Priceite
Sun W, Huang Y-X, Li Z, Pan Y, Mi J-X
The Canadian Mineralogist 49 (2011) 823-834
Hydrothermal synthesis and single-crystal X-ray structure refinement of
three borates: sibirskite, parasibirskite and priceite
Locality: synthetic
Note: T = 173 K
_database_code_amcsd 0018466
CELL PARAMETERS: 11.5800 6.9844 12.3520 90.000 110.573 90.000
SPACE GROUP: P2_1/c
X-RAY WAVELENGTH: 1.541838
Cell Volume: 935.309
Density (g/cm3): 2.480
MAX. ABS. INTENSITY / VOLUME**2: 6.272732545
RIR: 0.824
RIR based on corundum from Acta Crystallographica A38 (1982) 733-739
2-THETA INTENSITY D-SPACING H K L Multiplicity
8.16 100.00 10.8415 1 0 0 2
14.61 2.81 6.0626 -1 0 2 2
14.82 26.54 5.9786 0 1 1 4
15.09 6.62 5.8715 1 1 0 4
15.32 1.37 5.7821 0 0 2 2
15.57 3.93 5.6907 -1 1 1 4
16.35 19.54 5.4207 2 0 0 2
18.08 1.41 4.9076 -2 0 2 2
18.20 3.38 4.8742 1 1 1 4
19.39 1.94 4.5784 -1 1 2 4
19.78 9.10 4.4888 1 0 2 2
19.93 1.17 4.4539 0 1 2 4
20.01 6.15 4.4369 -2 1 1 4
20.74 18.78 4.2823 2 1 0 4
22.14 1.07 4.0155 -2 1 2 4
24.63 50.59 3.6138 3 0 0 2
25.11 1.03 3.5469 -1 1 3 4
25.51 56.14 3.4922 0 2 0 2
26.40 4.32 3.3762 -3 1 1 4
26.41 1.16 3.3749 0 1 3 4
26.47 3.77 3.3673 -2 1 3 4
26.66 1.08 3.3431 0 2 1 4
26.82 2.09 3.3240 1 2 0 4
27.10 3.84 3.2902 -1 2 1 4
27.25 1.54 3.2730 -3 1 2 4
29.19 3.00 3.0590 2 1 2 4
29.52 2.98 3.0261 -1 2 2 4
29.94 1.78 2.9841 -2 2 1 4
30.06 5.48 2.9732 1 1 3 4
30.16 10.66 2.9628 -3 1 3 4
30.45 1.14 2.9357 2 2 0 4
30.93 11.57 2.8911 0 0 4 2
31.16 6.01 2.8705 3 1 1 4
31.44 5.42 2.8454 -2 2 2 4
32.19 23.68 2.7807 -2 1 4 4
33.05 16.28 2.7104 4 0 0 2
33.54 2.51 2.6715 3 0 2 2
33.55 8.97 2.6713 0 1 4 4
33.65 1.39 2.6632 -1 2 3 4
34.65 1.27 2.5886 -3 2 1 4
34.66 2.00 2.5881 0 2 3 4
34.68 3.36 2.5868 -3 1 4 4
34.71 1.83 2.5846 -2 2 3 4
34.81 1.03 2.5771 1 0 4 2
35.32 3.52 2.5413 -3 2 2 4
35.53 2.38 2.5265 -4 1 3 4
35.76 7.91 2.5113 3 2 0 4
36.62 25.40 2.4538 -4 0 4 2
37.19 10.90 2.4177 1 1 4 4
37.59 4.51 2.3930 1 2 3 4
37.67 1.19 2.3876 -3 2 3 4
38.90 11.92 2.3153 -5 0 2 2
39.03 18.84 2.3080 -1 2 4 4
39.59 2.50 2.2762 1 3 0 4
40.18 3.81 2.2444 2 0 4 2
40.51 5.40 2.2270 0 2 4 4
40.67 1.11 2.2185 -4 2 1 4
40.97 2.92 2.2028 1 3 1 4
41.07 2.56 2.1977 -5 1 2 4
41.47 14.32 2.1776 4 0 2 2
41.47 2.06 2.1773 -3 2 4 4
41.55 21.15 2.1734 -1 3 2 4
41.65 1.61 2.1683 5 0 0 2
41.83 13.72 2.1596 0 3 2 4
42.25 2.70 2.1392 2 3 0 4
42.30 1.65 2.1368 2 1 4 4
