Gladite
Topa D, Makovicky E, Balic-Zunic T
The Canadian Mineralogist 40 (2002) 1147-1159
The structural role of excess Cu and Pb in gladite and krupkaite
based on new refinements of their structure
Sample: bd39
_database_code_amcsd 0005781
CELL PARAMETERS: 4.0100 33.5890 11.5020 90.000 90.000 90.000
SPACE GROUP: Pmcn
X-RAY WAVELENGTH: 1.541838
Cell Volume: 1549.226
Density (g/cm3): 6.938
MAX. ABS. INTENSITY / VOLUME**2: 74.19353258
RIR: 3.482
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
5.26 2.33 16.7945 0 2 0 2
11.03 3.30 8.0229 0 3 1 4
15.41 15.68 5.7510 0 0 2 2
15.83 2.75 5.5982 0 6 0 2
16.29 2.33 5.4408 0 2 2 4
17.33 20.22 5.1156 0 3 2 4
21.16 3.24 4.1986 0 8 0 2
22.16 54.22 4.0114 0 6 2 4
22.54 5.34 3.9441 0 8 1 4
23.57 27.17 3.7752 1 3 0 4
23.81 3.38 3.7378 0 2 3 4
24.16 2.09 3.6844 0 7 2 4
24.54 100.00 3.6272 0 3 3 4
24.82 54.47 3.5869 1 3 1 8
25.09 86.00 3.5499 0 9 1 4
25.54 1.46 3.4877 0 4 3 4
26.54 4.89 3.3589 0 10 0 2
26.77 1.48 3.3299 0 5 3 4
27.03 1.06 3.2986 1 5 1 8
27.11 18.39 3.2893 1 0 2 4
27.24 3.77 3.2737 1 1 2 8
27.63 1.32 3.2280 1 2 2 8
28.21 8.31 3.1633 0 6 3 4
28.28 58.74 3.1560 1 3 2 8
28.46 92.85 3.1364 1 6 1 8
28.51 7.59 3.1307 0 9 2 4
29.16 2.46 3.0627 1 4 2 8
29.83 1.67 2.9953 0 7 3 4
30.06 2.71 2.9725 1 7 1 8
31.10 3.61 2.8755 0 0 4 2
31.55 92.97 2.8360 1 6 2 8
31.97 3.54 2.7991 0 12 0 2
32.78 20.67 2.7320 1 9 0 4
32.93 3.78 2.7197 0 12 1 4
33.51 1.23 2.6743 0 9 3 4
33.72 36.53 2.6580 1 9 1 8
33.91 3.09 2.6435 0 5 4 4
35.08 43.23 2.5578 0 6 4 4
35.67 15.35 2.5168 0 12 2 4
36.17 20.22 2.4836 1 6 3 8
36.41 1.51 2.4677 1 9 2 8
36.43 1.89 2.4665 0 7 4 4
38.53 22.72 2.3368 1 0 4 4
38.62 4.18 2.3312 1 1 4 8
39.39 28.51 2.2875 1 3 4 8
39.56 2.96 2.2778 0 9 4 4
39.88 2.71 2.2607 0 12 3 4
40.06 20.39 2.2508 1 12 1 8
40.30 4.37 2.2379 1 11 2 8
40.55 5.85 2.2249 1 9 3 8
40.67 1.00 2.2187 0 4 5 4
41.06 3.27 2.1980 0 15 1 4
41.89 8.86 2.1565 1 6 4 8
42.18 2.58 2.1426 0 13 3 4
42.35 2.43 2.1342 1 13 1 8
42.40 14.33 2.1317 1 12 2 8
42.48 8.00 2.1278 0 6 5 4
43.22 1.39 2.0934 0 11 4 4
43.36 4.24 2.0867 0 15 2 4
44.13 1.36 2.0521 1 11 3 8
45.21 3.36 2.0057 0 12 4 4
45.23 35.81 2.0050 2 0 0 2
45.81 1.32 1.9806 1 9 4 8
46.09 35.02 1.9693 1 12 3 8
46.21 7.65 1.9644 1 3 5 8
46.37 9.51 1.9583 0 9 5 4
46.45 16.03 1.9551 1 15 0 4
46.80 1.09 1.9413 1 4 5 8
46.99 20.76 1.9336 0 15 3 4
47.15 2.66 1.9274 1 15 1 8
47.39 1.07 1.9182 1 10 4 8
47.43 8.97 1.9170 0 0 6 2
47.51 1.30 1.9139 0 1 6 4
47.54 1.11 1.9128 1 5 5 8
48.06 1.46 1.8932 2 0 2 4
48.16 1.07 1.8895 0 3 6 4
48.43 8.28 1.8796 1 6 5 8
48.78 1.99 1.8667 2 3 2 8
48.80 7.40 1.8661 0 18 0 2
49.22 1.25 1.8510 1 15 2 8
49.44 1.21 1.8434 0 5 6 4
49.48 1.16 1.8422 0 14 4 4
