinements of their structure
Sample: bd33
_database_code_amcsd 0005780
CELL PARAMETERS: 4.0044 33.5750 11.4800 90.000 90.000 90.000
SPACE GROUP: Pmcn
X-RAY WAVELENGTH: 1.541838
Cell Volume: 1543.460
Density (g/cm3): 6.903
MAX. ABS. INTENSITY / VOLUME**2: 73.71674933
RIR: 3.477
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
5.26 3.82 16.7875 0 2 0 2
11.04 3.21 8.0137 0 3 1 4
15.44 18.05 5.7400 0 0 2 2
15.84 3.62 5.5958 0 6 0 2
16.32 3.06 5.4313 0 2 2 4
17.36 21.22 5.1074 0 3 2 4
21.17 4.89 4.1969 0 8 0 2
22.19 55.57 4.0069 0 6 2 4
22.56 4.93 3.9417 0 8 1 4
23.60 28.49 3.7703 1 3 0 4
23.85 3.63 3.7310 0 2 3 4
24.18 1.97 3.6806 0 7 2 4
24.59 100.00 3.6209 0 3 3 4
24.86 55.11 3.5821 1 3 1 8
25.10 84.93 3.5479 0 9 1 4
26.55 5.17 3.3575 0 10 0 2
26.82 1.84 3.3247 0 5 3 4
27.15 19.14 3.2842 1 0 2 4
27.28 3.73 3.2686 1 1 2 8
27.68 1.43 3.2231 1 2 2 8
28.25 8.39 3.1587 0 6 3 4
28.32 54.68 3.1513 1 3 2 8
28.49 93.42 3.1329 1 6 1 8
28.54 8.05 3.1280 0 9 2 4
29.20 2.72 3.0584 1 4 2 8
29.87 1.83 2.9913 0 7 3 4
30.10 3.82 2.9693 1 7 1 8
31.16 3.02 2.8700 0 0 4 2
31.59 90.01 2.8324 1 6 2 8
31.63 1.11 2.8290 0 2 4 4
31.99 2.88 2.7979 0 12 0 2
32.81 21.59 2.7296 1 9 0 4
32.95 3.56 2.7183 0 12 1 4
33.55 1.19 2.6712 0 9 3 4
33.75 33.47 2.6555 1 9 1 8
33.97 2.82 2.6391 0 5 4 4
34.68 1.13 2.5864 1 8 2 8
35.14 41.06 2.5537 0 6 4 4
35.70 14.57 2.5150 0 12 2 4
36.22 19.09 2.4800 1 6 3 8
36.45 1.00 2.4651 1 9 2 8
36.48 2.03 2.4628 0 7 4 4
38.60 22.39 2.3327 1 0 4 4
38.69 3.85 2.3271 1 1 4 8
39.46 29.12 2.2837 1 3 4 8
39.62 2.93 2.2747 0 9 4 4
39.92 2.84 2.2586 0 12 3 4
40.09 18.40 2.2491 1 12 1 8
40.34 5.09 2.2358 1 11 2 8
40.60 5.05 2.2222 1 9 3 8
41.09 3.22 2.1970 0 15 1 4
41.96 8.48 2.1531 1 6 4 8
42.21 2.77 2.1407 0 13 3 4
42.38 2.19 2.1326 1 13 1 8
42.44 13.33 2.1298 1 12 2 8
42.56 7.64 2.1242 0 6 5 4
43.27 1.20 2.0909 0 11 4 4
43.39 4.37 2.0854 0 15 2 4
44.18 1.33 2.0498 1 11 3 8
44.63 1.04 2.0301 1 13 2 8
45.26 3.41 2.0034 0 12 4 4
45.29 33.59 2.0022 2 0 0 2
45.88 1.34 1.9779 1 9 4 8
46.14 34.37 1.9672 1 12 3 8
46.30 7.74 1.9610 1 3 5 8
46.44 9.14 1.9553 0 9 5 4
46.48 15.86 1.9538 1 15 0 4
46.88 1.05 1.9380 1 4 5 8
47.03 18.43 1.9321 0 15 3 4
47.19 2.46 1.9261 1 15 1 8
47.46 1.40 1.9157 1 10 4 8
47.52 9.03 1.9133 0 0 6 2
47.60 1.06 1.9102 0 1 6 4
47.62 1.28 1.9096 1 5 5 8
48.13 1.54 1.8905 2 0 2 4
48.25 1.01 1.8860 0 3 6 4
48.51 7.82 1.8765 1 6 5 8
48.82 6.50 1.8653 0 18 0 2
48.86 1.99 1.8641 2 3 2 8
49.27 1.20 1.8496 1 15 2 8