43.00 1.11 2.1034 -2 3 2 4
43.53 3.26 2.0789 4 1 2 4
43.65 2.41 2.0736 1 2 4 4
43.98 6.98 2.0586 -2 0 6 2
44.11 2.50 2.0532 2 3 1 4
44.45 4.25 2.0382 -5 1 4 4
44.72 2.23 2.0266 -1 3 3 4
44.85 9.28 2.0209 -3 0 6 2
45.16 2.28 2.0079 4 2 1 4
45.96 5.74 1.9747 -2 1 6 4
46.04 8.49 1.9713 -3 3 2 4
46.62 8.52 1.9482 3 0 4 2
46.72 4.23 1.9442 -1 1 6 4
46.80 2.85 1.9412 -3 1 6 4
47.09 9.61 1.9297 -5 2 2 4
47.11 1.86 1.9291 5 1 1 4
47.13 3.42 1.9283 -6 0 2 2
47.15 6.67 1.9274 0 0 6 2
47.61 1.25 1.9099 -5 2 1 4
47.96 1.82 1.8969 -3 3 3 4
48.64 2.39 1.8720 3 3 1 4
49.01 4.02 1.8588 -6 1 2 4
49.03 2.86 1.8579 0 1 6 4
49.17 1.47 1.8531 4 1 3 4
49.32 4.72 1.8478 4 2 2 4
49.36 5.28 1.8464 -2 3 4 4
49.83 2.25 1.8298 5 0 2 2
50.32 5.75 1.8133 0 3 4 4
50.46 8.57 1.8087 -4 3 2 4
50.51 1.64 1.8069 6 0 0 2
50.95 1.45 1.7922 1 0 6 2
51.00 12.39 1.7906 -6 1 4 4
51.14 3.54 1.7862 -3 3 4 4
51.53 2.39 1.7734 -2 2 6 4
52.11 8.18 1.7552 3 3 2 4
52.30 3.24 1.7491 -3 2 6 4
52.40 1.65 1.7461 0 4 0 2
52.59 1.07 1.7402 5 2 1 4
52.93 4.12 1.7297 -5 1 6 4
53.01 12.56 1.7276 1 3 4 4
53.89 2.41 1.7013 3 2 4 4
53.90 1.33 1.7011 -6 1 5 4
54.35 3.66 1.6881 -6 2 2 4
54.37 1.46 1.6874 0 2 6 4
54.70 1.05 1.6779 -1 4 2 4
55.60 6.20 1.6530 4 1 4 4
56.55 2.58 1.6273 1 4 2 4
56.71 1.05 1.6231 -7 0 4 2
57.42 1.42 1.6048 6 2 0 4
58.43 1.95 1.5795 -3 4 2 4
58.73 3.32 1.5722 3 4 0 4
58.92 1.01 1.5674 -6 2 5 4
59.70 1.01 1.5488 7 0 0 2
60.26 2.71 1.5358 6 1 2 4
60.53 1.32 1.5295 4 2 4 4
64.26 3.80 1.4496 -6 3 4 4
65.98 1.10 1.4158 7 2 0 4
66.43 1.78 1.4073 -2 2 8 4
68.28 4.12 1.3737 4 3 4 4
68.93 1.04 1.3622 4 4 2 4
69.49 1.37 1.3527 2 5 0 4
69.67 6.48 1.3496 -5 2 8 4
69.92 2.48 1.3454 1 1 8 4
72.29 1.34 1.3071 -3 5 2 4
72.47 1.62 1.3041 6 3 2 4
73.69 1.23 1.2855 -3 3 8 4
74.32 1.04 1.2763 1 2 8 4
75.28 2.93 1.2624 -9 1 4 4
77.77 1.94 1.2281 1 5 4 4
79.24 1.13 1.2089 2 2 8 4
80.38 1.09 1.1946 -5 1 10 4
81.00 1.14 1.1871 9 1 0 4
81.46 1.01 1.1815 1 3 8 4
82.95 1.22 1.1641 0 6 0 2
83.20 1.03 1.1612 -4 2 10 4
83.52 2.29 1.1576 -8 2 8 4
83.83 1.95 1.1540 -2 4 8 4
86.04 1.01 1.1299 -4 5 6 4
86.34 1.11 1.1268 1 6 2 4
86.85 2.02 1.1215 -5 4 8 4
87.45 1.39 1.1153 -6 5 4 4
88.18 3.10 1.1080 3 6 0 4
88.18 2.02 1.1080 4 1 8 4
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XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs
For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.