49.48 1.14 1.8420 0 18 1 4
50.30 2.00 1.8139 1 14 3 8
50.31 1.08 1.8136 0 6 6 4
50.65 1.92 1.8022 1 8 5 8
50.92 9.07 1.7935 2 6 2 8
51.49 2.38 1.7750 0 18 2 4
51.57 1.43 1.7724 1 17 0 4
51.65 2.24 1.7696 1 16 2 8
51.74 1.21 1.7667 0 15 4 4
51.97 10.58 1.7597 1 9 5 8
52.12 19.05 1.7548 2 3 3 8
52.36 1.22 1.7473 0 19 1 4
52.41 17.71 1.7458 2 9 1 8
52.54 3.63 1.7417 1 15 3 8
52.94 10.05 1.7295 1 0 6 4
53.20 1.02 1.7216 2 10 0 4
53.62 4.19 1.7093 1 3 6 8
53.76 1.76 1.7052 0 9 6 4
54.14 1.08 1.6940 1 4 6 8
54.16 1.74 1.6935 2 6 3 8
54.33 1.71 1.6884 2 9 2 8
54.85 2.78 1.6738 1 18 1 8
55.28 1.20 1.6618 0 20 1 4
55.62 1.50 1.6525 1 6 6 8
55.90 1.02 1.6447 2 0 4 4
56.65 3.45 1.6248 1 12 5 8
57.07 1.20 1.6139 2 12 1 8
57.54 1.82 1.6019 1 19 1 8
58.49 13.75 1.5780 2 6 4 8
58.85 1.80 1.5692 1 9 6 8
58.89 4.91 1.5682 2 12 2 8
59.01 2.37 1.5653 0 18 4 4
60.04 3.30 1.5410 0 21 2 4
61.21 1.66 1.5143 1 2 7 8
61.55 5.35 1.5066 1 3 7 8
61.63 1.11 1.5050 2 9 4 8
61.68 5.07 1.5038 0 9 7 4
61.85 1.12 1.5000 2 12 3 8
62.72 1.41 1.4813 2 15 1 8
63.10 1.62 1.4734 1 21 1 8
63.39 2.86 1.4673 1 6 7 8
63.55 1.05 1.4640 2 13 3 8
63.78 3.39 1.4592 2 6 5 8
63.83 3.34 1.4582 1 18 4 8
63.93 1.70 1.4563 0 15 6 4
64.28 1.12 1.4492 0 18 5 4
64.45 1.78 1.4458 2 15 2 8
64.82 6.28 1.4384 1 21 2 8
64.93 1.57 1.4363 1 20 3 8
65.45 1.33 1.4260 0 3 8 4
65.87 1.56 1.4180 2 12 4 8
65.92 2.21 1.4170 0 12 7 4
66.77 4.62 1.4009 2 9 5 8
67.27 9.97 1.3918 2 15 3 8
67.61 4.44 1.3856 2 0 6 4
67.65 1.42 1.3849 1 22 2 8
68.56 3.66 1.3688 1 15 6 8
68.72 3.79 1.3660 2 18 0 4
69.07 1.02 1.3599 0 24 2 4
70.42 1.90 1.3371 0 18 6 4
70.91 1.35 1.3290 2 18 2 8
71.27 1.39 1.3232 1 19 5 8
71.48 8.25 1.3199 1 21 4 8
71.56 1.49 1.3185 3 3 1 8
71.75 2.64 1.3155 1 6 8 8
71.93 2.09 1.3127 1 24 1 8
72.65 1.15 1.3014 1 17 6 8
72.81 1.03 1.2990 2 9 6 8
73.18 2.14 1.2932 3 3 2 8
73.27 3.26 1.2919 3 6 1 8
74.77 1.26 1.2698 0 3 9 4
74.88 3.70 1.2681 3 6 2 8
75.59 2.94 1.2579 1 15 7 8
76.09 1.59 1.2509 3 9 1 8
77.08 1.10 1.2373 1 11 8 8
77.12 1.03 1.2368 0 27 1 4
77.34 1.58 1.2338 2 18 4 8
77.53 1.16 1.2313 3 6 3 8
78.24 2.18 1.2218 2 21 2 8
78.50 1.48 1.2184 1 12 8 8
78.99 1.42 1.2121 3 0 4 4
79.54 1.99 1.2051 3 3 4 8
79.70 3.47 1.2030 2 9 7 8
79.98 1.45 1.1996 3 12 1 8
80.91 1.68 1.1882 1 27 0 4
81.54 1.04 1.1805 3 12 2 8
81.69 1.42 1.1787 1 18 7 8
81.73 1.21 1.1783 2 15 6 8
83.08 1.22 1.1626 0 12 9 4
83.45 1.04 1.1583 1 15 8 8
83.55 1.69 1.1572 2 12 7 8
84.14 3.23 1.1506 3 12 3 8
84.39 1.45 1.1477 3 15 0 4
87.33 1.01 1.1166 1 12 9 8
87.73 1.55 1.1125 2 18 6 8
88.42 1.30 1.1056 1 0 10 4
88.58 1.21 1.1040 3 9 5 8
89.35 1.22 1.0964 3 0 6 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.