49.51 1.31 1.8411 0 18 1 4
49.53 1.49 1.8403 0 14 4 4
49.54 1.08 1.8401 0 5 6 4
50.35 1.93 1.8121 1 14 3 8
50.41 1.05 1.8104 0 6 6 4
50.73 1.57 1.7994 1 8 5 8
50.99 8.77 1.7910 2 6 2 8
51.52 2.30 1.7740 0 18 2 4
51.60 1.57 1.7713 1 17 0 4
51.69 2.10 1.7683 1 16 2 8
51.80 1.23 1.7650 0 15 4 4
52.05 10.21 1.7571 1 9 5 8
52.21 18.16 1.7522 2 3 3 8
52.39 1.31 1.7465 0 19 1 4
52.48 16.54 1.7437 2 9 1 8
52.59 2.99 1.7401 1 15 3 8
53.05 9.21 1.7264 1 0 6 4
53.27 1.01 1.7196 2 10 0 4
53.72 3.50 1.7062 1 3 6 8
53.85 1.73 1.7025 0 9 6 4
54.24 1.64 1.6911 2 6 3 8
54.25 1.19 1.6910 1 4 6 8
54.41 1.74 1.6863 2 9 2 8
54.88 2.45 1.6728 1 18 1 8
55.30 1.36 1.6611 0 20 1 4
55.72 1.14 1.6497 1 6 6 8
56.73 2.99 1.6226 1 12 5 8
57.14 1.11 1.6121 2 12 1 8
57.57 1.63 1.6009 1 19 1 8
58.59 12.40 1.5757 2 6 4 8
58.95 1.66 1.5668 1 9 6 8
58.96 4.41 1.5664 2 12 2 8
59.07 2.28 1.5640 0 18 4 4
60.07 3.06 1.5402 0 21 2 4
61.33 1.40 1.5115 1 2 7 8
61.68 4.94 1.5039 1 3 7 8
61.72 1.05 1.5029 2 9 4 8
61.79 4.64 1.5013 0 9 7 4
61.93 1.10 1.4983 2 12 3 8
62.79 1.29 1.4798 2 15 1 8
63.14 1.12 1.4726 1 21 1 8
63.51 2.83 1.4647 1 6 7 8
63.63 1.06 1.4623 2 13 3 8
63.89 3.09 1.4570 2 6 5 8
63.90 2.73 1.4568 1 18 4 8
64.02 1.54 1.4544 0 15 6 4
64.52 1.77 1.4443 2 15 2 8
64.86 5.50 1.4375 1 21 2 8
64.98 1.84 1.4352 1 20 3 8
65.59 1.13 1.4233 0 3 8 4
65.96 1.51 1.4162 2 12 4 8
66.03 2.04 1.4149 0 12 7 4
66.88 4.18 1.3989 2 9 5 8
67.35 8.36 1.3903 2 15 3 8
67.70 1.25 1.3840 1 22 2 8
67.74 4.24 1.3833 2 0 6 4
68.66 3.54 1.3670 1 15 6 8
68.79 3.14 1.3648 2 18 0 4
70.51 1.62 1.3356 0 18 6 4
70.99 1.23 1.3278 2 18 2 8
71.35 1.38 1.3219 1 19 5 8
71.54 7.31 1.3188 1 21 4 8
71.68 1.38 1.3167 3 3 1 8
71.90 2.57 1.3132 1 6 8 8
71.97 1.88 1.3120 1 24 1 8
72.76 1.21 1.2998 1 17 6 8
73.30 1.79 1.2914 3 3 2 8
73.39 2.94 1.2901 3 6 1 8
74.93 1.23 1.2674 0 3 9 4
75.00 3.24 1.2664 3 6 2 8
75.72 2.41 1.2561 1 15 7 8
76.21 1.33 1.2493 3 9 1 8
77.43 1.42 1.2325 2 18 4 8
78.32 1.93 1.2208 2 21 2 8
78.65 1.31 1.2165 1 12 8 8
79.13 1.26 1.2103 3 0 4 4
79.68 1.80 1.2033 3 3 4 8
79.85 3.03 1.2012 2 9 7 8
80.10 1.14 1.1981 3 12 1 8
80.96 1.35 1.1876 1 27 0 4
81.82 1.27 1.1772 1 18 7 8
81.86 1.05 1.1767 2 15 6 8
83.25 1.02 1.1606 0 12 9 4
83.70 1.47 1.1555 2 12 7 8
84.27 2.87 1.1491 3 12 3 8
84.51 1.30 1.1464 3 15 0 4
87.87 1.25 1.1111 2 18 6 8
88.63 1.08 1.1035 1 0 10 4
88.74 1.06 1.1024 3 9 5 8
89.53 1.00 1.0947 3 0 6 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.