Volkovskite Poulin R S, Grice J D The Canadian Mineralogist 51 (2013) 157-169 Volkovskite, a complex borate mineral: refined crystallographic data and optics Locality: New Brunswick, Canada _database_code_amcsd 0020421 6.535 24.185 6.589 92.626 119.132 97.298 P1 atom x y z Uiso U(1,1) U(2,2) U(3,3) U(1,2) U(1,3) U(2,3) K1 .0213 .0228 .0364 .0266 .0257 .0235 .0274 .0018 .0102 .0053 Ca1 .8127 .1649 .6598 .0125 .0125 .0153 .0103 .0014 .0059 .0021 Ca2 .7163 .5816 .3900 .0121 .0114 .0146 .0106 .0006 .0055 .0023 Ca3 .4952 .9069 .0217 .0122 .0120 .0146 .0104 .0009 .0059 .0012 Ca4 .1913 .4891 .3453 .0121 .0113 .0145 .0103 .0012 .0053 .0007 B1 .3001 .5993 .9027 .0095 .0074 .0153 .0065 .0008 .0038 .0014 B2 .3921 .9167 .4268 .0098 .0091 .0124 .0077 .0022 .0038 .0022 B3 .7658 .4710 .8406 .0096 .0084 .0136 .0074 .0012 .0044 .0016 B4 .3997 .1603 .1575 .0107 .0092 .0156 .0079 .0005 .0048 .0012 B5 .2369 .2648 .5598 .0146 .0162 .0174 .0079 .0009 .0040 .0023 B6 .7085 .1537 .0586 .0098 .0096 .0135 .0075 .0007 .0049 .0017 B7 .1590 .7007 .3302 .0143 .0179 .0139 .0090 .0004 .0051 .0013 B8 .5700 .3693 .1692 .0142 .0181 .0142 .0083 .0009 .0048 .0014 B9 .0792 .4800 .7489 .0086 .0078 .0124 .0058 .0010 .0033 .0020 B10 .8743 .8040 .8213 .0145 .0170 .0146 .0098 .0017 .0050 .0021 B11 .6090 .5900 .8024 .0087 .0083 .0125 .0059 .0009 .0040 .0014 B12 .8347 .2889 .7479 .0159 .0181 .0164 .0117 .0018 .0058 .0030 B13 .4549 .7819 .9840 .0159 .0178 .0169 .0113 .0009 .0061 .0003 B14 .0784 .9106 .5200 .0106 .0096 .0155 .0063 .0018 .0035 .0017 B15 .0375 .6112 .0812 .0087 .0082 .0128 .0058 .0004 .0040 .0011 B16 .9865 .8899 .1057 .0100 .0085 .0153 .0053 .0011 .0025 .0017 B17 .2203 .6126 .5060 .0088 .0083 .0118 .0064 .0009 .0036 .0017 B18 .4959 .4588 .0067 .0090 .0069 .0142 .0058 .0014 .0030 .0019 B19 .1356 .1714 .3345 .0098 .0079 .0156 .0061 .0004 .0035 .0019 B20 .3168 .1788 .7629 .0102 .0083 .0160 .0074 .0018 .0044 .0034 B21 .8098 .8975 .6853 .0097 .0082 .0154 .0047 .0008 .0025 .0017 B22 .6774 .4576 .4307 .0092 .0083 .0115 .0072 .0006 .0032 .0012 Cl1 .5277 .0221 .0626 .0229 .0296 .0174 .0217 .0003 .0130 .0005 O1 .1362 .1526 .5386 .0104 .0099 .0160 .0052 .0003 .0035 .0021 O2 .8165 .9147 .9059 .0099 .0096 .0152 .0048 .0026 .0034 .0015 O3 .0353 .9162 .7014 .0130 .0087 .0245 .0068 .0004 .0046 .0016 O4 .0383 .5866 .2787 .0087 .0081 .0131 .0044 -.0003 .0028 .0011 O5 .9155 .4876 .5228 .0103 .0071 .0172 .0057 -.0003 .0024 .0024 O6 .6037 .4675 .6101 .0109 .0081 .0188 .0055 .0010 .0033 .0012 O7 .1405 .6026 .6757 .0107 .0079 .0188 .0057 .0014 .0033 .0027 O8 .9045 .2535 .9137 .0211 .0300 .0181 .0101 .0012 .0055 .0036 O9 .8351 .5888 .8553 .0109 .0073 .0182 .0062 .0003 .0028 .0001 O10 .5405 .5983 .9708 .0115 .0076 .0204 .0067 .0010 .0039 .0008 O11 .3187 .9153 .5913 .0137 .0089 .0252 .0074 .0014 .0042 .0029 O12 .2415 .1666 .9329 .0129 .0087 .0251 .0068 .0028 .0049 .0042 O13 .0340 .6727 .1105 .0134 .0188 .0114 .0086 .0015 .0055 .0020 O14 .7819 .8348 .6378 .0146 .0205 .0141 .0072 .0015 .0052 .0008 O15 .5312 .8170 .1835 .0204 .0287 .0173 .0102 .0019 .0060 -.0002 O16 .2297 .9140 .1939 .0119 .0080 .0210 .0061 -.0005 .0030 .0015 O17 .7214 .4750 .0203 .0119 .0088 .0210 .0072 -.0001 .0050 .0012 O18 .3525 .1553 .3333 .0134 .0087 .0263 .0075 .0030 .0053 .0042 O19 .2712 .6721 .5221 .0133 .0167 .0113 .0080 -.0013 .0032 .0011 O20 .4415 .5823 .5691 .0102 .0068 .0170 .0053 .0027 .0020 .0005 O21 .6202 .9211 .4880 .0117 .0071 .0202 .0077 .0019 .0030 .0041 O22 .5104 .4833 .2283 .0090 .0091 .0132 .0048 .0027 .0035 .0015 O23 .0061 .4718 .9095 .0111 .0076 .0191 .0071 .0015 .0037 .0033 O24 .6387 .1586 .2269 .0123 .0081 .0226 .0069 .0017 .0041 .0020 O25 .9184 .9009 .2890 .0126 .0084 .0238 .0058 -.0002 .0038 .0008 O26 .3691 .8119 .7961 .0246 .0400 .0156 .0109 .0023 .0069 .0009 O27 .2546 .5951 .0794 .0116 .0082 .0215 .0072 .0021 .0050 .0031 O28 -.0197 .8278 .0486 .0147 .0185 .0145 .0078 .0017 .0039 .0018 O29 .5648 .3121 .1580 .0294 .0515 .0122 .0098 .00002 .0040 .0002 O30 .5512 .1576 .8302 .0121 .0088 .0213 .0069 .0030 .0040 .0031 O31 .9345 .1458 .1147 .0115 .0072 .0189 .0073 .0011 .0030 .0005 O32 .1291 .2338 .3465 .0149 .0210 .0137 .0075 .0010 .0048 .0020 O33 .3350 .2411 .7636 .0147 .0188 .0139 .0075 .0008 .0034 .0015 O34 .6954 .3979 .3891 .0131 .0168 .0114 .0074 .0024 .0029 .0012 O35 .8578 .7466 .7707 .0293 .0529 .0144 .0114 .0024 .0085 .0015 O36 .2440 .3223 .5641 .0286 .0486 .0153 .0110 -.0003 .0062 .0013 O37 .3054 .4811 .8030 .0107 .0072 .0179 .0072 .0017 .0034 .0034 O38 .7356 .2591 .5308 .0255 .0425 .0159 .0104 .0017 .0068 .0028 O39 .7159 .6769 .3867 .0250 .0382 .0154 .0134 .0030 .0065 .0005 O40 .8613 .3459 .7909 .0308 .0524 .0158 .0137 -.0010 .0083 .0006 O41 .1827 .7579 .3724 .0282 .0499 .0127 .0105 .0007 .0058 .0023 O42 .4596 .3970 .9764 .0130 .0178 .0119 .0071 -.0004 .0044 .0008 O43 .7371 .0651 .6034 .0262 .0335 .0195 .0220 -.0021 .0113 -.0004 O44 .2711 .0419 .5207 .0376 .0567 .0259 .0246 .0054 .0155 .0032 O45 .4643 .7253 .9727 .0296 .0512 .0157 .0131 .0045 .0091 .0008 O46 .1379 .3934 .2510 .0256 .0393 .0145 .0139 -.0021 .0059 .0024 H1 .9981 .2606 .0832 .05 H2 .6179 .8111 .3477 .05 H3 .5134 .3029 .0566 .05 H4 .3196 .7916 .6438 .05 H5 .8925 .7265 .9048 .05 H6 .3166 .3434 .7210 .05 H7 .6763 .2742 .3830 .05 H8 .7656 .7070 .5123 .05 H9 .6427 .6932 .2396 .05 H10 .8202 .3636 .6495 .05 H11 .1086 .7805 .2439 .05 H12 .5834 .0551 .5840 .05 H13 .7618 .1047 .5966 .05 H14 .2184 .0796 .5229 .05 H15 .2992 .0321 .6516 .05 H16 .3947 .7033 .8202 .05 H17 .0589 .3763 .0905 .05 H18 .1692 .3650 .3562 .05