Rakovanite
Kampf A R, Hughes J M, Marty J, Gunter M E, Nash B
The Canadian Mineralogist 49 (2011) 595-604
Rakovanite, Na3{H3[V10O28]}*15H2O, a new member of the
pascoite family with a protonated decavanadate polyanion
Locality: Synthetic
_database_code_amcsd 0018383
CELL PARAMETERS: 12.0248 17.1210 18.1400 90.000 106.242 90.000
SPACE GROUP: P2_1/n
X-RAY WAVELENGTH: 1.541838
Cell Volume: 3585.550
Density (g/cm3): 2.402
MAX. ABS. INTENSITY / VOLUME**2: 14.03924809
RIR: 1.903
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
7.92 100.00 11.1681 -1 0 1 2
9.24 9.76 9.5720 1 1 0 4
9.45 6.03 9.3540 -1 1 1 4
10.16 27.97 8.7080 0 0 2 2
10.31 60.14 8.5807 1 0 1 2
11.52 96.95 7.6826 0 2 1 4
11.54 1.62 7.6712 1 1 1 4
12.87 68.07 6.8764 1 2 0 4
15.03 3.17 5.8954 -1 2 2 4
15.04 2.66 5.8897 -1 0 3 2
15.35 6.27 5.7724 2 0 0 2
15.87 3.60 5.5841 -2 0 2 2
18.47 2.01 4.8047 0 2 3 4
18.93 1.79 4.6870 1 0 3 2
20.35 2.90 4.3636 2 2 1 4
20.40 3.08 4.3540 0 0 4 2
21.14 1.84 4.2020 -2 2 3 4
21.90 1.17 4.0584 2 3 0 4
22.22 2.09 4.0008 -3 0 1 2
22.27 2.76 3.9914 -1 2 4 4
22.83 1.17 3.8958 -3 1 1 4
23.22 15.62 3.8302 1 4 1 4
23.47 1.96 3.7912 2 3 1 4
24.54 1.06 3.6270 -1 0 5 2
25.73 2.69 3.4625 -1 4 3 4
25.91 12.93 3.4382 2 4 0 4
26.75 2.71 3.3329 2 2 3 4
26.79 3.10 3.3278 -3 1 4 4
27.65 2.85 3.2263 0 2 5 4
28.30 1.08 3.1538 -3 2 4 4
28.34 2.66 3.1494 3 1 2 4
29.38 1.61 3.0399 -3 0 5 2
29.48 14.37 3.0302 2 4 2 4
29.61 1.93 3.0169 3 3 1 4
29.77 1.44 3.0008 3 2 2 4
29.85 1.60 2.9931 -3 1 5 4
30.04 1.24 2.9744 -2 5 1 4
30.32 14.90 2.9477 -2 4 4 4
30.35 2.86 2.9450 2 5 0 4
30.59 1.06 2.9228 -3 4 1 4
30.80 13.71 2.9027 0 0 6 2
30.94 1.76 2.8899 -4 1 3 4
31.39 3.65 2.8497 -1 2 6 4
31.52 1.53 2.8380 2 5 1 4
31.72 1.06 2.8211 3 1 3 4
31.86 2.53 2.8089 -3 4 3 4
32.03 2.39 2.7939 3 3 2 4
32.06 1.16 2.7921 -2 5 3 4
32.06 4.47 2.7920 -4 0 4 2
32.32 2.37 2.7701 1 6 0 4
32.35 1.48 2.7671 -1 4 5 4
32.49 2.64 2.7556 -4 1 4 4
32.75 1.98 2.7343 3 4 1 4
33.27 1.37 2.6931 4 1 1 4
33.28 1.55 2.6925 -1 6 2 4
34.63 3.03 2.5901 1 6 2 4
34.77 1.38 2.5800 -4 1 5 4
35.39 6.00 2.5360 4 0 2 2
35.79 3.68 2.5086 4 1 2 4
35.80 1.23 2.5080 -4 3 4 4
37.06 15.49 2.4261 -2 4 6 4
37.06 1.21 2.4261 -2 5 5 4
37.65 1.15 2.3891 0 2 7 4
37.91 1.20 2.3734 -4 3 5 4
38.89 4.10 2.3155 4 1 3 4
39.65 1.57 2.2733 -3 5 5 4
40.40 3.15 2.2327 -2 5 6 4
40.88 1.16 2.2074 0 6 5 4
41.11 6.01 2.1957 -2 6 5 4
41.19 1.18 2.1917 5 1 1 4
42.12 2.27 2.1452 4 0 4 2
42.23 1.43 2.1401 0 8 0 2
42.54 1.39 2.1252 -3 5 6 4
42.92 2.68 2.1071 -3 4 7 4
43.59 6.08 2.0762 5 1 2 4
43.63 7.50 2.0747 -1 6 6 4
44.17 2.04 2.0503 -2 5 7 4
46.19 10.88 1.9651 -3 6 6 4
46.52 6.57 1.9522 5 1 3 4
47.73 1.28 1.9056 -3 7 5 4
47.73 5.17 1.9055 -2 6 7 4
48.04 1.02 1.8938 -2 8 4 4
48.38 1.24 1.8815 -2 7 6 4
49.90 1.90 1.8277 5 1 4 4
50.25 2.44 1.8158 -3 7 6 4
52.89 2.58 1.7312 -2 8 6 4
53.00 1.76 1.7278 -6 5 3 4
53.43 3.04 1.7147 2 4 8 4
53.54 1.11 1.7116 -6 5 4 4
53.80 1.82 1.7039 0 10 1 4
54.16 1.17 1.6936 1 10 0 4
54.54 1.21 1.6825 6 1 3 4
55.40 1.56 1.6585 1 6 8 4
60.28 1.37 1.5354 -7 5 3 4
61.13 1.04 1.5160 6 5 3 4
63.67 1.51 1.4616 3 6 8 4
63.81 1.27 1.4587 2 6 9 4
65.41 2.48 1.4268 0 12 0 2
65.98 1.05 1.4159 -5 1 12 4
66.27 1.48 1.4104 0 10 7 4
66.52 1.40 1.4057 -7 7 3 4
66.78 1.01 1.4008 -7 7 4 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.